• Journal of the Korea Institute of Military Science and Technology
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• v.7 no.3 s.18
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• pp.110-121
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• 2004

Pyrolysis-mass spectrometry, incorporating an in situ thermal hydrolysis and methylation(THM) step, has been used to study biological materials for bacteria, toxin and virus. Newly developed pyrolyzer was used to decompose biological materials, and tetramethylammonium hydroxide(TMAH) was used as a methylation reagent. Chemical ionization(CI) using ethanol and ion trap mass spectrometer(ITMS) were used to ionize and analyze of pyrolysis components, respectively. Analytical characteristics of bacteria (including spore), virus and toxin were analyzed. Also acquisition and interpretation of mass spectra as biomarkers for classification/identification of biological material s were explained.

• Proceedings of the KAIS Fall Conference
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• 2008.11a
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• pp.113-116
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• 2008

본 연구에서는 차량-교량간 상호작용효과가 교량의 동적거동에 미치는 영향을 분석하기 위한 차량 주행 하중에 대한 실험적 및 이론적 연구를 수행하였다. 이를 위하여 차량 교량간 상호작용이 포함된 이동질량형 윤하중 실험기를 단순교형식 교량에 적용하여 반복주행실험을 수행하였다. 이동질량 반복 주행실험 결과를 분석하여 차량-교량간의 상호작용을 포함한 가속도 형태의 실동주행차량가속도를 규명하였다. 규명된 차량의 실동주행차량가속도를 범용 해석프로그램에 적용하여 차량-교량 상호작용을 재현할 수 있었다. 또한 차량주행시 교량의 사용성평가에 대한 기본자료를 판단할 수 있었다.

• The Bulletin of The Korean Astronomical Society
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• v.37 no.2
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• pp.178.2-178.2
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• 2012

정지궤도위성은 발사체에서 위성이 분리된 이후 천이궤도로부터 원하는 목표궤도로 궤도전이를 해야 한다. 또한 임무기간동안 궤도상에서 다양한 교란을 겪게 되며 이로 인해 시간이 증가함에 따라 위성의 위치가 변화하게 된다. 정지궤도위성은 이러한 궤도전이 및 궤도상 위치변화를 제어하기 위한 추진시스템을 장착하고 임무기간에 걸쳐 요구되는 추진제를 탑재해야 한다. 위성의 설계 초기에는 추정되는 위성의 건조질량을 기반으로 하여 궤도전이와 궤도상 임무에 필요로 하는 추진제 버짓을 계산하고 이를 토대로 하여 위성 시스템 설계를 진행한다. 또한 발사체별로 발사체의 성능과 발사장에 따라 근지점고도와 발사 경사각이 모두 상이하므로 발사체가 정해지지 않은 상태에서 발사체별 추진제 버짓을 계산, 비교하고 추진 시스템의 탱크가 이를 모두 수용할 수 있는지 분석하는 것이 중요하다. 본 논문에서는 정지궤도복합위성의 추정 건조질량과 임무분석을 통해 주어진 ${\Delta}V$와 각 발사체별 궤도전이에 필요한 ${\Delta}V$를 바탕으로 하여 발사체별 추진제버짓을 계산하였고 이를 비교검토 하였다. 이후 이러한 기본 자료를 바탕으로 하여 정지궤도복합위성 추진시스템의 추진제 수용가능 여부, 건조질량 증가 여유 등 기본설계를 진행할 수 있다.

• Journal of the Korean Vacuum Society
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• v.3 no.2
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• pp.173-178
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• 1994

박막성장을 위한 초고진공 응용시스템을 제작하고 이것의 특성을 사중극질량분석계로 측정하였 다. 초고진공 시스템을 박막성장에 활용하기 위해서는 챔버 뿐만 아니라 펌프, 이온게이지, 전자총 등도 베이킹이 요구되었다. 또한 이온게이지와 전자총은 적어도 박막성장 20분전에 탈가스를 하여야함을 알 았다. 이 시스템으로 달성된 진공도는 7x10-11 torr이었다.

• Journal of Convergence for Information Technology
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• v.9 no.6
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• pp.1-6
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• 2019

In this study, the development of a weight estimation model of electronic scale with nonlinear characteristics is presented using polynomial regression analysis. The output voltage of the load cell was measured directly using the reference mass. And a polynomial regression model was obtained using the matrix and curve fitting function of MS Office Excel. The weight was measured in 100g units using a load cell electronic scale measuring up to 5kg and the polynomial regression model was obtained. The error was calculated for simple($1^{st}$), $2^{nd}$ and $3^{rd}$ order polynomial regression. To analyze the suitability of the regression function for each model, the coefficient of determination was presented to indicate the correlation between the estimated mass and the measured data. Using the third order polynomial model proposed here, a very accurate model was obtained with a standard deviation of 10g and the determinant coefficient of 1.0. Based on the theory of multi regression model presented here, it can be used in various statistical researches such as weather forecast, new drug development and economic indicators analysis using logistic regression analysis, which has been widely used in artificial intelligence fields.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.44 no.4
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• pp.281-289
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• 2016

Accurate prediction of the trajectory and time of a time-varying mass parachute system remains essential in the mission requiring a precision airdrop to the ground. In this study, we investigate the altitude-varying behavior of a cross-type parachute system designed to deliver a time-varying mass object like flare. The dynamics of the descending parachute system was analyzed based on the Runge-Kutta method of the ordinary differential system. The drag coefficients of the cross-type parachute and flare were calculated by a CFD code based on the incompressible Navier-Stokes equation. Finally, by using a simplified gust wind model in troposphere, the combined effects of gust wind and time-varying mass were examined in detail.

