• Elastomers and Composites
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• v.35 no.1
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• pp.19-28
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• 2000

The fundamental study of additional silicone impression material has been performed by comparing the other import products. In order to estimate the possibility of usage of the impression material developed in this study, the several techniques such as IR, EDX, DSC, TGA, rubber rheometer, and contact angle measurement were used. According to the results, there were not any product satisfying all properties required in the impression material. The impression material developed in this study showed best mechanical properties among the all impression materials. However. the wetting property should be studied more by an introduction of a hydrophilic surfactant or modification of a base polymer.

• Applied Chemistry for Engineering
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• v.21 no.1
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• pp.46-51
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• 2010

Polyorganosiloxane modified polyurethane (PDMS-PU) polymers were prepared from copolymerization of ${\alpha}$,${\omega}$-hydroxypropyl terminated polyorganosiloxane with isophorone diisocyanate (IPDI), polypropylene glycol (PPG), and 2,2-bis(hydroxymethyl) propionic acid (DMPA). Hydrophobic polyorganosiloxane was introduced in polyurethane main chain as soft segment block unit. The isocyanate groups in PDMS-PU block copolymer was blocked with 2-butanon oxime and obtained PDMS-PU dispersions in water by neutralizing with triethylamine (TEA). The deblocking temperature of PDMS-PU polymer was measured from thermal analysis. The good stability of the PDMS-PU dispersion was obtained by dispersing into water. PDMS-PU prepolymers were prepared with various contents of DMPA under [NCO]/[OH] = 1.12~1.53 equivalent ratio. Increasing DMPA from 7.2, 13.4, and 18.7 mole% in preparation of PDMS-PU polymer, particle sizes were decreased from 156, 100, 65 dnm. Also contact angle and adhesive strength were measured.

• Journal of Hydrogen and New Energy
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• v.19 no.2
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• pp.132-138
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• 2008

금속산화물의 열화학싸이클에 의한 수소생산 소재중 안정성이 우수하고 물분해 수소생산능이 비교적 우수한 $NiFe_2O_4$를 합성하여 열화학수소생산공정 적용시 최적화의 조건에 대하여 검토하였다. 합성한 $NiFe_2O_4$는 격자상수가 $8.34\;{\AA}$이었고, 뫼스바우어에 의해 구조는 Ni이 페라이트 구조인 $AB_2O$의 B위치에 주로 위치하는, A 및 B의 상대적 흡수강도가 57.9:42.1인 역스피넬구조를 보이고 있다. 이러한 구조의 $NiFe_2O_4$의 열적환원은 $610^{\circ}C$부터 시작하여 $1200^{\circ}C$에 이르는 동안 약 1.1 wt%의 무게감소가 관찰된다. 물에 의한 산화과정에서 수소가 발생하게 되는데, $1200^{\circ}C$이하의 환원온도에서 가능한 수소생산량은 약 $0.45\;cm^3/g{\codt}cycle$ 이었다. 산화 환원의 반복과정에서 $NiFe_2O_4$의 XRD에 의한 구조변화는 관찰되지 않아 매우 안정한 구조를 갖는다는 것을 보여주었다. 수소생산을 위한 무게당 싸이클당 수소생산양은 산화 환원과정의 온도범위가 가장 중요하였고 물의 접촉시간은 중요한 요소가 되지 않았다. 열적 환원과정에서 많은 양의 수소생산성능을 보이기 위해서는 $1200^{\circ}C$이상의 고온을 필요로 하는 것을 보여주었다.

