• International Journal of Highway Engineering
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• v.10 no.3
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• pp.239-246
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• 2008

In this study, the influence of reaction temperatures, mixing time and flexible modifier for crumb rubber modified asphalt(CRMA) as processing conditions were investigated. The temperature susceptibility and adhesion properties of neat and modified asphalts at low temperature measured using the penetration and tensile adhesion test. It was found that processing temperatures and flexible modifier were important factors for tensile adhesion strength and toughness energy at low temperature. The CRMA in the higher processing temperature and flexible modifier exhibited improved tensile adhesion properties which indicated the flexible structure of neat and modified asphalt binder. In general, the improvements of the physical properties in the CRMAs were due to the improvements of miscibility between CR and asphalt binder. It was found that the adhesion properties of the flexible agent modified CRMA were higher than CRMA were related to the flexible agent tend to penetrate into CR particles and asphalt binder.

• Korean Chemical Engineering Research
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• v.50 no.1
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• pp.6-10
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• 2012

The main objective of this work was studying the influence of paraffin oil(PO) on the adhesion properties at low temperature in styrene-butadiene-styrene(SBS) copolymer and crumb rubber(CR) modified asphalt. The temperature susceptibility of SBS/CR asphalt and PO/SBS/CR/asphalt blends were measured by penetration and softening point. Adhesion properties at low temperature and dispersion of modifiers in PO/SBS/CR/asphalt blends were evaluated by universal test machine and florescence microscopy, respectively. The adhesion properties of PO/SBS/CR/asphalt blends at low temperature increased in the proportion of SBS contents with both 5 and 10 wt % of paraffin oil. Results showed that the maximum tensile adhesion strength and toughness energy at $-20^{\circ}C$ were obtained when PO and SBS contents were 10 wt % and 6 wt %, respectively. The addition of PO is effective for enhancing the flexibility of SBS/CR/asphalt blends and leads to the increase of toughness at low temperature.

• Journal of Adhesion and Interface
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• v.3 no.3
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• pp.15-21
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• 2002

The modified polyethylene(m-PE) films were prepared from aqueous dispersions which were synthesized by reacting poly(ethylene-co-methylacrylate) with aqueous KOH and ammonia solution to attach -COOK, $CONH_2$, and COOH as pendent groups in the polyethylene backbones. Thermal, tensile and heat-seal properties were measured to investigate the effect of the pendent groups. Endothermic peaks on DSC curves were affected by the thermal history of the samples and a melting peak was observed at around $86^{\circ}C$ on the second heating curve while three melting peaks were shown on the first heating curve. A minimum value of tensile strength was shown at 70 mole% of COOK based on pendent groups. Tensile modulus increased with increasing the amide content in pendent groups. The m-PE films were heat-sealed at lower temperature than LDPE films and showed a minimum heat seal strength at around 70 mole% COOK content in pendent groups.

• KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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• v.8 no.1
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• pp.15-22
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• 2002

We received 2 types flexible packaging films from two companies that laminated PET $16{\mu}m/dry$ lamination/aluminium foil $7{\mu}m/dry$ lamination/CPP $80{\mu}m$ films. For the reason of hot sealing's trouble through filling process, We separated each layer and compared thicks, film types and tested IR, DSC and sensory test. At the result, one sample's thick is different but film types is same between samples. Optimum hot-sealing conditions between two samples is $195^{\circ}C\;and\;210^{\circ}C$. The difference is $15^{\circ}C$. According to test of direct filling packaging process by four face fluid filling machine, two sample's sealing strength of hot-sealing is $4.76kg/cm2/15mm$(sample of optimum hot-sealing condition is $195^{\circ}C$) and $3.84kg/cm2/15mm(210^{\circ}C)$.

• Restorative Dentistry and Endodontics
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• v.28 no.4
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• pp.314-325
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• 2003

이 연구의 목적은 수종 상아질 접착 시스템과 복합 레진 및 resin-modified glass ionomer를 상아질 표면에 접착하여 재료 및 상아질내 위치에 따른 미세전단결합강도를 측정, 비교하는 것이다. 상아질 접착 시스템으로는, 3-step인 Scotchbond Multi-Purpose Plus, 2-step인 Single Bond와 자가 부식형 시스템인 Clearfil SE Bond를, 1-step인 Prompt L-Pop을 사용하였다. 이와 함께 hybrid type의 복합 레진인 Clearfil AP-X와 2250을 사용하였으며 resin-modified glass ionomer로는 Fuji II LC를 사용하였다. 상악 소구치를 치아의 근원심 중앙부를 절단하여 상아질면을 노출시켰다. 5개 실험군으로 분류하고 상아질면을 위치에 따라 치관부의 occlusal $\frac{1}{3}$, middle $\frac{1}{3}$, cervical $\frac{1}{3}$과 치근부로 구분지어 시편을 부착하였다. 미세전단결합강도측정는 Universal testing machine(EZ-test; Shimadzu, Japan)에서 측정하였다. Occlusal 1/3부위에서는 SE가 가장 높은 값을, SM과 SB간에는 유의차가 없었으며, PL, GI순으로, Middle 1/3부위에서는 $SM{\;}{\geq}{\;}SE{\;}{\geq}{\;}SB{\;}{\geq}{\;}PL{\;}{\geq}{\;}GI$순으로, cervical 1/3부위에서는 SM, SE, SB간에 유의차가 없었다. Root dentin에서는 SM이 가장 높은 값을 보였으며 SE, PL, GI간에 유의차가 없었다. SE만이 치관부 상아질에 비해 치근부에서 유의할만한 결합강도의 감소를 나타냈다(p<0.05). GI는 치관부 상아질에서는 다른 군에 비해 유의성 있게 낮은 결합강도를 보였으나 치근부에서는 SE, PL과 유의차가 없었다.

