• Analytical Science and Technology
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• v.10 no.3
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• pp.216-224
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• 1997

In the study of cyclic voltammogram of rubeanic acid, rubeanic acid has two reduction peaks; first peak is similar with that of $S^{2-}$ and thiourea, which is conceded to by HgS, second peak is very weak and unidentified. The study also describes the differential pulse cathodic stripping voltammetric method for the determination of rubeanic acid. The followings were optimal conditions of rubeanic acid for the study : 0.05M borate buffer solution(pH 10.0) ; an accumulation potential of -0.30V(vs. Ag/AgCl); accumulation time of 120sec. : scan rate of 10mV/sec. The detection limit of trace analysis shows $2.7{\times}10^{-8}M$ of rubeanic and at optimal conditions.

• Journal of Food Hygiene and Safety
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• v.5 no.4
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• pp.213-217
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• 1990

A simple and practical method for the determination of caffeine in coffee, black tea and green tea was studied. The analysis of caffeine was performed by reverse phase high perfomance liquid chromatography using a ${\mu}-Bondapak$ C18 column at isocratic condition with methanol-acetic acid-water (20: 1: 79) on UV detector at 280 nm. The extraction and clean-up of caffeine in sample is based on combing a simple pretreatment with the use of a Sep-Pak Alumina A cartridge. The average recoveries of caffeine from several samples were 95.2 -101.3%, the relative standard deviation for the whole procedure was 0.10 ~ 0.62%, and the detection limit of caffeine in sample solution was about $0.1\;\mu\textrm{g}\;per\;ml$.

• Analytical Science and Technology
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• v.6 no.3
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• pp.313-318
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• 1993

The rose petal tissue biosensor has been constructed by immobilizing New carina rose tissue. Optimum conditions for the determination of urea were investigated using this sensor. Selectivity and life time of this sensor were also obtained. As a result, the biosensor showed the optimum response characteristics in 0.20M phosphate buffer solution at pH 8.0, $37^{\circ}C$ and 50mg of tissue amounts. This sensor was linear from $9.0{\times}10^{-5}$ to $4.0{\times}10^{-3}M$ urea with a slope of 42mV/decade. The limit of detection and response time are $7.0{\times}10^{-5}M$ and 17~19 min.

• Journal of the Korean Applied Science and Technology
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• v.30 no.4
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• pp.664-671
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• 2013

Determination of xanthan gum as watersoluble-polymer in commercial cosmetic samples was carried out by High Perfomance Liquid Chromatography(HPLC). An $C_{18}$ reversed-phase column and the selected ELSD detector was applied. The 25mM ammonium acetate/acetonitrile was used for the mobile phase of gradient conditions. The analysis results of HPLC showed good linearity with correlation coefficient of $r^2=0.9993$ in the rage of $50.3{\sim}604.1{\mu}g/ml$ and detection limit of $12.0{\mu}g/ml$.

• Proceedings of the Korea Water Resources Association Conference
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• 2008.05a
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• pp.1116-1120
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• 2008

댐은 사회경제적으로 다양한 편익을 제공하고 있지만, 댐을 철거하자는 많은 NGO와 다른 환경단체들이 주장하는 생태비용의 이유로 최근에 재평가를 시행하고 있다. 댐 건설로 인한 유사의 차단과 첨두 홍수량의 감소는 하천의 장갑화와 유사의 하구이송을 감소시켜 댐 직하류 하천에 영향을 미치고 있다. 이러한 직 간접적인 영향들은 하도 내에 물리적 서식처 형상, 생태학적 연관성, 이로 인해 하천지형학에서의 변화를 초래하게 된다. 댐 운영이 하류의 하도 및 생태계에 미치는 영향 정도를 정량화하는데 있어 기존의 단순한 유황 분석을 통한 갈수량, 저수량, 평수량, 풍수량은 댐으로 인한 하류 하천의 영향을 정량적으로 분석하는 데는 한계가 있다. 따라서 본 연구에서는 다양한 수문변화를 정량적으로 계산할 수 있는 IHA(Indicators of Hydrologic Alteration) 모형을 이용하여 합천댐 직하류 하천의 수문변화 특성을 분석하였다. 댐의 유입량과 방류량을 비교한 결과, 대체적으로 홍수기(6월$\sim$9월)에는 댐에 의한 유량 조절효과로 첨두량이 감소하였으며, 그 이외의 월 평균유량은 증가하여 유황이 개선되는 경향을 나타났으며, 수문변화율은 댐의 방류량이 유입량보다 작게 나타났다. 본 연구에서 산정된 수문특성 변화 지표는 댐 유역의 치수, 이수, 환경생태적인 변화를 종합적으로 이해하고 적응하는데 있어, 댐 운영을 최적화하거난 효과적으로 이용될 수 있을 것으로 판단된다.

