• Proceedings of the Materials Research Society of Korea Conference
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• 2010.05a
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• pp.50.2-50.2
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• 2010

니켈기 초내열합금 Inconel 617은 수소생산용 초고온 가스 냉각로의 열 교환기와 고온 가스관 등의 고온 배관용 후보재료로써, Cr, Mo, 와 W등의 첨가물이 함유된 고용 강화된 합금으로, 우수한 고온 강도, 크립 저항성, 내부식성 및 내산화성을 가지고 있는 것으로 알려져 있다. 본 연구에서는 결정립 미세화가 고온열화에 의해 입계를 따라 형성되는 internal oxide에 미치는 영향에 대해 평가하였고, 이러한 internal oxide가 인장응력 하에서 크렉 형성 및 전파에 미치는 영향을 평가하기 위하여 3-point bending test를 수행하였다. 미세한 결정립을 가지는 Inconel 617은 냉간압연 후 재결정을 통해 확보하였으며, as-received(AR)과 grain-refined(GR) Inconel 617은 $950^{\circ}C$에서 2000시간 동안 He분위기 하에서 열화시험을 수행하였다. AR과 GR에 형성된 internal oxide은 깊이와 분포 등의 뚜렷한 차이를 보였으며, 이러한 차이로 인해 인장응력 하에서 크렉 전파의 큰 차이를 나타내었다.

• Journal of Pharmaceutical Investigation
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• v.5 no.4
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• pp.17-23
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• 1975

복용량이 비교적 적고, 난용성 의약품(醫藥品)으로 antirheumatism에 사용되고 있는 phenylbutazone을 macromolecule polymer로서 water soluble carrier인 polyvinylpyrrolidone과 solvent method로 1:1, 1:5, 및 1:9(w/w)의 coprecipitate를 형성(形成)시켰으며, 이들 coprecipitate의 용출 속도를 Pure drug 및 coprecipitate 형성 용매인methanol에서 재결정한 recrystallized pure drug의 그것과 측정 비교(比較)하였다. 1:1,1:5 및 1:9(w/w)의 coprecipitate는 recrystallized pure phenylbutazone보다 약 4.5배의 용출의 증가를 보였고, 이들 1:1,1:5,1:9(w/w)에서의 그 carrier의 양(量)에 따른 용출에의 영향은 거의 없었다. 시간(時間)에 대(對)한 log probit를 plot하여 구(求)한 dissolution half life, $T_{50%}$는 coprecipitate ratio 1:1(w/w)에서는 5.5분, 1:5에서는 10분, 1:9에서는 12.5분이었다.

• Journal of Power System Engineering
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• v.9 no.4
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• pp.90-95
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• 2005

The wire-arc process is a low-cost thermal spray method simply utilizes electrical energy to melt the feedstock wire. It is more userful for field applications, especially to coat large surface area. In this paper, a special Fe-based alloy coatings by using the wire-arc process were developed. Nanoscale composite coatings were achieved either during spraying or through a post heat treatment. As-sprayed Fe-based alloy coatings had been an amorphous matrix structure, after heating to $700^{\circ}C$ for 10 minutes a solid state transformation occurred in the some fraction of amorphous matrix which resulted in the formation of nanostructured recrystallized phase. Scanning electron microscopy (SEM) and field emotional scanning electron microscope(FE-SEM) were applied to analyze the microstructure of the coatings. Additionally hardness and bend resistance of the Fe-based alloy coatings were examined, and these results were compared with those of partially stabilized zirconia(PSZ) coatings by using the plasma spray process.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1996.10a
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• pp.150-156
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• 1996

The cold rolling of metal sheets leads to the formation of an inhomogeneous microstructure and texture. The type and sharpness of texture through the thickness and the degree of inhomogeneity depend on the friction between rolls the rolled material and the geometry of the rolling gap. In order to follow the effect of friction, two kinds of stecimens were prepared by applying with and without lubrication during the cold rolling. Although the deformed microstructure of the specimens rolled without lubrication was much inhomogenous than that of the specimens rolled with lubrication, the effect of lubrication on the cold rolling texture was not found. the recrystallization behavior was strongly dependent on the deformation process. Thus, the retardation of the recrystallization was observed in the specimens rolled without lubrication.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1996.03b
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• pp.48-54
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• 1996

The continuous deformation , multistage deformation and stress relaxation were carried out to investigate the strain induced procipitation by torsion tests in the range of 1000∼800$^{\circ}C$, 0.05/sec∼5/sec for V-microalloyed steel. The starting temperature and time for the initiation of precipitation were determined by stress relaxation tests and the distribution of percipitates increased at higher strain rate and the mean size of precipitates was found to be about 50nm. The precipitation starting time decreased with increasing strain rate from 0.05/sec to 5 /sec and pre-strain. The effect of deformation conditions on the no-recrystallization temperature(Tnr) was determined in the multistage deformation with declining temerature. The Tnr decreased with increasing strain and strain rae. In the controlled rolling, grain refinement and precpitation hardening effects could be achieved by the alternative large pass strain at the latter half pass stage under the condition of low temperature and high strain rate.

