• Title/Summary/Keyword: 질량 분석

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Nano-Bio Surface Analysis

  • Lee, Tae-Geol
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.02a
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    • pp.88-88
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    • 2013
  • 최근 각광을 받고있는 나노바이오 질량이미징 분석법의 측정원리를 이해하고, 세포/생체조직/생체샘플/바이오칩의 측정결과를 바탕으로 핵심측정 능력을 파악하여 각자의 연구에 적용 가능성을 탐색할 수 있는 역량을 배양하고자 한다.

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Determination of Plutonium in HANARO Irradiated Fuel by IDMS (동위원소희석 질량분석법에 의한 조사 후 하나로 핵연료 중 Pu 정량)

  • Jeon, Young Shin;Son, Sae Chul;Kim, Jung Suk
    • Analytical Science and Technology
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    • v.16 no.3
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    • pp.191-197
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    • 2003
  • Two methods, IDMS (Isotope Dilution Mass Spectrometry) and controlled potential coulometry are compared by the determination of Pu for the NBL, CRM No.122, $PuO_2$. The recovery of Pu was found to be $1.002176{\pm}0.000452$ within the relative standard deviation of 0.045% (95% conf. level) although a small size of sample ($0.9{\mu}g$-Pu) was used in IDMS. The recovery using controlled potential coulometry were obtained in the range of 0.9923~0.9960. The analytical results of IDMS and controlled potential coulometry were good agreement within 0.6~1%. Base on these experiment results, The plutonium in HANARO irradiated fuel rod that separated portion of top, middle, and bottom were determined. The measured values of Pu are 1.155 mg, 2.483 mg and 1.920 mg in one gram of sample(fuel+clad), respectively.

An experimental study on the effect of mass injection location and flow rate for tip vortex cavitation of 3D hydrofoil (수중익 날개 끝 보텍스 캐비테이션 제어를 위한 질량분사 위치 및 분사량 영향에 대한 실험적 연구)

  • Eunsue Hwang;So-Won Jeong;Hongseok Jeong;Hanshin Seol
    • The Journal of the Acoustical Society of Korea
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    • v.42 no.3
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    • pp.233-242
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    • 2023
  • In this paper, the effect of mass injection on the control of tip vortex cavitation was studied experimentally. A mass injection system for a 3D hydrofoil was designed to control the location of injection as well as the injection rate. A series of cavitation tests were carried out in a cavitation tunnel for different injection locations and rates. The cavitation behaviour was observed using a high-speed camera and the corresponding noise was measured using a hydrophone installed in the observation window. The results showed that the tip vortex cavitation was suppressed under certain conditions and the noise was reduced in some frequency bands. It was also found that there is a location where the effect of mass injection could be maximized and hence the noise reduction.

Mass Spectra of Chlorinated Organophosphorus Pesticides (염소화 유기인제 농약의 질량 분석법)

  • Hong, Jongki;Eo, Yunwoo;Rhee, Jaeseong;Kim, Taekjae;Kim, Kangjin
    • Analytical Science and Technology
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    • v.6 no.1
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    • pp.93-106
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    • 1993
  • Fragmentation patterns on electron impact of 8 chlorinated organophosphorus pesticides were investigated. In most cases, characteristic ions could e identified and the peak clusters due to the $^{35}Cl$ and $^{37}Cl$ isotopes in the fragment ions were found to be highly characteristic. The fragmentation patterns of phosphorus moiety were coincident with previous report in the aspect of mechanism.

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The Observations of Water, Carbon Dioxide, Hydrgen, Nitrogen, Oxygen, Carbon Monoxide and Methane as Impurities in Natural Garnets (석류석의 불순물인 물, 이산화탄소, 수소, 질소, 산소, 일산화탄소 및 메탄의 고찰)

  • R. Everett Langford;A. A. Giardini;Charles E. Melton
    • Journal of the Korean Chemical Society
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    • v.17 no.5
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    • pp.353-356
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    • 1973
  • A unique method of destructive analysis has been developed for the study of gaseous impurities in minerals. Samples are crushed in a high vacuum sample system of a research mass spectrometer. This is done by means of a suitably designed crusher which is incorporated in the inlet system of the instrument. Crusher elements are constructed of tungsten carbide. The mass spectrometer used for this preliminary study has a detection sensitivity of about $10^{-10}cc$at STP. In a study of rhodolite garnets obtained from near Lavonia, Georgia, U.S.A., the gases$H_2$, $O_2$, $H_{2}O$, $CO_2$, CO, and $CH_4$have been identified and their composition determined.

