• Title/Summary/Keyword: 접합제

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Analysis of the Edge Sealing Strength for Vacuum Glass Panel Using Design of Experiment (실험계획법을 이용한 진공유리 패널 모서리 용융 접합 강도실험 분석)

  • Kim, Seung-Jong;Jeon, Euy-Sik
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.15 no.4
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    • pp.1819-1824
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    • 2014
  • The vacuum-glazing panel is a panel that keeps two glasses completely sealed in a vacuum condition. It is the high function insulation material of having the wall level minimizing the heat loss by the conduction and convection heat transmission coefficient. The edge sealing is a very important process of vacuum glass on the strength, thickness and air tightness. In this study, by using the hydrogen mixture gas torch, two sheets of glass was sealing in the furnace. The thickness and strength of the glass according to the process parameters is measurement and analysis, and predicting the edge sealing strength of glass by using taguchi method of experiment. We verified the validity of the experiment by checking the error rate through additional experiment.

Homogeneous Enzyme-linked Binding Assay for Mistletoe Lectin I Based on the Mistletoe Lectin I/D-galactose Interaction (Mistletoe lectin I/D-galactose의 인식결합에 기초한 Mistletoe lecti I에 대한 용액상 효소결합분석법에 관한 연구)

  • Rhee Paeng, Insook;Lee, Eun Ah;Chon, Chong Soon
    • Analytical Science and Technology
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    • v.13 no.5
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    • pp.624-629
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    • 2000
  • A simple and rapid homogeneous enzyme-linked binding assay for mistletoe lectin I(ML I) was developed using a coupled enzyme system of malate dehydrogenase (MDH) and D-galactose. A highly substituted MDH-galactose conjugate was prepared by employing an isothiocyanate method for formation of thiourea bond. In the presence of ML I, ML I inhibits the activity of the conjugate based on the ML I/D-galactose specific interaction. Thus, the concentration of ML I can be related to the homogeneous inhibition of the MDH-galactose conjugate. Using this method. ML I can be measured at the level of microgram per milliliter within 10 minutes.

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Fabrication of silicon Voltage Variable Capacitance Diode-II (VVC 다이오드의 시작연구(II))

  • 정만영;박계영
    • Journal of the Korean Institute of Telematics and Electronics
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    • v.7 no.2
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    • pp.33-42
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    • 1970
  • This report is concerned with the fahrication with the falricationof silicon VVC diode by the double diffusion planer technique. At first, some design charts for VVC diode were derived by considering the voltage-capacitance relations, the critical field intensity at the metallurgical junction, and the cut-off frequency of the diode. These charts enables the fabrication engineers to design VVC diode easily without going into the sophisticated design theory. We started with a 2.5 ohm-cm n-type epitaxial silicon wafer. The phosphorous was diffused by POCl3 impurity source. Then boron diffusion followed make hyperabrupt p-n junction by BN source. The maximum to minimum capacitance ratio of the diode as a tuning diode for a TV tuner made in these experiments was 4:1. Measured electrical characteristics of the sample diodes showed in good agreement with the theoretical expectations. Slicing and polishing technique of the silicon wafer and diffusion technique of the impurity atoms, which were employed in our study, are also stated briefly in this report.

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Antimicrobial Drug Resistance and R-plasmid of Salmonella species (Salmonella 균속의 항균제 내성 및 R-plasmid)

  • Lee Myung-Won;Chung Tae-Wha;Lee Yun-Tai;Kang Jeung-bok
    • Journal of environmental and Sanitary engineering
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    • v.3 no.2 s.5
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    • pp.23-41
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    • 1988
  • Two hundred and eighty-six strains of Salmonella species were isolated from the twelve provincial institutes of health and 19 general hospitals of urban and rural areas in Korea from January to December in 1986. The antimicrobial susceptibility test of these cultures was done by the method of agar diluton. The resistance frequency of Salmonella cultures was $29.7\%$. Among these resistant cultures, the most provalent resistance pattern of Salmonella was ampicillin, carbenicillin, chloramphenicol, tetracycline, streptomycin, and its resistance frequency was $15\%$. In plasmid profile of resistance strains, average number of plasmid harboring in Salmonella was 1-4 and molecular weight of plasmid ranged 1.6 to 70 megadalton (Md.). Plasmid pattern of strains isolated from Seoul and Kang-won showed the same or similar profiles. Plasmid pattern was identical in the same resistance pattern.

