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A study on the shear bond strength between Co-Cr denture base and relining materials (금속의치상과 의치이장재료 간의 결합력에 관한 연구)

  • Lee, Na-Young;Kim, Doo-Yong;Lee, Young-Soo;Park, Won-Hee
    • The Journal of Korean Academy of Prosthodontics
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    • v.49 no.1
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    • pp.8-15
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    • 2011
  • Purpose: This study evaluated the bonding strength of direct relining resin to Co-Cr denture base material according to surface treatment and immersion time. Materials and methods: In this study, Co-Cr alloy was used in hexagon shape. Each specimen was cut in flat surface, and sandblasted with $110\;{\mu}m$ $Al_2O_3$ for 1 minute. 54 specimens were divided into 3 groups; group A-control group, group B-applied with surface primer A, group C-applied with surface primer B. Self curing direct resin was used for this study. Each group was subdivided into another 3 groups according to the immersion time. After the wetting storage, shear bond strength of the specimens were measured with universal testing machine. The data were analyzed using two-way analysis of variance and Tukey post hoc method. Results: In experiment of sandblasting specimens, surface roughness of the alloy was the highest after 1 minute sandblasting. In experiment of testing shear bond strength, bonding strength was lowered on group B, C, A. There were significant differences between 3 groups. According to period, Bonding strength was the highest on 0 week storage group, and the weakest on 2 week storage group. But there were no significant differences between 3 periods. According to group and period, bonding strength of all group were lowered according to immersion time but there were no significant differences on group B and group C, but there was significant difference according to immersion time on group A. Conclusion: It is useful to sandblast and adopt metal primers when relining Co-Cr metal base dentures in chair-side.

Effects of sonication on physicochemical properties and pore formation of maize starch (초음파처리가 옥수수전분의 이화학특성과 기공 형성에 미치는 영향)

  • Choi, Eun-Hee;Lee, Jae-Kwon
    • Korean Journal of Food Science and Technology
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    • v.49 no.5
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    • pp.507-512
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    • 2017
  • The physicochemical properties of maize starch sonicated at various amplitudes (100, 200, and 300 W) and times (10, 30, and 50 min) were examined. The amount of enzyme-susceptible starch increased marginally after sonication. Sonication increased the amount of oil absorbed in the starch although the degree of oil absorption decreased with an extension of the sonication time, implied that different types and extent of damages occurred. Scanning electron microscopy revealed that ultrasound sonication did not form pores on the surfaces, but caused damages such as depression and erosion. Pasting viscosity of starch decreased with an increase in the severity of sonication conditions because of the weakened polymer network. X-ray diffraction suggested that the crystalline domains in starch were not susceptible to sonication and were more resistance to degradation. Sonicated starch formed more pin-holes on the surfaces in the initial glucoamylase reaction; subsequently, as the reaction proceeded, porous starch with enlarged pores was formed and finally, disrupted granular fragments were observed.

Effects of Brine Immersion and Electrode Contact Type Low Voltage Ohmic Thawing on the Physico-chemical Properties of Pork Meat (염수 침지식 및 전극 접촉식 저전압 Ohmic 해동 처리가 돈육의 이화학적 특성에 미치는 효과)

  • Hong, Geun-Pyo;Min, Sang-Gi;Ko, Se-Hee;Shim, Kook-Bo;Seo, Eun-Ju;Choi, Mi-Jung
    • Food Science of Animal Resources
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    • v.27 no.4
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    • pp.416-423
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    • 2007
  • This study investigated the effect of ohmic thawing on the physicochemical properties of pork meat. The physicochemical properties of pork meat thawed by brine immersion and electrode contact ohmic systems were compared. A more rapid thawing rate was seen with the electrode contact thawing system than with brine immersion. No significant differences in pH were found with increasing voltage for both thawing methods (p>0.05). Increasing the voltage level tended to decrease drip loss, resulting in increased water holding capacity. The shear forces of pork thawed at 50 V did not differ from the control (p>0.05) for both thawing methods. Although significantly high TBARS (p<0.05) values were found at 20 and 40 V for immersion, and 0 V for contact thawing, increasing the voltage level tended to decrease the TBARS values. Regarding TVBN, no significant effect was observed with increasing voltage levels (p>0.05). The total color difference of pork was significantly higher (p<0.05) with immersion thawing than with electrode contact thawing. These results indicate that brine immersion thawing is favorable at high voltage levels, while lower voltage levels are applicable for electrode contact thawing.

