• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2009.05a
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• pp.145-146
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• 2009

크롬 도금된 AISI 316L 스테인리스강에 펄스 바이어스를 사용한 유도결합 플라즈마로 질화 처리하여 고분자 전해질 연료전지용 분리판에 적합한 물성을 확인하였다.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.10 no.4
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• pp.96-101
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• 2011

The thin films of TiN have been used extensively as wear-resistant materials, for instance, such as tools of high-speed cutting, metal mold forming etc. In these days, because the thin films capable of being used more severe conditions are needed, the technologies of arc ion plating are tried to improve its characteristics. The purpose of this study is to investigate the characteristics of thin films of (Ti,Cr)N compared with those of TiN. The method of arc ion plating, which is known as showing good tight-adherence and productivity, was used. After manufacturing thin films of ($Ti_{1-x}Cr_{x}$)N (x=0~1) with change of Cr in (Ti,Cr) target, atomic concentration, structure, size of crystallite, residual stress and surface roughness of thin films on substrate were investigated. As the results, it was confirmed that Cr atomic concentrations of thin films were proportionally changed with Cr atomic concentrations of target, and thin films of ($Ti_{1-x}Cr_{x}$)N (x=0~1) showed NaCl type and CrN existed as solid solution to TiN.

• Journal of the Korean institute of surface engineering
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• v.34 no.3
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• pp.231-239
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• 2001

The structure and composition of Cr-nitrides formed on an electroplated hard Cr layer during an ionnitriding process was analyzed, and the growth kinetics of the Cr-nitrides was examined as a function of the ion-nitriding temperature and time in order to establish a computer simulation model prediction the growth behavior of the Cr-nitride layer. The Cr-nitrides formed during the ion-nitriding at $550~770^{\circ}C$ were composed of outer CrN and inner $Cr_2$N layers. A nitrogen diffusion model in the multi-layer based on fixed grid FDM (Finite Difference Method) was applied to simulate the growth kinetics of Cr-nitride layers. By measuring the thickness of each Cr-nitride layer as a function of the ion-nitriding temperature and time, the activation energy for growth of each Cr-nitride was determined; 82.26 KJ/mol for CrN and 83.36 Kj/mol for $Cr_2$N. Further, the nitrogen diffusion constant was determined in each layer; $9.70$\times$10^{-12}$ /$m^2$/s in CrN and $2.46$\times$10^{-12}$ $m^2$/s in $Cr_2$N. The simulation on the growth kinetics of Cr-nitride layers was in good agreements with the experimental results at 550~72$0^{\circ}C$.

• Proceedings of the Korean Society Of Semiconductor Equipment Technology
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• 2003.05a
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• pp.98-105
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• 2003

반도체 집적회로 제조 장치의 부품으로 사용되는 전도성 발열체를 박막형태로 제조하는 기술을 얻기 위하여 반도체와 금속을 혼합한 물질을 스퍼터 증착 기술 및 전자빔 증착기술을 이용하여 제작하고, 전기적, 재료적 특성을 분석하였다. 발열재료로는 몰리부덴과 실리콘 및 크롬 및 실리콘의 합금을 이용하였으며, 기판 물질은 알루미나와 실리콘질화막. 시리콘 산화막을 사용하였다. 발열물질은 온도의 상승파 하강에도 안정된 재료적 성질을 가져야 제품으로써 신뢰도를 유지할 수 있으므로 금속 (몰리부텐 또는 크롬) 실리사이드 (silicide)의 최종 phase 를 갖도록 하였는데, 실리사이드는 실리콘과 금속의 합금물질로 안정된 재료로 알려져 있다. 또한 발열재료의 온도저항계수를 최소화하도록 하였으며 온도저한계수 값의 범위가 20% 이내인 발열재료의 제조기술을 얻었다. 이러한 온도저항계수 최소화는 열교환 부품의 온도 정밀제어를 가능하게 한다.

• Journal of the Korean Society for Precision Engineering
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• v.17 no.5
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• pp.160-167
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• 2000

In this research, the fatigue behaviors of carbonitrided Cr-Mo(SCM415) steel are examined. From fatigue test results, we propose a modified fatigue strength evaluation model and modified formulae. That is, we develop improved models fur evaluating and predicting the fatigue strength of carbonitrided SCM415 by modifying specific terms in the Murakami and Endo's model which is the representative fatigue strength evaluation formulae fur high strength steel.