• Journal of the Korean Applied Science and Technology
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• v.29 no.4
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• pp.585-593
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• 2012

The EO separation and quantitative determination of polysorbate 20, polysorbate 40, polysorbate 60 and polysorbate 80 was carried out by reversed phase HPLC. The water/acetonitrile was used for the mobile phase of gradient conditions. An YMC Pack Ph ($250mm{\times}4.6mm$ i.d., $5{\mu}m$) and Phenomenex C4 ($250mm{\times}4.6mm$ i.d., $5{\mu}m$) and the selected ELSD detector was applied. The analysis results of HPLC showed good linearity with correlation coefficient of $r^2$=0.997 in the rage of $180.2{\sim}980.5{\mu}g/mL$ and detection limit.

• Journal of the Korean Chemical Society
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• v.43 no.4
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• pp.430-437
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• 1999

The determination of total chlorine residuals in drinking water by flow injection analysis(FIA) with iodometric UV detection was investigated. The pH of the acid stream, the concentration of the iodide ion,the length of the mixing and reaction coils, the injection sample size, and flowrate were optimized as parameters for determining total chlorine residuals by FIA method. lodide was selectively oxidized to iodine by hypochlorite at pH 8.3 Ethylenediamine as masking agent for masking interference ions from the sample was given the best efficency. Calibration curve presented linear range of 0.03-3 mg/L for hypochlorite ion with a correlation coefficient of 0.999 or better. The detection limit was found to be 0.007 mg/L for hypochlorite ion. Under these analytical conditions, total chlorine residuals in several tap water sampled in the city of Jeonju were analyzed.

• Analytical Science and Technology
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• v.13 no.1
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• pp.22-26
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• 2000

2-Hydroxybenzaldehyde-5-Nitro-pyridylhydrazone (2HB-5NPH) was synthesized and its application in the spectrophotometric determination of vanadium ion(IV) was studied in the presence of surfactant. The optimum conditions of pH, solvent effect, concentration of ligand and surfactant were evaluated. The procedure was applied to determination of vanadium (IV) in mixture sample and real sample with satisfactory results (recovery ${\geq}$ 97% ; relative standard deviation ${\leq}$ 3.0% in the concentration range of $0{\sim}1.5{\mu}g/mL$ ; detection limit, $0.02{\mu}g/mL$ in solution).

• Journal of the Korea Institute of Information Security & Cryptology
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• v.19 no.6
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• pp.175-184
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• 2009

There have been two methods of estimating computer related security risk such as qualitative and quantitative methods which have distinctive advantages or disadvantages. The former is too narrative and somehow abstract to implement and the latter produces concrete result but needs lots of data, so that it is needed to develop a method overcoming such difficulties. It is advised to mix such two methods in a proper way depending on the conditions of a computer system. In this article, a concept of fuzzy number is employed on the way of mixing the two methods and provide a simple example using fuzzy numbers. Simulation was conducted for an assumed model system and it is demonstrated how to calculated expected and unexpected risk.

• Journal of Environmental Impact Assessment
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• v.27 no.5
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• pp.475-488
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• 2018

Surveying urban tributary vegetation is based mainly on field sampling at present. The tributary vegetation survey integrating UAV NIR(Unmanned Aerial Vehicle Near Infrared Radiance) imagery and in-situ point photo has received only limited attentions from the field ecologist. The reason for this could be the largely undemonstrated applicability of UAV NIR imagery by the field ecologist as a monitoring tool for urban tributary vegetation. The principal advantage of UAV NIR imagery as a remote sensor is to provide, in a cost-effective manner, information required for a very narrow swath target such as urban tributary (10m width or so), utilizing very low altitude flight, real-time geo-referencing and stereo imaging. An exhaustive and realistic comparison of the two techniques was conducted, based on operational customer requirement of urban tributary vegetation survey: synoptic information, ground detail and quantitative data collection. UAV NIR imagery made it possible to identify area-wide patterns of the major plant communities subject to many different influences (e.g. artificial land use pattern), which cannot be acquired by traditional field sampling. Although field survey has already gained worldwide recognition by plant ecologists as a typical method of urban tributary vegetation monitoring, this approach did not provide a level of information that is either scientifically reliable or economically feasible in terms of urban tributary vegetation (e.g. remedial field works). It is anticipated that this research output could be used as a valuable reference for area-wide information obtained by UAV NIR imagery in urban tributary vegetation survey.