Effect of Feeding of Citrus Byproduct on the Physicochemical Properties and Palatability of Pork Loin during Growing Period (성장기에 급여한 감글 부산물이 돈육등심의 이화학적 특성 및 기호성에 미치는 영향)

  • Jung, In-Chul;Moon, Yoon-Hee;Yang, Sung-Joo
    • Journal of Life Science
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    • v.16 no.7 s.80
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    • pp.1164-1168
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    • 2006
  • This study was carried out to investigate the possible for utilization of garbage in pig feed by investigating the functional characteristics of pork from pigs fed dried citrus byproduct. The samples consisted of the pork loin from pigs not fed with dried citrus pulp (DCP-0) and fed with 6% and 10% dried citrus pulp during growing and fattening period (DCP-1) there is no respective comparison here The pH, VBN content, TBARS value, bacterial counts, surface color, water holding capacity, loss degree and rheological properties of the samples were determined by physicochemical properties, and the sensory scores were evaluated. The pH, VBN content, surface color, water holding capacity and loss degree were not different between the samples, but the TBARS value and bacterial counts of DCP-1 were significantly lower than those of the DCP-0 (p<0.05). The cohesiveness, gumminess, chewiness, shear forte value, taste, flavor, tenderness, juiciness and palatability were not different between the samples, but the hardness of DCP-0 was higher than that of the DCP-1 and the springiness of DCP-1 was higher than that of the DCP-0 (p<0.05).

The influence of moisture control on bond strength of composite resin treated with self-etching adhesive system (Self-etching adhesive system에서 수분 조절이 레진의 치질접착강도에 미치는 영향)

  • Jin, Myoung-Uk;Kim, Young-Kyung;Park, Jeong-Won
    • Restorative Dentistry and Endodontics
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    • v.27 no.4
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    • pp.363-369
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    • 2002
  • 최근에 많이 사용되어지고 있는 치과용 접착제는 산 부식 후 수분이 있는 상태에서 적용하는 wet-bonding 술식을 많이 추천하고 있다. 하지만 self-etching primer의 경우 산부식과 priming 과정이 동시에 시행되고, 제조자들은 건조된 치아표면에 적용할 것을 추천하고 있다. 그러나 건조된 정도에 대하여서는 별다른 추천사항이 없으며. 수분이 self-etching primer에 어떤 영향을 미치는지에 대하여서는 별다른 연구가 이루어져 있지 않은 상태이다. 이에 본 연구에서는 치질 삭제 후 남아있는 수분이 self-etching primer의 레진 접착 강도에 어떤 영향을 미치는 지를 알아보고자 하였다. 발거한 대구치 96개를 이용하여 물기가 있는 상태에서 #600 사포로 표면을 연마하고, 법랑질 면을 노출시킨 군과 상아질을 노출시킨 군으로 분류 후, 30분 공기 중 방치 군 (1군), 5초 공기 건조 군 (2군), 1초 공기 건조 군 (3군), 솜으로 약간의 물기를 제거한 군(blot dry) (4군) 등 총 8개의 군으로 나누었다. Self-etching adhesive system인 Clearfil SE Bond primer를 20초간 적용하고, bonding제 도포 후 10초간 광중합 시행하였다. 접착제 처리한 치아면에 몰드를 고정한 후 Clearfil AP-X 복합레진을 2mm 충전하고, 40초간 광중합을 시행하였다. 24시간 후 전단 응력 결합강도를 측정하였으며, 그 결과는 다음과 같이 나타났다. 법랑질과 상아질 모두에서, 30분 건조군과 5초 공기건조군이 1초와 blot drying 군보다 높은 결합강도를 보였으며 통계학적으로 유의한 차이를 보였다(p<0.05). 본 실험 결과에 의하면 self-etching adhesive system을 사용함에 있어서 법랑질과 상아질군 공히 건조된 상태에서 사용하여야 하며 수분의 존재시 치아와의 결합력이 감소하는 것으로 나타났다. 따라서 임상에서 접착제의 적용시 수분의 조절에 주의하여야 할 것으로 사료된다.

