• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2006.06a
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• pp.280-281
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• 2006

Cordierite 결정상을 LTCC공정 적용온도에서 소결하기 위한 glass 조성을 조사하였다. 상용의 glass중 Pb-B-Si-O계, Na-Zn-B-O계 glass를 선택하였고 LTCC용 기판소재로서의 가능성을 확인하기 위하여 저온 동시소성이 가능한 소결온도인 $850^{\circ}C$와 $1000^{\circ}C$ 사이에서 소재의 소결실험을 진행하였다. 소결조건에 따른 상변화, 유전특성을 확인한 결과 glass상, 결정상, 용융에 의한 glass상으로 상의 변화가 있음을 확인 할 수 있었으며, LTCC 소결 조건에서 Pb-B-Si-O계 glass의 경우 2.9~3.7의 낮은 유전율과 0.0027의 우수한 dielectric loss, 내전압 특성을 가지고 있음을 확인하였다.

• Journal of the Microelectronics and Packaging Society
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• v.22 no.3
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• pp.25-30
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• 2015

SAC-coated Cu specimens were fabricated by novel pad finish process using a phenomenon that metal nanoparticles less than 20 nm in diameter melted at a temperature lower than the melting point of bulk metal, and their wettabilities were evaluated. The thickness of SAC305 layer coated at low temperature of $160^{\circ}C$ using SAC305 ink was extremely thin as the level of several nanometers. It was analyzed by Auger electron spectroscopy that $Cu_6Sn_5$ intermetallic layer with a thickness of 10~100 nm and $Cu_3Sn$ intermetallic layer with a thickness of 50~150 nm were sequentially formed under the SAC305 coating layer. The thickness of formed intermetallic layers was thicker in electroplated Cu than rolled Cu, which attributed to improved surface roughness in the electroplated Cu. The improved surface roughness induces the contact, melting, and reaction of a larger number of SAC305 nanoparticles per the unit area of Cu specimen. In the wetting angle test using SAC305 solder balls, the Cu coated with SAC305 through the low temperature process presented evidently low wetting angles than those in non-coated Cu, indicating that only a few nanometer-thick SAC305 coating layer on Cu could also cause the enhancement of wettability.

• The Journal of the Korea Contents Association
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• v.10 no.11
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• pp.243-250
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• 2010

The bonding strength and color reproducibility of titanium-ceramic prosthesis were analyzed the effect according to the surface treatments of titanium and the glazing temperatures of the low fused porcelain. The result of bonding strength compared with respect to the surface treatments was observed that the STB1 group coated by TiN had strongest boding strength and then came the SB1 group used special bonding agent, the SGB1 group coated by gold in that order. The bonding strength by the glazing temperature was indicated that the group with $770^{\circ}C$ of glazing temperature was observed increasing the bonding strength as compared with it of the other group, and the group with $810^{\circ}C$ of glazing temperature was observed to be decreased the bonding strength. Glazing temperature increases, the color by the surface treatment of titanium influenced the color of titanium-ceramic on account of getting higher brightness(${\Delta}L$). As a this result, the SB1 and SGB3 groups was evaluated to has the best color reproducibility.

• Polymer(Korea)
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• v.26 no.4
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• pp.483-491
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• 2002

Polyurethane (PU)/nylon 6 blends were prepared by melt blending with Haake Rheomix at $250^{\circ}C$. The compositions of PU/nylon 6 blends were 10/90, 20/80, 30/70, 40/60, and 50/50 (wt%). The effects of PU contents and blending time on the crystal structure, tan $\delta$, the tensile properties, and the impact behavior were investigated by means of WAXD and DMA, etc. The crystalline diffraction peaks are broadened, and their intensities are reduced with increasing PU contents and blending time. The glass transition temperature, the tensile strength, and the tensile modulus of the blends are also decreased and the elongation at break is increased. The influence of PU content on the crystal structure, tan 3, and the tensile properties of PU/nylon 6 blends is more significant than that of blending time. The impact strength of PU/nylon 6 (10/90 wt%) blends measured at 20 and $-35^{\circ}C$ could be greatly improved.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.6 no.2
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• pp.247-253
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• 1996

Microscopic analysis has been performed in order to investigate effects of the microstructure of the starting feed rods on the morphology of the S-L interface and the stability of the molten zone during single crystal growth of $SrTiO_{3}$ using a floating zone method. Undoped and $Fe_{2}O_{3}$ doped $SrTiO_{3}$ doped $SrTiO_{3}$ specimens, sintered at the different temperatures have been used. In the case of the feed rods sintered at the lower temperature($1400^{\circ}C$), the poor densification made the stability of the molten zone difficult to maintain. The feed rods sintered at the higher temperature ($1600^{\circ}C$) exhibited the higher density but their molten zone was difficult to maintain due to the presence of the abnormally grown grains. It is concluded that the uniform grain size distribution of the feed rod is the critical factor to maintain the stable molten zone and therefore to give optimum growth condition during FZ single crystal growth.