• Transactions of Materials Processing
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• v.22 no.8
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• pp.450-455
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• 2013

In the current study, a new dynamic recrystallization model for predicting high temperature flow stress is developed based on a physical model and the mean field theory. In the model, the grain aggregate is assumed as a representative volume element to describe dynamic recrystallization. The flow stress and microstructure during dynamic recrystallization were calculated using three sub-models for work hardening, for nucleation and for growth. In the case of work hardening, a single parameter dislocation density model was used to calculate change of dislocation density and stress in the grains. For modeling nucleation, the nucleation criterion developed was based on the grain boundary bulge mechanism and a constant nucleation rate was assumed. Conventional rate theory was used for describing growth. The flow stress behavior of pure copper was investigated using the model and compared with experimental findings. Simulated results by cellular automata were used for validating the model.

• Transactions of Materials Processing
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• v.5 no.4
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• pp.305-319
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• 1996

In this paper a finite element based system is presented for the prediction of the distributions of the recrystallized grain sizes in the workpiece in hot forging. The system adopts a fully coupled finite element thermo-mechanical model for predicting plastic deformation and heat transfer occurring in the workpiece and employs existing metallurgical models relating the recrystalliza-tion behavior with the thermo-mechanical variables such as temperatures strain and strain rate. The system is applied to upsetting of cylindrical preform. The predicted grain sizes are compared with the measurements. It is further applied to forging of a complex-shaped product.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2002.05a
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• pp.169-172
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• 2002

Recently, the application of 3-roll mill is increasing, because of its flexibility in spread control and stand arrangements due to its compact size. But deformation characteristics and microstructural change in the process is not well known. In this study, austenite grain size (AGS) predictions were made by isothermal FE analyses and a microstructure model available in the literature. From this study, the effect of draught on the AGS characteristics was analyzed based on the divided zones of two major recrystallization behaviors.

• Proceedings of the Materials Research Society of Korea Conference
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• 2012.05a
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• pp.102.1-102.1
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• 2012

Ti 및 Ti 합금은 치과 및 정형외과 등의 분야에서 생체재료로써 다양한 용도로 적용되고 있으며, 보다 안전하고 우수한 특성의 Ti 합금 개발에 대한 관심이 높아지고 있다. 본 연구에서는 Ti-Nb-Ge 합금의 초탄성 특성에 미치는 집합조직의 영향에 대해 조사하였다. 집합조직 제어를 위해 등속 및 이주속 압연을 적용한 후 $850^{\circ}C$에서 30분~2시간까지 어닐링하였다. 광학현미경과 SEM-EBSD를 이용하여 미세조직 및 집합조직을 분석하고, 순환식 인장시험을 통해 시편의 초탄성 특성을 평가하였다. 등속압연 후 어닐링한 시료의 경우 alpha-fiber 집합조직이 발달하는 한편, 이속압연 후 어닐링한 시료는 {113}// 및 {331}의 집합조직이 발달하는 것으로 나타났다. 마르텐사이트 변태에 의한 변형회복능과 집합조직 성분별 강도의 관계를 비교한 결과, alpha-fiber 집합조직이 발달할수록 변형회복능이 증가하는 것으로 나타났다.

• Journal of the korean Society of Automotive Engineers
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• v.13 no.6
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• pp.39-47
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• 1991

본 연구논문의 내용은 현재 국내 자동차 업계에서 자동차 배기부품으로 전량 수입되고 있는 STS 409L 스테인레스강을 국산화하기 위한 개발연구에 대한 내용으로서 배기관용 스테인레스강 409L의 제조기술과 관련된 국내외 기술개발 동향과 포항제철 스테인레스 제조설비에 맞는 적정합금성분계와 조업조건을 도출하기 위하여 실험적으로 시험조사하여 품질 제특성을 평가한 연구결과이다. 주요 내용으로서 합금원소가 열연 및 냉연 소둔조업조건에 미치는 영향을 조사하기 위하여, C, N과 Ti 또는 Ti+Nb 원소 첨가를 변화시킨 409L 계열강에 있어서 소둔조업조건에 따른 재결정과 상변태 거동을 조사하엿으며, TIG용접에 의한 용접부의 기계적 특성과 가공성 그리고 고온부식 및 응축수 부식 시험을 통한 내식성 등의 품질 특성 평가를 조사 서술하였다.