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New Methods of Measuring Magnetization and Coercivity by Torque Magnetometer (토크마그네토미터를 이요한 자화 및 보자력측정의 새로운 방법)

  • Heo, Jin;Sin, Seong-Cheol
    • Journal of the Korean Magnetics Society
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    • v.2 no.3
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    • pp.263-267
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    • 1992
  • We have developed new techniques to measure the magnetization and coercivity of a uniaxial magnetic material using a torque magnetometer. The magnetization could be measured from the slope of the linear region in a plot of the torque ${\tau}/H$ versus the applied field H, when the direction of the applied field was normal to the uniaxial orientation. While, the coercivity could be obtained by taking the value of applied field where the torque was zero, when the direction of the applied field was $(180+{\delta})$ degrees from the uniaxial orientation. The techniques were applied to determine the magnetizations and coercivities of several Co /Pd multilayer thin films and the results were confirmed to be similar within a 2 % difference to those obtained by a vibrating sample magnetometer.

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Effect of quenching rate and crystallization behavior on the magnetic properties of annealed Nd-Fe-B ribbons (Melt-spun Nd-Fe-B 리본의 자기적 특성에 미치는 급속응고속도 및 결정화 거동의 영향)

  • 이경섭;서수정
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.8 no.4
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    • pp.655-659
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    • 1998
  • The effect of quenching speed of melt-spinning on intrinsic coercivity ($_iH_c$$) of annealed ribbons and the crystallization behavior from amorphous $Nd_{14.73}Fe_{78.67}B_{6.60}$ alloy have been studied. We have found that the intrinsic coecivity for annealed melt-spun ribbon is reduced with increasing of quenching rate. $\alpha$-Fe and $Fe_3B$ were formed as intermediate phases prior to the formation of $Nd_2Fe_{14}B$ phase during crystallization. The $Fe_3B$ is disappeared with crystallization of $Nd_2Fe_{14}B$ phase. But the $\alpha$-Fe phase is retained in fully crystallized ribbon by annealing. The intrinsic coercivity loss of annealed ribbon with increasing of quenching speed is believed to be due to existence of soft magnetic phase $\alpha$-Fe in annealed ribbons.

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Frture mapping and deep-seated ground water exploration in the crystalline rocks by integrated geophysical techniques (종합적 물리탐사에 의한 파쇄대 및 심부 지하수 탐사)

  • 정승환;김정호;조인기;전정수
    • The Journal of Engineering Geology
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    • v.2 no.2
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    • pp.113-130
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    • 1992
  • Groundwater in crystalline basement is controlled primarily by tectonic fractures. It is evident that the delineation of the heavily faulted area and/or fractures deeply developped should be considerable value in deep-seated low enthalphy geothermal water. Electrical and electromagnetic methods have effectively been employed to map hydraulic faults and shear zones for groundwater exploration. In this study VLi; dipoledipole resistivity, controlled source audio~frequency magneto-telluric(CSAMT) and magnetic methods were applied in the Bomun resort area, adjacent to Kyongju city, southeastern part of Korea. The integrated geophysical tools employed in this experiment can be manifested themselves as: 1. Magnetic high for granite intrusions which is more favorable for geothermal gradient increase in depth. 2. VLF cross-over trends for mapping linear shallow conductive fractures and shear zones. 3. Dipole-dipole resistivity distributions for the deep-seated(less than 500m in depth) fractures and shear zones. The dipole-dipole resistivity field data were inverted to the true resistivity distribution with two-dimensional automatic inversion program based on the finite-difference method. 4. CSAMT provides an efficient way of delineating fractures and fault zones if the depth is greater than about 500m.