• Journal of the Korea Organic Resources Recycling Association
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• v.14 no.3
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• pp.85-90
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• 2006

The purpose of this research is to design an imitation boiler similar to the waste heat boiler installed on a plasma melting furnace in order to acquire a capability of a thermal design as to the circulation of heat and the discharge of noxious gas inside a boiler and to improve the efficiency of a waste heat boiler using the CFD (Computation Fluid Dynamics) program. The position of corrosion and the generation of a clinker inside a boiler due to temperature changes, combustion gas flows, and corrosive gases inside a boiler are examined to design the structure of an efficient boiler and recycle energy. As a result of this research, the boiler installed on a plasma melting furnace met the conditions of design by cooling the combustion gases discharged after the second combustion from an exhaust port, originally at 1,200 degrees Celsius, down to around 450 degrees Celsius. On the other hand, the circulation of corrosive gases (SOx and HCL) may lead to the generation of corrosion or a clinker in the upper and lower parts of an exhaust port more easily than any other parts of a boiler. Accordingly, the corrosion on the inside and outside walls of a boiler may result in a shortened lifespan of a boiler and an inability to recycle waste heat in an efficient manner. A prevention against corrosion at high and low temperatures needs to be considered in detail.

• Journal of the Microelectronics and Packaging Society
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• v.10 no.4
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• pp.1-8
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• 2003

Thermo-mechanical behavior of a ceramic ball grid array (CBGA) package assembly are characterized by high sensitive moire interferometry. Moir fringe patterns are recorded and analyzed at various temperatures in a temperature cycle. Thermal-history dependent analyses of global and local deformations are presented, and bending deformation (warpage) of the package and shear strain in the rightmost solder ball are discussed. A significant non-linear global behavior is documented due to stress relaxation at high temperature. Analysis of the solder interconnections reveals that inelastic deformation accumulates on only eutectic solder fillet region at high temperatures.

• Proceedings of the KAIS Fall Conference
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• 2011.12b
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• pp.382-384
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• 2011

최근 오일샌드, 극지유전, 심해저자원 등 극한지 자원개발이 활발해짐에 따라 수요가 증대되고 있는 극한지용 내마식 소재는 내마식성과 함께 저온 인성이 요구되고 있다. 철계 합금에서 관찰되는 변형유기 마르텐사이트 상변태는 입자의 충돌에 의한 충격을 흡수하고 소재의 표면을 가공경화시켜 내마식성 향상 및 저온 인성에 기여할 수 있을 것으로 기대되고 있지만 합금조성의 정교한 제어가 필요하기 때문에 오버레이 용접에 적용하기 위해서는 모재와의 희석률을 제어하는 방안이 필요하다. 용접플럭스 설계기술은 용접시 금속이행모드, 용융풀 거동 등과 같은 용접현상 제어를 통해 오버레이 용접재료의 용접성과 용접비드형상, 용접부 희석률을 최적화할 수 있는 기술이다. 본 연구에서는 내마식 고인성 오버레이 용접재료의 개발을 위해 다양한 용접플럭스를 첨가한 메탈코어드 와이어를 제조하고 일정 송급속도에서 GMA 용접시 용접전압과 용접전류 간의 관계를 분석하여 용접플럭스가 아크현상 및 희석률에 미치는 영향을 조사하였다.

• Proceedings of the KWS Conference
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• 2010.05a
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• pp.72-72
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• 2010

최근 오일샌드, 극지유전, 심해저자원 등 극한지 자원개발이 활발해짐에 따라 수요가 증대되고 있는 극한지용 내마식 소재는 내마식성과 함께 저온 인성이 요구된다. 철계 합금에서 관찰되는 변형유기 마르텐사이트 상변태는 입자의 충돌에 의한 충격을 흡수하고 소재의 표면을 가공경화시켜 내마식성 향상 및 저온 인성에 기여할 수 있을 것으로 기대되고 있지만 합금조성의 정교한 제어가 필요하기 때문에 오버레이 용접에 적용하기 위해서는 모재와의 희석률을 제어하는 방안이 필요하다. 용접플럭스 설계기술은 용접시 금속이행모드, 용융지 유동거동 등과 같은 용접현상 제어를 통해 오버레이 용접재료의 용접성과 용접부 희석률을 최적화할 수 있는 기술이다. 본 연구에서는 내마식 고인성 오버레이 용접재료의 개발을 위해 Fe-12Cr-1.2C 합금조성을 갖는 메탈코어드 와이어에 대하여 아크안정제로 사용되는 Ca 함유 용접플럭스 첨가가 용착부 형상 및 희석률 변화에 미치는 영향을 조사하였다.

• Composites Research
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• v.35 no.3
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• pp.147-152
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• 2022

Low-temperature characteristics according to internal temperature conditions during rotational molding of Type 4 pressure vessel liners were studied in this paper. Since rotational molding has a sensitive effect on the formability of the liner depending on the temperature conditions, the temperature conditions for the polyamide used should be accurately set. The structural changes of polyamide as the liner material was analyzed the surface by atomic force microscope (AFM), and the crystallinity measured with a differential scanning calorimeter (DSC) is used to evaluate the change of the mechanical strength value at low temperature. In addition, the formability of the liner was confirmed by observation of the yellow index inside the liner. As a result, as the melting range of the internal temperature becomes wider, the yellow index shows a lower value, and the elongation and impact characteristics at low temperatures are improved. It was also confirmed that the structure of the polyamide was uniform and the crystallinity was high by AFM and DSC. These experimental results contribute to the improvement of characteristics at low temperatures due to changes in temperature conditions during rotational molding.