• 제목/요약/키워드: 접합강도

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Solvent-assisted sealing of poly(methylmethacrylate) microchannel under mild conditions (용매를 이용한 Poly(methylmethacrylate)의 저온 저압 본딩 및 마이크로 채널 표면의 선택적 소수성 코팅기법 개발)

  • Lee, Jae-Seon;Lee, Nae-Yun
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2017.05a
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    • pp.110-110
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    • 2017
  • 마이크로 플루이딕 디바이스는 화학, 생물학 실험 및 생체 의학 진단을 위한 플랫폼으로 지난 20년간 그 사용 및 연구가 증가되어 왔다. 마이크로 플루이딕 디바이스를 제작하는 데 있어 가장 일반적으로 사용되는 재료는 실리콘이지만 비용이 많이 들고 불투명하므로 광학 검출이 필요한 곳에 적용이 제한된다. 이러한 측면에서 열가소성 플라스틱은 상업화의 중요한 요소인 대량 생산에 있어 큰 잠재력을 가지고 있으며 저렴하고, 가공이 쉽고, 유연하고, 광학적으로 투명하고, 화학적으로 불활성이며, 생체적합성을 가진다. 본 연구에서는 열가소성 플라스틱의 일종인 PMMA Poly(methylmethacrylate)를 효율적으로 접합하기 위해 비교적 낮은 온도와 낮은 압력에서 에탄올을 활용한 접착방식을 개발하였다. 먼저, PMMA 기판의 전체 표면을 $80^{\circ}C$에서 20 분 동안 에탄올로 처리한 후, $60^{\circ}C$에서 20 분간 열 압착하는 방식으로 영구적인 결합이 이루어졌다. 결합 강도 및 채널의 sealing 정도를 확인하기 위해, 인장 강도, 누수 및 파열 테스트를 수행하였다. 결합강도는 약 12.4 MPa로 타 연구와 비교할 때 매우 높았으며 마이크로 채널의 전체 내부 체적보다 거의 450 배 높은 강한 액체 흐름을 견딜 정도로 견고한 결합이 유지되었다. 열가소성 플라스틱의 본딩에 사용되는 유기 용매는 광학 특성을 희생시키지 않으면서 결합 속도를 높일 수 있지만, 결합 공정 중에 용매로 인해 마이크로 채널이 막히는 현상이 발생될 수 있다. 따라서, 견고한 본딩을 유지하면서 채널 막힘을 방지하기 위해 마이크로 채널을 소수성으로 선택적으로 처리하여 내벽의 표면 특성을 튜닝해 주는 기법을 추가로 적용하였다. 본 연구에서 사용한 방법은 아민-PDMS (polydimethylsiloxane) 링커를 적용하여 기판 표면의 극성을 변경시켜 주었다. 아민-PDMS 링커는 PC (polycarbonate), PET (polyethylene terephthalate), PVC (polyvinyl chloride) 및 PI (polyimide)와 같은 다양한 열가소성 플라스틱의 표면 소수성을 현저히 증가시키며 화학적, 열적 안정성이 뛰어나다. 아민-PDMS 링커는 PMMA의 카보닐 그룹과 반응할 수 있는 아민 사이드 그룹을 포함하는 PDMS 백본으로 구성되며 처리된 대상표면을 소수성으로 만든다. 아민-PDMS 링커 처리 이후 채널은 소수성으로 변화되었으며 이는 접촉각(contact angle)의 증가로 확인되었다. 코팅된 채널을 에탄올로 30분간 80도에서 처리하여도 소수성은 그대로 유지되어 마이크로 채널의 선택적인 소수성 코팅이 성공적으로 수행되었다.