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Relationship between Magnetic and Mechanical Properties of Cermet Tools (절삭공구용 서멧의 자기적 특성과 기계적 성질의 관계)

  • Ahn, Dong-Gil;Lee, Jeong-Hee
    • Journal of the Korean Society for Nondestructive Testing
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    • v.20 no.3
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    • pp.231-237
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    • 2000
  • The commercial cermet cutting tools consist of multi-carbide and a binder metal of iron group, such as cobalt and nickel which are ferromagnetic. In this paper, a new approach to evaluate the mechanical properties of TiCN based cermet by magnetic properties were studied in relation to binder content and sintering conditions. The experimental cermet was prepared using commercial composition with the other binder contents by PM process. It was found that the magnetic properties of the sintered cermets remarkably depended on the microstructure and the total carbon content. The magnetic saturation was proportional to increment of coercive force. At high carbon content in sintered cermet, the magnetic saturation was increased by decreasing the concentration of solutes such as W, Mo, Ti in Co-Ni binder. As the coercive force increases, the hardness usually increases. The strength and toughness of the cermet also increased with increasing the magnetic saturation. The measurement of magnetic properties made it possible to evaluate the mechanical properties in the cermet cutting tools.

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Analysis of Regional Potential Mapping Factors of Metal Deposits using Machine Learning (머신러닝을 이용한 광역 금속 광상 배태 잠재성 평가 인자 분석)

  • Park, Gyesoon
    • Geophysics and Geophysical Exploration
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    • v.23 no.3
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    • pp.149-156
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    • 2020
  • The genesis of ore bodies is a very diverse and complex process, and the target depth of mineral exploration increases. These create a need for predictive mineral exploration, which may be facilitated by the advancement of machine learning and geological database. In this study, we confirm that the faults and igneous rocks distributions and magnetic data can be used as input data for potential mapping using deep neural networks. When the input data are constructed with faults, igneous rocks, and magnetic data, we can build a potential mapping model of the metal deposit that has a predictive accuracy greater than 0.9. If detailed geological and geophysical data are obtained, this approach can be applied to the potential mapping on a mine scale. In addition, we confirm that the magnetic data, which provide the distribution of the underground igneous rock, can supplement the limited information from the surface igneous rock distribution. Therefore, rather than simply integrating various data sets, it will be more important to integrate information considering the geological correlation to genesis of minerals.

Characterization of FePtN Nano-particles Synthesized by Thermal Decomposition and Mixed-gas Nitrification (열분해법과 혼합가스 질화법으로 합성한 FePtN 나노 입자의 특성)

  • Oh, Young Woo
    • Journal of the Korean Magnetics Society
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    • v.26 no.4
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    • pp.129-132
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    • 2016
  • The effect of thermal-nitrification on L1o transfomation in nano-sized FePt particles was studied. As-synthesized FePt nanoparticles by thermal decomposition method have fcc structured phase and their Hc and Ms were 247.34 Oe and 27.308 emu/g, respectively. According to the XRD analysis, phase transformation from fcc (face centered cubic) to fct (face centered tetragonal) structure was revealed by heating under $NH_3+H_2$ mixed-gas atmosphere. Also a slight shift of each (111) peak indicated phase transformation from fcc to fct structure. Hc and Ms of fct FePtN were 1058.2 Oe and 32.718 emu/g, respectively. The nano-sized FePtN magnetic particles synthesized by thermal decomposition method and mixed-gas nitrification are expected for advanced applications such as high density magnetic recording media and biomedical materials.

Effects of process temperature on the microstructure and magnetic properties of electrodeposited Co-Pt alloy thin films (전해도금 공정온도가 Co-Pt 합금 박막의 미세구조 및 자기적 특성에 미치는 영향)

  • Lee, C.H.;Jeong, G.H.;Park, J.K.;Lee, K.K.;Suh, S.J.
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.18 no.2
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    • pp.87-90
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    • 2008
  • Co-Pt alloy thin films were galvanostatically electrodeposited on Ru (30 nm)/Ta (5 nm)/Si (100) substrates from a amino-citrate based electrolyte. We used Ru(0002)-oriented buffer layers to control the crystallinity and orientation of the Co-Pt alloy thin films. The effect of solution temperature on the microstructure and magnetic properties of the Co-Pt alloy thin film was investigated. The samples were characterized by EDS, FESEM, XRD diffractometer using Cu $K{\alpha}$ radiation. The magnetic properties of these films were analyzed by a VSM and torque magnetometer. The Co-Pt alloy thin films were exhibited very high out-of-plane coercivity and squareness of the multilayer were 6527 Oe and 0.93, respectively, without heat treatment.