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BIACORE 바이오센서를 이용한 B형 간염 표면항원 정량분석의 기초연구

  • Yu, Chang-Hun;Ryu, Gang;Jeon, Jun-Yeong;Lee, Hyeon-Ik;Choe, Seong-Cheol;Lee, Eun-Gyu
    • 한국생물공학회:학술대회논문집
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    • 2001.11a
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    • pp.231-234
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    • 2001
  • We performed a basic experiment for rapid. on-line, real-time measurement of HBsAg by using a BIACORE biosensor, a chip-based sensor utilizing surface plasmon resonance technology to quantify the recognition and interaction of biomolecules. We immobilized an a -HBsAg antibody on a CM5 chip surface which was activated by N-hydroxysuccinimide for amine coupling with HBsAg, and measured the mass increase from the coupling. This study showed the potential of this biosensor-based method as a rapid, multi-sample, on-line assay. Once properly validated, it can serve as a more powerful method for HBsAg quantification.

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A Real Vehicle Tracking Acceleration Using A Tire-Wheel-Tracking Machine (제작차륜이동 시험기의 실동주행 가속도측정)

  • Sung, Ikhyun;Seung, Seoungyoul
    • Journal of the Society of Disaster Information
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    • v.7 no.3
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    • pp.190-197
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    • 2011
  • In this paper, an analytical and experimental study is performed in order to determine the effects of interaction between a vehicle and a structure. For this purpose, a wheel tracking machine and an adequate single span bridge are designed. Results presented in the paper show that the real vehicle tracking accelerations including the interaction between the vehicle and the structure produce additional effects on the dynamic behavior of the structure including reversal and contrary behavior. Also, the interaction between the vehicle and the bridge is reproduced by applying the identified real vehicle tracking accelerations to a general finite element analysis program.

A Study on Piano String Vibration (피아노현의 진동에 관한 연구)

  • Kang, T.-H.;Yoon, Y.-K.;Lee, S.-J.
    • The Journal of the Acoustical Society of Korea
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    • v.8 no.1
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    • pp.13-22
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    • 1989
  • This study made an analysis of the characteristics of vibration & tone color of the piano strings on which a concentrated mass was set to give variety of different variations to the gamut. Theoretical analyses in this study were based on discrete and continuous system, of which the former was transformed into a multi-degree of freedom system by dividing into a number of small parts, while the latter utilized mode summation and Laplace transformation methods. And experiments were carried out with setting concentrated masses on upright piano string.

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냉각재상실사고시 질량 및 에너지 방출량 감소를 위한 고찰

  • 허재영;이남호;정재훈;권영민;이상종
    • Proceedings of the Korean Nuclear Society Conference
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    • 1996.05b
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    • pp.399-404
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    • 1996
  • 1000MWt 급 가압경수로의 질량 및 에너지 방출량을 감소시키기 위한 방안으로 울진 3,4호기를 기준으로 안전주입계통의 형태 및 용량을 변화시키면서 원자로냉각재펌프 토출관 및 고온관 파단에 대한 질량 및 에너지 방출량 계산과 격납건물 첨두압력 및 온도의 민감도를 분석하여, 후속호기 설계에 활용하고자 한다. 분석한 여러 경우 중에서, 토출관 파단사고시 안전주입탱크 용량은 변화시키지 않고 고압안전주입펌프 용량을 l75%로 증가시키면서 저압안전주입펌프를 제거하였을 경우가 격납건물 첨두압력 및 온도가 61.98 psia (3.32 kg/$\textrm{cm}^2$A), 288.03 ℉ (142.24$^{\circ}C$)로써 가장 낮게 나타났다. 이러한 결과는 격납건물의 설계여유도를 기존보다 더 확보하므로 안전성이 향상 될 뿐만 아니라. 저압안전주입펌프를 안전주입계통에서 제외함으로써 발전소 운전에도 큰 도움이 될 것이다.

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