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Investigation of Adhesion property between Glass Fiber Reinforced Plastic and Polyurethane adhesives on Peel strength under Gyogenic tempernture (극저온에서 유리섬유강화플라스틱 표면의 유리섬유와 폴리우레탄 접착제간의 접착특성이 전체 박리강도에 미치는 영향에 대한 연구)

  • Shon, Min-Young;Lee, Jae-Kwang;Hong, Jeong-Lak
    • Composites Research
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    • v.22 no.4
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    • pp.13-19
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    • 2009
  • Adhesive joints are widely used for structural joining applications in various fields and environmental conditions. Polyurethane adhesive is using for LNG carrier with cryogenic temperature condition. Even if similar polyurethane adhesive is used for different substrate, it shows different adhesion properties. Specially, variation of adhesion properties depending on the resin system or fiber is very important factor for selection of adhesive on industrial application. In present study, we got different peel strength according to the different test temperature when different polyurethane adhesive was used for same fiber reinforced composite. The main cause was investigated using by SEM and it was proven that the different adhesion property between glass fiber on composite surface and polyurethane adhesives at cryogenic temperature.

Punching Shear Strength of the Void Transfer Plate (중공 전이 슬래브의 뚫림 전단 강도)

  • Han, Sang-Whan;Park, Jin-Ah;Kim, Jun-Sam;Im, Ju-Hyeuk;Park, Young-Mi
    • Journal of the Korea Concrete Institute
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    • v.22 no.3
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    • pp.367-374
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    • 2010
  • The transfer slab system is a structural system that transfers the loads from the upper shear wall structure to the lower columns. This is a costly system due to a very thick slab, and the relatively high cost can be mitigated by introducing voids in the slab. However, this system of flat plate containing voids is vulnerable to brittle failure caused by punching shear in vicinity of slab-column connection. Thus, the punching shear capacity of the void system is very important. However, the current code doesn't provide a clear design provision for the strength of slabs with a void section. In this study, experimental study was conducted to investigate the punching shear strength of the void slab system. The shear strength of the specimens was predicted by current code and previous researches. In result, the punching shear strength of the void system is determined as the least value calculated at critical section located a distance d/2 from the face of the column and the center of the void section using the effective area at critical section.

Effect of Adhesive Shear Strength of CFRP/Ni-Cr Alloy Under Severe Environmental Condition (가혹 환경이 복합재/Ni-Cr 합금 접착전단강도에 미치는 영향 연구)

  • Cho, Hyeon-Tae;Park, Seong-Min;Kim, Min-Jun;Hoang, Van-Tho;Kim, Hak-Inn;Son, Myung-Sook;Ahn, Jong-Kee;An, Ji-Min;Choi, Jin-Ho;Nam, Young-Woo;Kweon, Jin-Hwe
    • Composites Research
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    • v.33 no.5
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    • pp.275-281
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    • 2020
  • The mechanical property related to lap shear strength of the joint structure between carbon fiber reinforced polymer (CFRP) composite and metal (Ni-Cr Alloy) under varying environmental conditions (temperature and humidity) was studied in order to apply to the aircraft fan blade. Room temperature dry (RTD), elevated temperature wet (ETW), and cold temperature dry (CTD) environmental conditions were chosen for investigation based on the flight conditions of aircraft. Lap shear strength tests were conducted according to ASTM Standard D3528 to evaluate the shear strength. The microstructure characteristic of failure zone was analyzed by SEM images to check the adhesive shear strength with the three environmental conditions. In comparison with shear strength for the RTD condition, the shear strength in the ETW condition was reduced by 72.8% while those for the CTD condition increased by 56.5%. The moisture absorption and high temperature in ETW condition strongly had an affect on mechanical property of adhesive, while cold temperature could enhance the adhesive shear strength due to the higher brittleness.

Initial Imperfection and Axial Strength of Struts with Octagonal Hollow Section fabricated from HR Plate (열연강판 팔각강관 버팀보의 초기편심과 축방향 압축강도)

  • Jo, Jae Byung
    • Journal of Korean Society of Steel Construction
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    • v.27 no.1
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    • pp.23-30
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    • 2015
  • Developed in this study were Octagonal-hollow-section(OHS) struts, whose compressive strengths against flexural and local buckling is higher than H-shape or rectangular-hollow-section(RHS) struts with the same unit weight. OHS members are also advantageous in handling and storing compared to circular hollow sections(CHS). OHS members were fabricated from HR Plates by cold forming and fillet welding. 5 numbers of 20m long OHS struts were assembled, each of which consist of two 9.6m long OHS member and two end connection elements made of cast iron. The compressive strength of the OHS strut was evaluated by comparing the test results, design codes and FEM analysis each other. Test results show that all of the struts have almost same or larger compressive strength than Korean Road Bridge Design Code(KRBDC) (2012). The initial imperfections can be estimated by using measured strains and are turned out to be less than L/450 for all the struts tested. The results of FEM analysis show that the variation of initial imperfection has less effects on the compressive strength for struts with vertical surcharge than for those with self-weight only, while the strength decreases as the initial imperfection increases. As the result of this study, the allowable initial imperfection for 20m long OHS struts is recommended to be less than L/350 on job sites.

