Journal of the Korean Applied Science and Technology (한국응용과학기술학회지)

The Korean Society of Applied Science and Technology (한국응용과학기술학회)
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Sturdy of analysis of Xanthan gum as watersoluble-polymer in cosmetics

화장품 중 수용성 고분자인 Xanthan gum 분석연구

  • Lee, Yong-Hwa (Hoseo University, Fusion technology) ;
  • Yang, Jae-Chan (Mokwon University, College of Sciences & Technology, Division of Biomedicinal & Cosmetics)
  • 이용화 (호서대학교 융합기술연구소) ;
  • 양재찬 (목원대학교 테크노과학대학 생의약화장품학부)
  • Received : 2013.12.09
  • Accepted : 2013.12.27
  • Published : 2013.12.30
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Abstract

Determination of xanthan gum as watersoluble-polymer in commercial cosmetic samples was carried out by High Perfomance Liquid Chromatography(HPLC). An $C_{18}$ reversed-phase column and the selected ELSD detector was applied. The 25mM ammonium acetate/acetonitrile was used for the mobile phase of gradient conditions. The analysis results of HPLC showed good linearity with correlation coefficient of $r^2=0.9993$ in the rage of $50.3{\sim}604.1{\mu}g/ml$ and detection limit of $12.0{\mu}g/ml$.

역상 HPLC 에 의한 화장품에 사용하는 수용성 고분자인 Xanthan gum의 간편하고 정확한 정량분석 방법을 개발하였다. 분석조건은 $C_{18}$분리관과 ELSD 검출기를 사용하였으며, 25mM ammonium acetate/acetonitrile의 기울기 용리에 의해 분리 되었다. 이때 검량선의 상관계수(correlation coefficient) $r^2=0.9993$, 정량범위 $50.3{\sim}604.1{\mu}g/ml$, 검출한계 $12.0{\mu}g/ml$ 및 정확성이 우수하였다. 이 방법은 화장품 중 Xanthan gum를 정확하고 간편하게 정량분석 가능함을 보여 주었다.

Keywords

References

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