• Journal of the Korean Society for Precision Engineering
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• v.15 no.8
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• pp.135-144
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• 1998

In this research, the fatigue behaviors of Cr-Mo(SCM415) steel and carbonitrided CrMo(SCM415) steel are examined. The description of experiments in detail as follows. For SCM415 and carbonitried Cr-Mo(SCM415) steel, smooth specimens and hole defected specimens are fabricated and tested under a rotary bending tester, respectively. By performing the rotary bending fatigue test for smooth and hole defected specimens, the characteristics of the fatigue strength are examined for parameters such as tensile strength, hardness at surface, and residual stresses.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 1999.05a
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• pp.692-695
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• 1999

This paper presents annealing characteristics of CrN thin-film strain gauges, which were deposited on glass by DC reactive magnetron sputtering in an argon-nitrogen atmosphere)Ar-(5-~25%)$N_2$. The physical and electrical characteristics of these films investigated with the thickness range 3500$\AA$ of CrN thin films, annealing temperature (100~30$0^{\circ}C$) and annealing time (24-72hr) . The optimized condition of CrN thin-film strain gauges were thickness range of 3500$\AA$ and annealing condition(30$0^{\circ}C$ , 48hr) in Ar-10%$N_2$ deposition atmosphere. Under optimum conditions, the CrN thin-films for strain gauge is obtained a high resistivity, $\rho$=1147.65$\Omega$cm a low temperature coefficient of 11.17. And change in resistance after annealing for the CrN thin film were quitely linear and stable.

• Proceedings of the KSME Conference
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• 2004.04a
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• pp.722-727
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• 2004

This paper includes the comparative study between Cr plating and nitriding process with an aim at improving corrosion, wear and maintainability for KNR(Korean Next Generation Rifle) 5.56mm barrel. The endurance test was conducted to compare the performance of standard barrel, Cr plating barrel and nitriding barrel. Main activities are described as follows; optimal Cr plating and nitriding process set-up for KNR 5.56mm barrel; durability test of each barrel(20,000 rounds); salt water immersion test; dispersion, initial velocity, inner diameter data acquisition. According to the results of this firing test, Cr plating barrel is superior to standard barrel and nitriding barrel in view of corrosion, wear and maintainability

• Journal of the Korea Institute of Military Science and Technology
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• v.7 no.1
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• pp.5-12
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• 2004

This paper includes the comparative study between Cr plating and nitriding process with an aim at improving corrosion, wear and maintainability for KNR(Korean Next Generation Rifle) 5.5mm barrel. The endurance test was conducted to compare the performance of standard barrel, Cr plating barrel and nitriding barrel. Main activities are described as follows; optimal Cr plating and nitriding process set-up for KNR 5.56mm barrel; durability test of each barrel(20,000 rounds); salt water immersion test; dispersion, initial velocity, inner diameter data acquisition. According to the results of this firing test, Cr plating barrel is superior to standard barrel and nitriding barrel in view of corrosion, wear and maintainability.

• Journal of Dental Rehabilitation and Applied Science
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• v.32 no.3
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• pp.194-201
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• 2016

Purpose: The purpose of this study was to evaluate of Zirconium Nitride (ZrN) coating on shear bond strength with denture base resin in Co-Cr and Ti-6Al-4V alloy. Materials and Methods: Co-Cr and Ti-6Al-4V alloy disks (10 mm in diameter, 2.5 mm in thickness; each other: n = 14) were prepared and divided with 2 groups each other by ZrN coating. After primer was applied to disks surface, denture base resin with diameter 6 mm, height 5 mm was bonded on metal disk surface. After surface roughness was measured by Profiler, shear bond strength was determined with Universal testing machine and analyzed with two-way ANOVA. The specimen surfaces and failure mode were examined using a scanning electron microscope. Results: ZrN coated groups showed significantly higher rough surface than non-coated groups (P < 0.05). Irrespective of alloy materials, shear bond strength of ZrN coated groups were lower than non-coated groups (P < 0.001). The scanning electron microscope (SEM) of ZrN coated groups showed mixed and adhesive fractures. Conclusion: ZrN coating weakened bonding strength between denture base resin and Co-Cr, Ti-6Al-4V alloy.