The examination of application possibility and development of new welding joint shape for aluminum alloy (Al어선 선체용접부의 신형상 개발 및 적용 가능성 검토)

  • Jong-Myung Kim;Chong-In Oh;Han-Sur Bang
    • Journal of the Society of Naval Architects of Korea
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    • v.38 no.1
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    • pp.99-107
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    • 2001
  • Manufacture of fishing vessel is needed the effective material for light, strength, fire and corrosion of water in order to improve durability by high-speed and fishing. These fishing vessel can be divided into FRP and AI alloys fishing vessel. FRP fishing vessel is light and effective for strength but highly ignited and susceptible to heat during the manufacturing ship by-produce noxious component for human. In the case of a scrapped ship, it cause environmental pollution. On the other hand, aluminum is a material in return for FRP and has merit of high-strength and lightness. It's more heat proof and durable than FRP and superior to prevent from corrosion. Al alloys fishing vessel development is rising as an urgent matter. But, al alloy has some defect of bad weldability, welding transformation, cracks and overcost of construction. Therefore this study is to develop the new welding joint shape solving aluminum defects and mechanical behavior. First of all, strength was compared and reviewed by analysis of plate, stiffen plate, new model simplified by using plate theory. On the base of this result, plate and new model of temperature distribution, weld residual stress and strength of tensile, compressive force were compared and reviewed by finite element computer program has been developed to deal with heat conduction and thermal elasto plastic problem. Also, new model is proved application possibility and excellent mechanic by strength comparison is established to tensile testing result.

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Flexural Strength Evaluation of Steel Plate-Concrete Composite Beam using Bolted (절곡 강판을 볼트로 체결한 강판-콘크리트 합성보의 휨강도 평가)

  • Han, Myoung-Hwan;Choi, Byong-Jeong
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.19 no.6
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    • pp.126-136
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    • 2018
  • A steel-plate concrete composite beam is composed of a steel plate, concrete and shear connector to combine inhomogeneous two materials. The steel plate is assembled by welding an existing composite beam. In this study, new steel-plate concrete composite beam, called a SPC Beam, was developed to reduce the shear connector and improve the workability. The SPC Beam was composed of folding steel plates and concrete, without a shear connector. The folding steel plate was assembled using high strength bolt instead of welding. To improve the workability in field construction, a hat-shaped Cap was attached to the junction with a slab. Monotonic load testing under two points was conducted under displacement control mode. The flexural strength of the specimen for positive moment and negative moment was calculated using the plastic stress distribution method. The test results showed that the flexural strength of the new SPC Beam had 80% of the strength of a complete composite beam. In addition, increasing the composite ratio was possible through clearance controls of the cap. In this study, the performance of the SPC Beam was verified through additional experiments and analyses with the cross-sectional shape and cap as variables, because the representative shape in the positive negative moment region is targeted.

Overstrength and Response Modification Factor in Low Seismicity Regions (약진지역에서의 초과강도 및 반응수정계수)

  • Lee, Dong-Guen;Cho, So-Hoon;Ko, Hyun;Kim, Tae-Jin
    • Journal of the Earthquake Engineering Society of Korea
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    • v.10 no.3 s.49
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    • pp.57-64
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    • 2006
  • Seismic design codes are mainly based on the research results for the inelastic response of structures in high seismicity regions. Since wind loads and gravity loads may govern the design in low seismicity regions in many cases, structures subjected to design seismic loads will have larger overstrength compared to those of high seismicity regions. Therefore, it is necessary to verify if the response modification factor based on high seismicity would be adequate for the design of structures in low seismicity regions. In this study, the adequacy of the response modification factor was verified based on the ductility and overstrength of building structures estimated from the result of nonlinear static analysis. Framed structures are designed for the seismic zones 1, 2A, 4 in UBC-97 representing the low, moderated and high seismicity regions and the overstrength factors and ductility demands of the example structures are investigated. When the same response modification factor was used in the design, inelastic response of structures in low seismicity regions turned out to be much smaller than that in high seismicity regions because of the larger overstrength of structures in low seismicity regions. Demands of plastic rotation in connections and ductility in members were much lower in the low seismicity regions compared to those of the high seismicity regions when the structures are designed with the same response modification factor.