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고속도강에 Ti/W 복합중간층을 이용한 나노결정질 다이아몬드 코팅

  • Na, Bong-Gwon;Myeong, Jae-U;Gang, Chan-Hyeong
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.08a
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    • pp.127-127
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    • 2012
  • 나노결정질 다이아몬드(Nanocrystalline Diamond: NCD) 박막은 고경도와 낮은 마찰계수를 가지고 있어 고속도강과 같은 절삭공구 위에 코팅하여 공구의 성능 향상을 도모하고자 하는 노력이 있어 왔다. 그러나 NCD 박막의 잔류응력이 크고, 철계금속에는 NCD가 증착되지 않는다는 문제점이 있다. 잔류응력 완화와 다이아몬드 핵생성을 위하여 제3의 중간층 재료가 필요하다. 본 연구에서는 Ti과 W을 중간층으로 하여 고속도강(SKH51)에 NCD 박막을 코팅하고 기계적 특성을 비교하였다. 고속도강 위에 DC 마그네트론 스퍼터를 이용하여 2 ${\mu}m$ 두께의 Ti 또는 W 중간층을 증착하고, 그 위에 Microwave Plasma Chemical Vapor Deposition (MPCVD) 방법으로 NCD 박막을 2 ${\mu}m$ 두께로 코팅 한 것과 Ti, W순으로 각각 1 ${\mu}m$ 두께로 증착 후 그 위에 NCD 박막을 2 ${\mu}m$ 두께로 코팅 한 시편을 비교하였다. 세 가지 종류의 시편에 대하여 FESEM을 이용하여 표면과 단면의 형상을 관찰하였고, XRD와 Raman spectroscopy를 통해 NCD 박막의 결정성을 확인하였다. 그리고 Tribometer를 이용해 코팅된 박막의 내마모성을 비교하였으며 Rockwell C Indentation test를 이용하여 접합력을 비교하였다. 연구 결과 Ti/W 복합중간층 위에 코팅된 NCD의 접합력이 가장 우수하였으며 그 다음 W, Ti 순으로 나타났다. NCD와 고속도강의 큰 열팽창계수 차이가 복합중간층으로 인해 줄어들고 잔류응력이 완화되어 접합력이 향상되는 것으로 여겨진다.

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A Study of Hygroscopic Moisture Diffusion Analysis in Multimaterial System (이종 소재 접합체의 흡습 질량 확산 해석)

  • Kim, Yong-Yun
    • Journal of the Microelectronics and Packaging Society
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    • v.18 no.2
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    • pp.11-15
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    • 2011
  • Heat transfer equation is first reviewed and then governing equation of moisture diffusion. Analogy scheme is applied to analysis the moisture absorption problem of polymers. It make possible to numerically analyze the diffusion problem for single medium by using commercial finite element code if it is under the isothermal loading condition. It is extended to special multimaterial system by introducing pressure ratio function, whose moisture characteristics of materials are proportional to temperature only. The weight changes of silicon-nonconductive-polymer joint model due to moisture absorption is measured and been very close to the numerical results as for single media with boundary condition with zero concentration, but yields numerical errors as for multisystem media.

Strength Experimets on Head and Cooling Channel Specimens of a Preburner (예연소기 헤드 및 냉각채널 시편 강도 시험)

  • Yoo, Jae-Han;Moon, In-Sang;Lee, Soo-Yong
    • Journal of the Korean Society of Propulsion Engineers
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    • v.15 no.2
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    • pp.50-55
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    • 2011
  • A preburner for the high performance, staged combustion cycle liquid rocket engine is being developed. For the structural design processes, strength experiments and finite element analyses on specimens simulating the brazing joints of the preburner, were performed and compared. Total two kinds of the specimen were manufactured for the tests. One simulated the joints between the oxygen injectors and the head junctioned by the conventional vacuum brazing. The another was made to test the brazing surfaces by vacuum compression between the combustion chamber cooling channel and the outer wall. During the burst experiments, it was observed that the fractures were occurred not at the brazed joining but in the middle of the face plate and the cooling wall. In addition, the analysis showed that the predicted fracture locations and the strains were well matched with the experiment results.