• Analytical Science and Technology
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• v.18 no.6
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• pp.483-490
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• 2005

Mass resolution of the time of flight aerosol mass spectrometer for an aerosol component analysis depends on the initial direction and the initial energy of the ions. We have found that the shape of the optimum post focusing electric field is not linear. The maximum electric potential should be applied to the ions whose initial direction is 90 degree. To check on the post focusing effects, we have installed a laser ablation mass spectrometer. By using this LA-MS, we have found that the average energy distribution of the laser ablated ions is 8 eV. To establish the optimum mass resolution, a time delay and a high voltage are needed, and the results of the study show that 1500 nsec, and 3.7 kV are the optimum parameters for our system respectively. The isotope mass signals of copper show a good resolution.

• The Journal of the Petrological Society of Korea
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• v.10 no.3
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• pp.157-171
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• 2001

This study investigated the effects of Pb/Tl ratio, Pb concentration and concomitant matrix elements on the measurement of Pb isotope ratios using multi-collector ICP/MS (AXIOM MC model). Accuracy and reproducibility of Pb isotope ratios in NBS 981 solution were estimated for 42 data measured from March to August 2001. Pb isotopes measured in rocks, bronzes and sediments were compared to data measured by TIMS. Reproducibilities for $^{206}Pb/^{204}Pb,\; ^{207}Pb/^{204}Pb,\;and\;^{208}Pb/^{204}Pb$ ratio were about 500 ppm (2sd) and for $^{207}Pb/^{206}Pb$\;and\;^{208}Pb/^{206}Pb$ were 100~200 ppm for 200 ng of Pb in NBS 981 solution. The optimum conditions for the analysis of Pb isotope ratios with AXIOM MC for best accuracy and reproducibility were defined as follows; 1) Pb/Tl ratio is about 10 2) Pb concentration is about 100 ng/ml 3) correction for mass discrimination is performed by exponential law using 2.3887 of $^{205}Tl/^{203}Tl$ and Pb mass fractionation factor empirically obtained from $ln(^{208}Pb/^{206}Pb)-ln(^{205}Tl/^{203}Tl)$ relationship. The sample data measured with MC/ICP/MS for acid-digested and chemically separated rock samples, and acid-digested bronze samples and sediment samples coincide with those of TIMS within analytical errors. Therefore, MC/ICP/MS is a rapid analytical technique for Pb isotope ratios with the similar precision compared with TIMS.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.6 no.2
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• pp.134-143
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• 2005

Collagen is the important structural proteins in mammals with various peptide composition and cross-linkings. The direct analysis of collagen protein was not suitable because of its structural complexity and diversity. In this study, we suggest the simple way of collagen analysis by introducing matrix-assisted laser desorption/ionization time-of flight mass spectrometry (MALDI-TOF MS) to identify the collagen and its trypsin-digested fragments, and by subsequent time-of-flight tandem mass spectrometry(Q-TOF MS/MS) to analyze the amino acid sequences of identified fragments. Using the collagen samples extracted from the tail of mouse, 10 separated bands were found in SDS-PAGE, and the masses of most bands could be more finely determined by MALDI-TOF MS. When each 10 separated proteins was tryptic digested and introduced to MALDI-TOF, the Gly1056-Arg1073 fragment from $\alpha_1$-chain was identified in four bands, and the Gly1056-Arg1073 fragment from $\alpha_2$-chain was identified in five bands, both in type I collagen. Although few fragments were found because of the cross-linkings left in digested collagen sample, it could be determined that the type I collagen existed at least in 7 separated bands. When the amino acid sequences of two identified fragments were analyzed by Q-TOF MS/MS, both sequences were identical with those determined by MALDI-TOF MS. It suggested that the two peaks in MALDI-TOF MS caused by the fragments identified in this work could be used as the fingerprint to simply identify type I collagen in protein samples.

• Membrane Journal
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• v.15 no.4
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• pp.297-309
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• 2005

As a number of potential endocrine disrupting compounds (EDCs) are released into the environment, recently growing attention has been drawn to them. Therefore sensitive and reliable analytical methods are essential to monitor those compounds. In this study, complementary CC-MS and LC-MS were employed to analyze the endocrine disrupters, and the results of two methods were compared for di(2-ethylhexyl)phthalate (DEHP), benzylbutylphthalate (BBP), pentachlorophenol (PCP), and 4,4'-Isopropylidenediphenol (Bisphenol-A, or BPA). The results indicate that it was possible to lower the detection limits of EDCs by LC-MS. Also, LC-MS enabled to identify the EDCs as almost intact molecules. Furthermore, this study presented a nanofiltration membrane (MWCO 250) and a ultrafiltration membrane (MWCO 1,000) filtration system as methods far removing EDCs from drinking water containing $\gamma$-BHC, p,p'-DDE, BBP, p,p'-DDT, DEHP, PCP, and BPA. Cross-flow type nanofiltrations showed $100\%$ removal of EDCs, and the result implies that MWCO 250 nanofilter was sufficient for treatment of EDCs. The ratio of permeate flux to mass transfer coefficient of nanofiltration, high flux ultrafiltration, and low flux ultrafiltration with ultrapure water were 0.67, 3.4, and 0.44, respectively. It was found that nanofiltration and low flux ultrafiltration were operated at a diffusion dominant condition, and the high flux ultrafiltration was operated at a convection dominant condition. Furthermore, a diffusion dominant process attained reasonable rejection of EDCs. The removal in the ultrafiltration was depending on the molecular weight of an EDC, and the filtration was governed by diffusion-dominant hydrodynamic conditions.