Influence of Column Aspect Ratio on the Hysteretic Behavior of Slab-Column Connection (슬래브-기둥 접합부의 이력거동에 대한 기둥 형상비의 영향)

  • Choi, Myung-Shin;Cho, In-Jung;Ahn, Jong-Mun;Shin, Sung-Woo
    • Journal of the Korea Concrete Institute
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    • v.19 no.4
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    • pp.515-525
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    • 2007
  • In this investigation, results of laboratory tests on four reinforced concrete flat plate interior connections with elongated rectangular column support which has been used widely in tall residential buildings are presented. The purpose of this study is to evaluate an effect of column aspect ratio (${\beta}_c={c_1}/{c_2}$=side length ratio of column section in the direction of lateral loading $(c_1)$ to the direction of perpendicular to $c_1$) on the hysteretic behavior under earthquake type loading. The aspect ratio of column section was taken as $0.5{\sim}3\;(c_1/c_2=1/2,\;1/1,\;2/1,\;3/1)$ and the column perimeter was held constant at 1200mm in order to achieve nominal vertical shear strength $(V_c)$ uniformly. Other design parameters such as flexural reinforcement ratio $(\rho)$ of the slab and concrete strength$(f_{ck})$ was kept constant as ${\rho}=1.0%$ and $f_{ck}=40MPa$, respectively. Gravity shear load $(V_g)$ was applied by 30 percent of nominal vertical shear strength $(0.3V_o)$ of the specimen. Experimental observations on punching failure pattern, peak lateral-load and story drift ratio at punching failure, stiffness degradation and energy dissipation in the hysteresis loop, and steel and concrete strain distributions near the column support were examined and discussed in accordance with different column aspect ratio. Eccentric shear stress model of ACI 318-05 was evaluated with experimental results. A fraction of transferring moment by shear and flexure in the design code was analyzed based on the test results.

Conservation Process of Large-earthen ware in Geumgangsa Temple Site - A Study on the Cyanoacrylate Adhesive Used for Large-earthen Ware Joining - (금강사지 출토 대형 토기의 보존 - 대형 토기접합에 사용된 순간 접착제에 대한 연구 -)

  • Lee, Dahae;Hwang, Hyunsung;Shin, Minkyeong
    • Conservation Science in Museum
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    • v.13
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    • pp.1-11
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    • 2012
  • While the project for registering the unregistered relics that had been stored in the relic storage warehouse was in progress, restoration operations were started for the large size pottery pieces that had been excavated from the Geumgangsa Temple Site and it is attempted to explain the pottery pieces and to introduce the process of the overall conservation treatment. About 600 pieces of large size pottery had been separately stored in more than 40 relic boxes in their original damaged condition without making it possible to figure out their shape, size, usage and quantity at all. Due to the enormous number and weight of the pottery pieces, they were, first of all, pre-classified largely into 6 groups of pottery pieces in consideration of the visible features such as pottery thickness, color sense and glaze brilliance, etc. for each kind of pottery raw material. However, as a result of making them adhere together on a temporary basis, they turned out to be only one piece of pottery in reality. In this restoring process, in order to see if the generally used cyanoacrylate adhesive was in fact safe when a very large, heavy and deformed pottery piece was to be put together, its safeness was checked by examining the adhesion velocity, adhesion strength and dissolution velocity for both from low to high viscosities through preliminary experiments. In order to restore the lost parts after putting the existing pieces together, diversified epoxy resins were used to fit their shapes. Considering that the bottom of the restored relic was shaped to be not flat but round without allowing it to stand alone, an exhibition mount was manufactured so that the relic could be stored stably and used readily for exhibition.