A stable solid state quantum dot sensitized solar cell with p-type CuSCN semiconductor and its dopping effect

  • Kim, Hui-Jin;Seol, Min-Su;Yong, Gi-Jung
    • Proceedings of the Korean Vacuum Society Conference
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    • 2011.02a
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    • pp.378-378
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    • 2011
  • 본 연구에서는 ZnO 나노선 기판을 제작하여 그 위에 밴드갭이 낮은 물질인 CdS, CdSe를 증착시킨 후 p-type 반도체 물질인 CuSCN을 증착시켜 안정성이 향상된 양자점 감응형 태양전지를 제작하였다. ZnO 나노선 기판은 투명한 FTO 기판 위에 ZnO를 진공증착시켜 seed layer를 제작하고 그 위에 $10{\mu}m$정도의 길이의 나노와이어를 성장시킨 후, 밴드갭이 낮은 CdS, CdSe 물질과의 다중접합을 이용하여 제작하고, 이러한 나노선 구조위에 chemical solution deposition을 이용하여 ${\beta}$-CuSCN을 형성시켰다. 양자점 감응형 태양전지는 ZnO 나노선을 photoanode로 이용하고 ZnO 나노선은 암모니아수와 아연염을 이용한, 비교적 저온의 수열합성법을 통해 합성하였고, sensitizer로 쓰인 CdS, CdSe 물질은 CBD방식을 통하여 합성된 나노선 위에 in-situ로 접합시켰다. 또한, 기존의 액체전해질을 이용한 양자점 감응형 태양전지의 안정성을 향상시키기 위해 p-type의 반도체 물질인 CuSCN물질을 propyl sulfide를 이용, ${\sim}80^{\circ}C$의 열을 가하여 in-situ 방식으로 다공성 구조에 효율적으로 접합이 가능하도록 deposition하였다. 일반적으로, CuSCN film은 홀 전도체로서의 장점을 지닌 반면, 전도성이 낮은 단점이 있기 때문에 이를 향상시키기 위해서 첨가제를 이용, 농도에 따라서 전도도가 향상되고 셀의 성능이 향상되는 것을 확인하였다. 이와 같이 합성된 구조는 주사전자현미경(SEM), X-선 회절(XRD), 솔라시뮬레이터 등의 분석장비를 이용하여 태양전지로서의 특성을 분석하였다. 또한 안정성 평가를 위하여 시간에 따른 셀의 특성변화도 비교하였다.

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The Effect of Temperature Variations and Bonding Agents on Piezoelectric Sensor Diagnostics (온도 변화에 따른 압전체 센서 자가진단법 및 접합제의 영향에 대한 실험적 고찰)

  • Jo, HyeJin;Park, Tong-il;Park, Gyuhae
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2013.10a
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    • pp.799-804
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    • 2013
  • The sensor/actuator active sensor diagnostics procedure, where the sensors/actuators are confirmed to be functioning properly during operation, is a critical component to successfully complete the structural health monitoring (SHM) process with large numbers of active sensors typically installed in a structure. The basis of this process is to track the changes in the capacitive value of piezoelectric materials, which shows up in measured admittance. Due to the temperature dependent nature of piezoelectric materials, we investigated the effects of temperature variations on sensor diagnostic process. The effect of temperature variations found to be remarkable, modifying the measured capacitive values significantly. In addition we analyzed the effect of bonding agents between a PZT patch and a host structure. This paper summarizes considerations needed to develop such sensor diagnostic processes, experimental procedures and results, and additional issues that can be used as guidelines for future investigations.

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Numerical Analysis of Piezoelectric Element for Ultrasonic Joinning (초음파 접합용 진동자 냉각에 관한 수치해석)

  • Park, Sang-Jun;Lee, Young-Lim
    • Proceedings of the KAIS Fall Conference
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    • 2011.12b
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    • pp.398-401
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    • 2011
  • 초음파의 응용분야에는 음파 성질을 이용한 정보 측정분야와 에너지를 이용한 용접 및 가공 등을 들수 있다. 초음파 용접의 경우 저항용접이나 용융 용접을 적용할 수 없는 재료의 접합에 이용되는데 이는 모재를 음극간에 놓고 압입하면서 초음파를 발신하여 그 진동을 이용하는 용접방법이다. 압전소자의 경우 피에조 물질을 사용하는데 일반적으로 $150^{\circ}C$이상에서 분자구조의 변형을 일으켜 제 역할을 못하게 된다. 본 연구에서는 압전소자와 공구혼의 온도를 최적으로 유지하기 위하여 추가적인 공기 유로와 방열핀을 설계하여 이것이 방열성능에 미치는 영향에 대해 고찰하였다.

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