Variation of Magnetic Properties of Fe/CoNbZr with Multilayer Structure and Annealing Condition (Fe/CoNbZr 다층박막의 구조 및 열처리 조건에 따른 자기적 특성)

  • 이성래;김은학;김영근
    • Journal of the Korean Magnetics Society
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    • v.11 no.2
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    • pp.45-49
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    • 2001
  • Effects of multilayer structure and annealing condition on the soft magnetic properties of sputtered Fe/CoNbZr multilayers were investigated. We observed a minimum coercivity (1.1 Oe) at 5 nm thick Fe layer and the maximum permeability (2300) at 15 nm Fe layer and high saturation magnetization in the as-deposited state. As a result of increase of Fe grain size, coercivity increases with increasing Fe layer thickness. Degradation of ${\mu}$ at the thin Fe layer region may be due to the intermixed phase of high magnetostriction, such as CoFe. Optimum annealing condition was obtained through annealing at 300 $^{\circ}C$ for 40 min (${\mu}$=2500, H$\sub$c/=0.35 Oe). Enhancement of permeability was observed in the temperature range of 250∼300$^{\circ}C$. These results may closely be related with lowering the anisotropy energy by lattice deformation (0.4%) and enhanced uniaxial anisotropy.

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Improvement of Magnetic Properties of Nd-Fe-B Type Sintered Magnet (Nd-Fe-B계 소결자석의 자기적특성 향상 연구)

  • Kim, Yoon-B.;Jung, W.S.;Jeung, W.Y.
    • Journal of the Korean Magnetics Society
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    • v.12 no.2
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    • pp.57-63
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    • 2002
  • In order to increase the magnetic properties of a Nd-Fe-B sintered magnet, the general factors including particle size and its distribution, volume fraction of Nd$_2$Fe$_{14}$B phase, degree of alignment of Nd$_2$Fe$_{14}$B grain, oxygen content and grain size etc. should be optimized by controlling the composition of Nd-Fe-B alloy as well as the manufacturing process. In this study, fabrication of the Nd-Fe-B sintered magnet was carried out in a laboratory scale by controlling the composition of Nd-Fe-B alloy and the manufacturing process. The optimum milling condition was found by investigating the milling media, milling time and ball size. The addition of FeGa was effective to increase the coercivity of the Nd-Fe-B sintered magnet. A remanence of 14.4 kG, a coercivity of 9.4 kOe and a maximum energy product of 47 MGOe were obtained from the sintered magnet.

Effects of Deposition and Annealing Conditions on Structural and Magnetic Properties of CoNbZr Alloy Films (제조 조건 및 열처리 조건에 따르는 CoNbZr 합금 박막의 구조 및 자기적 성질에 관한 연구)

  • 양준석;이성래
    • Journal of the Korean Magnetics Society
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    • v.10 no.2
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    • pp.54-61
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    • 2000
  • The structural and magnetic properties of sputtered CoNbZr alloy films were investigated. In the as-deposited $Co_{87.0}$N $b_{8.5}$Z $r_{4.5}$ film deposited at 2 mTorr and 130 W, we observed the minimum coercivity of 1.75 Oe, the maximum resistivity of 3000 $\mu$Ω.cm and permeability of 1095 at 100 MHz. As the Ar pressure or the RF input power increased, the permeability of films at 100 MHz decreased and the coercivity increased because of the development of columnar structure and the formation of unstable amorphous phase. Permeability lower than 100 and coercivity of 60 Oe were observed in film deposited at 1 mTorr or 190 W due to the formation of crystalline phase. Magnetic anisotropy field of as-deposited films could be reduced by rotating field annealing for 120 minutes at 30$0^{\circ}C$. After the annealing, the anisotropy field (Hk) decreased from 1.43 Oe to 0.3 Oe and the permeability increased from 1095 to 1345 because defects in as-deposited films were eliminated by the annealing.aling.

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