• Title/Summary/Keyword: 진공압추출법

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2-D Simulation of Fiber Orientation in Short Fiber Preform (단섬유 예비성형체의 섬유배향에 대한 2차원 수치모사)

  • 정성욱;남현욱;정창규;한경섭
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 1999.11a
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    • pp.107-110
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    • 1999
  • 본 연구에서는 진공압추출법에 의해 제조되는 알루미나(AI$_2$O$_3$) 단섬유예비성형체의 제조공정시 발생하는 섬유들의 배향분포의 특징을 2차원 수치모사를 통해 밝혔다. 수치해석은 섬유의 배향분포를 2차원으로 가정한 후 제조공정시 섬유들이 적층되는 현상을 섬유의 낙하, 회전, 미끄러짐, 이동의 단계의 나누어 모델링하였다. 해석결과 섬유의 배향과 부피분율은 섬유의 종횡비(길이/지름)에 의해 크게 영향을 받으며, 배향 분포는 정규분포와 유사한 것으로 밝혀졌다.

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Study on the Improvement for Measuring Procedures of Volumetric Pressure Plate Extractor (체적압력판추출기의 측정법 개선에 관한 연구)

  • Yoo, Kun-Sun
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.30 no.4C
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    • pp.185-191
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    • 2010
  • Volumetric pressure plate extractor (VPPE) can be used for measurement of the soil-water characteristic curve in the laboratory using the axis-translation technique. The volume of extracted water from the soil specimen in VPPE can be measured continuously during the test without stoppage of air pressure for the measurements. However, the water volume measurement in VPPE using an air trap, a ballast tube, a burette, and a vacuum device so as to maintain a constant pore-water pressure in the soil specimen, is quite complicated and tedious. In order to improve the measuring problems of VPPE, a modified volumetric pressure plate extractor (MVPPE) was developed and tested on residual soil specimens. In addition, the modified apparatus can measure the volume of the extracted water using both Method A and Method B of ASTM D 6836-02 depending on the range of matric suction. Measuring principles and the improvements of MVPPE and typical results obtained from the tests are discussed in the paper.

Development of a Noble Gas Isotope Dilution Mass Spectrometric System Combined with a Cryogenic Cold Trap (초저온 냉각 트랩을 결합한 비활성기체 동위원소 희석 질량분석 시스템의 제작)

  • HONG, BONGJAE;SHIN, DONGYOUB;PARK, KEYHONG;HAHM, DOSHIK
    • The Sea:JOURNAL OF THE KOREAN SOCIETY OF OCEANOGRAPHY
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    • v.27 no.3
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    • pp.144-157
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    • 2022
  • Noble gases, which are chemically inert and behave conservatively in marine environments, have been used as tracers of physical processes such as air-sea gas exchange, mixing of water masses, and distribution of glacial meltwater in the ocean. For precise measurements of Ne, Ar, and Kr, we developed a mass spectrometric system consisting of a quadrupole mass spectrometer (QMS), a high vacuum preparation line, an activated charcoal cryogenic trap (ACC), and a set of isotope standard gases. The high vacuum line consists of three sections: (1) a sample extraction section that extracts the dissolved gases in the sample and mixes them with the standard gases, (2) a gas preparation section that removes reactive gases using getters and separates the noble gases according to their evaporation points with the ACC, and (3) a gas analysis section that measures concentrations of each noble gas. The ACC attached to the gas preparation section markedly lowered the partial pressures of Ar and CO2 in the QMS, which resulted in a reduced uncertainty of Ne isotope analysis. The isotope standard gases were prepared by mixing 22Ne, 36Ar, and 86Kr. The amounts of each element in the mixed standard gases were determined by the reverse isotope dilution method with repeated measurements of the atmosphere. The analytical system achieved precisions for Ne, Ar, and Kr concentrations of 0.7%, 0.7%, and 0.4%, respectively. The accuracies confirmed by the analyses of air-equilibrated water were 0.5%, 1.0%, and 1.7% for Ne, Ar, and Kr, respectively.