Interfacial Characterization of Mineralized Carbon Nanotubes (광물화된 탄소나노튜브 첨가재의 계면 특성화)

  • Park, Chanwook;Jung, Jiwon;Yun, Gunjin
    • Composites Research
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    • v.31 no.5
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    • pp.282-287
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    • 2018
  • In this paper, we explore interfacial properties of the mineralized CNTs when they are employed as reinforcing fillers in a polymer nanocomposite using molecular dynamics (MD) simulations. Recently, several studies on mineralizing carbon nanotubes (CNTs) with an aid of nitrogen doping to CNTs have been reported. However, there is a lack of studies on the reinforcing effects of the mineralized CNTs when it is employed as a filler of nanocomposites. Silica ($SiO_2$) is used as a mineral material and poly (methyl metacrylate) (PMMA) is used as a polymer matrix. Pull-out simulations are conducted to obtain the interfacial energy and the interfacial shear stress. It was found that the silica mineralized CNTs have higher interfacial interaction with the polymer matrix. In the future, by examining various thermomechanical properties of the mineralized-CNT-filler/polymer nanocomposites, we will search for potential applications of the novel reinforcing filler.

한지 도침처리에 따른 광택도 및 강도적 성질 변화

  • Choi, Chan-Ho;Seo, Yeong-Beom;Jeon, Yang;Lee, Ho-Won
    • Proceedings of the Korea Technical Association of the Pulp and Paper Industry Conference
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    • 2001.04a
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    • pp.201-205
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    • 2001
  • 본 연구에서는 한지가공공정의 하나인 도침공정을 현대의 칼렌다링 공정과 비교 분석을 실시한다. 도침은 커다란 나무뭉치를 사용하여 반복적으로 여러 장이 겹쳐 진 한지를 두두림으로서 한지 표면을 평활하게 하며, 광택도를 높이는 효과를 볼 수 있다. 나무뭉치는 밑면이 평활해야만 할 것이다. 보통 한지 제조업자들은 경험 을 토대로 얼마만큼의 도침이 필요한지 결정하고 실시하곤 한다. 이러한 도침공정 에서 현대의 칼렌다링이 할 수 없는 중요한 공정이 존재한다면, 현대의 초지기에도 이러한 원리를 적용함으로써 효과적인 종이의 품질개선을 이룰 수 있는 여지가 충 분히 있다고 판단된다. 한지에 있어서 도침의 역할이 무었인지, 도침은 칼렌다링으 로 대치할 수 있는 지 둥을 비교 검토하였다. 도침공정 연구를 위하여 라이너지 한 종류, 백상지 한종류, 최근에 제조된 전통 한지 세 종류를 사용하였다. 라이너지와 백상지는 일반 제지공장에서 제조되는 방 식을 그대로 사용하여 기계 칼렌다를 통과한 샘플을 얻었으며 칼렌다를 통과하지 않은 라이너지와 백상지를 특별히 같은 지종에서 얻어서 실험을 실시하였다. 기계 칼렌다링을 하지않은 라이너지와 백상지 세 종류의 전통한지는 실험실 칼렌다를 통과시켰고, 또 각각에 도침을 실시하였다. 샘플들의 기본 물성과 처리조건을 표 1 에 정리하였다. 도침 공정에서 사용한 나무 뭉치의 무게는 약 64Kg 이며, 최대 높이 41cm 로 들어올려져 자유낙하에 의한 충격을 종이에 가하였고, 분당 충격횟수는 63회 였다. 라이너지는 도침 및 칼렌다에 의해 밀도가 서서히 증대되는 것을 볼 수 있었다 (그림 1). 도침은 칼렌다에 비해 밀도 증대에 효과적이지는 못하였다. 반면 백상 지에서는 도침이 기계 칼렌다나 실험실 칼렌다보다 현저히 크게 밀도를 증대시킴을 볼 수 있었다 (그림 2). 칼렌다는 종이를 높은 전단력과 압축력으로 변형시키는데 비해 도침은 단순히 압축 압력만을 종이에 가하는 것이 다르다고 볼 수 있는데, 라 이너지와 백상지가 같은 조건하에서 왜 이러한 큰 차이를 보이는 이유를 아직 알수 없다.