• Korean Journal of Materials Research
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• v.3 no.6
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• pp.638-644
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• 1993

The degradation of dielectric breakdown field of 8nm-thick gate oxide ($SiO_2$) for Tipolycide MOS(meta1-oxide-semiconductor) capacitor with different annealing conditions and thickness of the polysilicon film on gate oxide was investigated. The degree of degradation in dielectric breakdown strength of the gate oxide for Ti-polycide gate became more severe with increasing annealing temperature and time, especially, for the case that thickness of the polysilicon film remained on the gate oxide after silicidation was reduced. The gate oxide degradation may be occurred by annealing although there is no direct contact of Ti-silicide with gate oxide. From SIMS analysis, it was confirmed that the degration of gate oxide during annealing was due to the diffusion of titanium atoms into the gate oxide film through polysilicon from the titanium silicide film.

• Journal of the Computational Structural Engineering Institute of Korea
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• v.26 no.2
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• pp.157-164
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• 2013

In this study, the structural performance of nuclear power plant containment buildings, which are made of steel fiber reinforced concrete(SFRC) and subject to aircraft crash, is examined by finite element analyses. The applied loads by aircraft crash against the buildings are modeled using Riera impact load function and by the varying aircraft contact area with respect to time. CSCM concrete model in LS-DYNA is employed to model SFRC. The parameters for the material model are determined from SFRC strength prediction models. Based on the volume ratio of steel fiber in SFRC, the structural performance of nuclear containment buildings subject to aircraft crash are analysed using a commercial finite element analysis program LS-DYNA. The safety assessments of the buildings subject to the crash are discussed and the effectiveness of SFRC for nuclear power plant containment building on the increase of aircraft crash resistance is also evaluated.

• Journal of Adhesion and Interface
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• v.10 no.3
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• pp.148-153
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• 2009

An atmospheric plasma pre-treatment method was applied to PU foam, Leather (Action), Rubber to improve its adhesion using solvent and water soluble type pressure sensitive adhesion in atmospheric plate type reactor. In order to investigate the optimum reaction condition of plasma treatment, type of reaction gas (nitrogen), rate of gas flow (30~100 mL/min), and reaction time (0~30 s) were examined in a plate plasma reactor. The result of the surface modification with respect to the treatment procedure was characterized by using SEM. Due to a de-crease of the contact angle of various materials, the greatest adhesion strength was achieved at optimum condition such as flow rate of 100 mL/min, reaction time of 10 second for an atmospheric plasma treatment of the PU foam, EVA foam, Leather (Action) and Rubber also resulted in the improvement of the adhesion.

• 한국신재생에너지학회:학술대회논문집
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• 2010.06a
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• pp.185.1-185.1
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• 2010

원격탐사(remote sensing)란 관측 대상과의 접촉 없이 멀리서 정보를 얻어내는 기술을 말한다. 기상관측분야에는 이미 소다(SODAR) 장비가 폭넓게 사용되거 왔으나 최근 풍력자원평가(wind resource assessment)를 위한 풍황측정에 SODAR와 더불어 라이다(LIDAR)가 적극적으로 활용되기 시작하고 있다. 참고로 SODAR(SOnic Detection And Ranging)는 수직 및 동서 남북 방향으로 음파를 발생시키고 대기유동에 의해 산란 반사된 에코를 수신하여 진동수 변화와 반사에코 강도를 측정하여 각 방향의 에코자료를 벡터 합성함으로써 풍향 및 풍속을 산출하는 원리이다. 반면 LIDAR(Light Detection And Ranging)는 비교적 최근에 풍황측정 용도로 개발된 레이저 탐지에 바탕을 둔 원거리 센서로, 공기입자(먼지, 수증기, 구름, 안개, 오염물질 등)에 의해 산란된 레이저 발산의 도플러 쉬프트(Doppler shift)를 이용하여 풍향 및 풍속을 측정하는 원격탐사 장비이다. 풍력자원평가 측면에서 라이다는 그 정확도가 IEC61400-12에 의거한 풍황탑(met-mast) 측정자료 다수와의 비교검증 실측평가(Albers et al., 2009)를 통하여 입증된 바 있다. 한편 한국에너지기술연구원에서 운용 중인 라이다 시스템은 그림 1의 우측 그림과 같이 1초에 $360^{\circ}$를 스캔하여 50지점에서 반사되는 레이저를 스펙트럼으로 측정하되 설정된 관측높이에서 풍속은 샘플링 부피(sampling volume)의 평균값으로 정의된다. 그런데 샘플링 부피는 설정된 관측높이로부터 상하 12.5m, 총 25m의 높이구간에서 관측한 스펙트럼의 평균값을 그 중앙지점에서의 풍속으로 환산하는 알고리듬(algorithm)을 채택하고 있다. 따라서 비선형적으로 변화하는 풍속연직분포 관측 시 풍속환산 알고리듬에 의한 측정오차가 개입될 가능성이 존재하는 것이다. 이에 본 연구에서는 라이다에 의한 풍속연직분포 측정 시 샘플링 부피의 구간 평균화 과정에서 발생하는 불확도(uncertainty)를 정량적으로 분석함으로써 라이다에 의한 풍속연직분포 관측의 불확도를 정량평가하고자 한다.