• Journal of Adhesion and Interface
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• v.17 no.3
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• pp.104-109
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• 2016

Compare AC corona and DC corona treatment effects, polyester fabrics were AC corona treated with different current intensity (5, 10, 15 A) and feeding speed (5, 10, 15 m/min) as the same DC corona treatment conditions of the preceding research. We confirmed the surface change of polyester fabrics using scanning electron microscopy (SEM) and X-ray photoelectron spectrometer (XPS), and the change of physical properties through measuring the dry and wet bonding strength. The surface changes of polyester fabrics by treating in air atmosphere with AC corona discharge are shown similar tendency with DC corona discharge. Generally dry bonding strength were increased with increasing current intensity and feeding speed, but wet bonding strength were increased with increasing current intensity and decreasing feeding speed in both AC and DC corona treatment. When the current is 20 A, carbonization occurs in DC corona discharge but carbonization does not occur in DC corona discharge.

• Composites Research
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• v.28 no.6
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• pp.348-355
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• 2015

NDT (Non Destructive Test) of the adhesive joints is very important because their strengths have greatly affected by the worker's skill and environmental condition. Recently, the electric impedance method in which 1-2 wt% CNT was dispersed in the adhesive and the electric resistance of the adhesive joint was measured was suggested for the defect detection of the adhesive joint. The uniform dispersion of CNT in the electric impedance method is very important to make a constant electric resistance of the adhesive joint and the accuracy of defect detection depends on the uniform dispersion. In this paper, the adhesive joints in which CNT was dispersed in the adhesive by the four dispersion methods were made and their electric resistance were measured. The pre-process and evaporation process of CNT using the ultrasonic method and agitation method was used and the effective dispersion method was suggested. Also, the criteria to evaluate the dispersivity was proposed.

• Journal of Adhesion and Interface
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• v.9 no.1
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• pp.9-15
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• 2008

EVA foam was treated by oxygen plasma under a various treatment time for surface modification. The effect of plasma treatment on surface properties of EVA foam was investigated in terms of FT-IR ATR, XPS, contact angle, and SEM analysis and the adhesion characteristic of the EVA foam was studied in peel strength. As a results, EVA foam treated by plasma led to an elimination of organic compound, an increase of oxygen content, and an increase of surface roughness, resulting in improving the adhesion properties of the EVA foam. As the plasma treatment time increased, the hydrophilicity and physical change of surface of the EVA foam were increased and showed maximum value at 180 s and 420 s, respectively. The maximum adhesion strength appeared at plasma treatment time of 420 s and therefore, in this study the physical change was thought to be a major factor for improving the adhesion of the EVA foam.

• Journal of Adhesion and Interface
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• v.18 no.2
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• pp.53-58
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• 2017

In this study, to overcome a complicated shoe adhesion process such as buffing, pre-treatment by primer in the rubber component of the shoe, we studied adhesion and mechanical properties with rubber compound added $MgCl_2$. We determined adhesion properties of $MgCl_2$ content. Especially, the rubber containing $MgCl_2$ exhibited good adhesion properties to water-based adhesion. Since $MgCl_2$ is a water-soluble salt, it was judged that this phenomenon occurred. The results are confirmed by contact angle and surface morphology measurement. In addition, in the case of rubber compound added $MgCl_2$, the crosslinking efficiency was increased and the NBS resistance was increased.

• Journal of Adhesion and Interface
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• v.19 no.3
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• pp.118-122
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• 2018

In this study, polyurethane hot melt adhesive containing ester groups was synthesized. Three kinds of chain extenders were used to find out the best chain extender. Results showed that adhesive containing 1,4-butanediol as a chain extender exhibited the highest peel strength among them. Also, it was found that there existed the optimum molecular weight of 1,4-butanediol containing adhesive for make the highest peel strength.. Moreover, hot melt adhesive containing 1,4-butanediol chain extender was applied to various kinds of textiles substrate such as cotton, polyester, and urethane coated polyester textiles to study the effects of different substrates on the peel strength and water resistance at $60^{\circ}C$. It was found that cotton substrate showed the highest peel strength and urethane coated polyester substrate showed the highest resistance on $60^{\circ}C$ water.