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Physical and Sensory Characteristics of Pork from Korean Native Black Pig and Crossbred Black Pig Reared in Jeju Island (제주도에서 사육한 재래 및 개량 흑돼지 고기의 물리적, 관능적 품질 특성)

  • Moon, Yoon-Hee
    • Journal of the East Asian Society of Dietary Life
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    • v.17 no.6
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    • pp.846-852
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    • 2007
  • The objective of this study was to compare the physical and sensory characteristics of pork from Korean native black pigs ($78{\pm}7kg$, female) to the pork of crossbred black pigs ($115{\pm}5kg$, female), both of which were reared for the same period on Jeju Island. The Korean native black pig showed a lower $L^*$ value (lightness) and higher $a^*$-(redness) and $b^*$-values (yellowness) than the crossbred black pig. There were no statistically meaningful differences between the two pigs' loins, hams and bellies of the two breeds of pig in terms of water holding capacity, thawing loss, cooking loss, myofibrillar protein extract, and fragmentation index. The crossbred black pigs showed greater significant differences among the physical characteristics of each part, as compared to the Korean native black pigs. The cooked meat of the Korean native black pig had superior hardness to that of the crossbred black pig, whereas the raw meat had a lower hardness, chewiness, and shear force value. Finally, there was no significant difference between the two pigs in terms of palatability.

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Strengthening Performance of RC Beams Exposed to Freezing and Thawing Cycles after Strengthening in Shear with CFRP Sheet (CFRP 쉬트로 전단보강후 동결융해에 노출된 철근콘크리트 보의 보강성능)

  • Yun, Hyun-Do;Kim, Sun-Woo;Kim, Yun-Su;Lee, Min-Jung;Seo, Soo-Yeon;Choi, Ki-Bong
    • Proceedings of the Korea Concrete Institute Conference
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    • 2008.04a
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    • pp.161-164
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    • 2008
  • In recent years, carbon fiber-reinforced polymer (CFRP) has been widely used for repairing and/or strengthening structural elements in concrete. Not enough test data, however, are available to predict the long-term performance of the repaired and improved structures exposed to weathering. The objective of this research is to study the effect of freeze-thaw cycling on the behavior of reinforced concrete (RC) beams strengthened in shear with carbon fiber sheet. Six small-scale RC beams (100mm${\times]$100mm${\times]$400mm) were strengthened with CFRP in shear, subjected to up to 400 cycles freeze-thawing from -17${\sim}4^{\circ}C$, and tested to failure in four-point bending. Test result, there was no significant damage to carbon fiber sheet strengthened concrete beams had been suffered 30 cycles of freeze-thawing, and more over 60 cycles of freezing-thawing brought about a reduction in resistance of only 25% of the initial level.

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Numerical Study on Roughness Effect for Axi-symmetry Submerged Body in High Reynolds Number (고 레이놀즈 수에서의 축대칭 몰수체의 거칠기에 대한 수치연구)

  • Joung, Tae-Hwan;Song, Hyung-Do;Yum, Jong-Gil;Song, Seongjin;Park, Sunho
    • Journal of the Korean Society of Marine Environment & Safety
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    • v.24 no.2
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    • pp.246-252
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    • 2018
  • In this paper, the friction drag force of 3D submerged body is investigated by considering the surface roughness, the first grid height, and the Reynolds number using open CFD source code, OpenFOAM 4.0. A procedure for estimating drag components by CFD code is set up and suggested in this study. In the 3D submerged body, because of the form factor in the 3D computations, the friction resistance with the small roughness of $12{\mu}m$ obtains different result with the smooth wall. As the Reynolds number increased, the boundary layer becomes thinner and the fiction resistance tends to decrease. In the computations for the effect of y+, the friction resistance and wall shear stress are excessively predicted when the y+ value deviates from the log layer. This is presumably because the boundary layer becomes thicker and the turbulence energy is excessively predicted in the nose due to the increase in y+ value. As the roughness increases, the boundary layer becomes thicker and the turbulence kinetic energy on the surface increases. From this study, the drag estimation method, considering the roughness by numerical analysis for ships or offshore structures, can be provided by using the suggested the y+ value and surface roughness with wall function.