• Korean Journal of Medicinal Crop Science
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• v.14 no.3
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• pp.130-133
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• 2006

This study was conducted to select Codonopsis lanceolata seed's new pelleting particulate materials and adhesives. Different adhesives (Polyvinyl alcohol (PVA), Carboxymethyl cellulose (CMC), Polyvinyl pyrrolidone (PVP), Xanthan gum (XG), Arabic gum (AG)) and particulate materials (Illite, Diatomite, Pyrophyllite + Illite + Diatomite (PID), Pyrophyllite + Illite + Talc (PIT), Bentonite + Talc (BT)) were tested for seed pelleting. PID for Codonopsis lanceolata seed pelleting appeared to be the best particulate material. Among the pelleting adhesives, PVP was the best adhesive for seed pelleting, and the optimum concentration for germination of pelleting seed was 1 %. Germination rate of the pelleted seeds treated with PID particulate material and PVP adhesive was higher (86.8%) than those of raw seeds (85.5%). $T_{50}$ and MDG of pelleted Codonopsis lanceolata seed required five and eight days at soil moisture content of 50%, respectively.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.21 no.3
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• pp.511-518
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• 1997

The technique of fretting fatigue test was developed and fretting fatigue tests of A12024-T4 were conducted under several conditions. The newly developed calibration methods for measuring surface contact tractions showed good linearity and repeatability. The plate type specimen to which tow bridge type pads were attached and vision system was used to observe the crack behaviour. The oblieque cracks appeared in the early stage of crack growth and they became mode I cracks as they grow about 1 mm. The mode I transition points were found to be longer when surface tractions are higher or bulk stress is lower. Before the crack becomes mode I crack, 'well point' where crack grow about rate is minimum, was detected under every experimental condition. The crack behaviour was found to be affected by surface tractions, contact area, bulk stress. It was also found that partial slip and stick condition is most detrimental and the crack starts from the boundary of stick and slip. For gross slip crack started at the outside edge of pad. After crack mode transition, fretting fatigue cracks showed almost same behaviour of plain mode I fatigue cracks. Equivalent stress intensity factor was used to analyze the behaviour of fretting fatigue cracks and it was found that stress intensity factors can be applied to fretting fatigue cracks.

• Journal of the Korean Society for Nondestructive Testing
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• v.22 no.4
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• pp.393-401
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• 2002

Pipelines in power plants, nuclear facilities and chemical industries are often affected by corrosion effects. It is important to inspect the internal defects in pipelines in oder to guarantee safe operational condition. We have taken relatively much time, cost and manpower to use conventional NDT methods because these methods are contact measuring methods. In this paper, we used digital shearography, a laser-based optical method which allows full-field measurement of surface displacement derivatives. This method has many advantages in practical use, such as low sensitivity to environmental noise, simple optical configuration and real time measurement. The experiment was performed with pressure vessels which has different internal cracks and detected internal cracks in the pressure vessels at a real time using phase shifting method.