• Journal of the Korean Magnetics Society
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• v.3 no.4
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• pp.289-292
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• 1993

[Ni/Fe/Cu] and [Fe/Ni/Fe/Cu] multilayers were prepared with three gun rf-magnetron sputtering, and dependence of magnetoresistance on the Ni IFe thickness ratio was investigated. Vaccum annealing was tried to invetigated the effect of annealing. Oscillation of magnetoresistance on the Cu spacer thickness was dbserved in these two kinds of multilayers. When the thickness of Fe inserted into the Ni/Cu interface was about $3\;\AA$. the maximum value of magnetoresistance(13 %) could be observed. In a sample of $1~2\;\AA$ Fe thickness, saturation field decreased significantly, while magnetoresistace decreased slightly in comparison with the sample of $3\;\AA$ Fe. In ${[Cu(23\;\AA)/Fe(1\;\AA)/Ni(18\;\AA)/Fe(1\;\AA)]}_{20}/Fe(80\;\AA)/Si$, 6 % magnetoresistance with 100 Oe saturation field could be obtained. No appreciable change in magnetoresistance and saturation field could be observed by low temperature annealing. Formation of Ni-Fe alloy was not confinred.

• Journal of the Korean Magnetics Society
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• v.7 no.6
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• pp.293-298
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• 1997

$Fe_5Si_Xb_{5-x}$ (x=0, 1, 2, 3) powders were prepared by mechanical alloying, and their phases and magnetic properties were investigated by using XRD, TEM, Mossbauer spectroscopy and VSM. Starting elements are incorporated into $\alpha$-Fe in the early stage of mechanical alloying, and the stable phases are formed as the milling proceeds. After the annealing at 80$0^{\circ}C$ for 2 hours, it is found that the FeB and $Fe_2B$ phases coexist for the $Fe_5B_5$(x=0) composition. By substituting Si for B, the formation of $Fe_2B$ phase is restricted and the $Fe_5SiB_2$, $Fe_2Si_{0.4}B_{0.6}$ and paramagnetic phase begin to appear. The FeB phase has wide range of hyperfine magnetic field because it is not fully crystallized on the annealing at 800 $^{\circ}C$. On the contrary, others have good crystalline phases and show well-defined hyperfine magnetic field. Magnetic saturation is highest for the $Fe_5B_5$ composition where the amount of the $Fe_2B$ phase in large.

• Proceedings of the Korean Vacuum Society Conference
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• 2016.02a
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• pp.227.2-227.2
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• 2016

환형 전자 빔이 진행됨에 따라 표면파의 전단 유동에 의해 발생 및 진행되는 diocotron instability(다이오코트론 불안정성)를 안정시키기 위해, 나선형 자기장이 인가된 상황을 2차원 PIC 시뮬레이션을 통해 구현하고 그 효과에 대한 조사가 수행되었다. 나선형 자기장은 2차원 단면 상에서 회전하는 자기장으로 표현되었고, 이에 대해서 자기장이 회전하는 각도와 회전 주기, 회전 방향을 변수로 하여 그 효과를 나타내었다. 결과적으로, 자기장이 회전 하는 방향과 전자 빔이 회전하는 방향이 반대가 되었을 때, diocotron instability가 진정되는 효과를 얻었으며 이는 불안정성의 근원인 전단 유동을 완화시킴으로써 얻어진 결과임이 확인되었다. 이 때, 동반되는 밀도 분산 현상에 대해서도 고려가 되었고, 결론적으로 인가되는 나선형 자기장에 대하여 가장 적절한 조건에 대한 조사가 수행되었다.

• Journal of the Korean Magnetics Society
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• v.9 no.2
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• pp.71-77
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• 1999

본 연구에서는 이방성 Nd-Fe-B계 자성분말과 바인더로 polypropylene을 사용하여 compound를 제조한 후 사출성형에 의해 이방성 Nd-Fe-B 레진본드자석을 제조하여 자성분말의 함량, 인가자장 및 사출성형 온도에 따른 자기적 특성 및 유변학적 특성을 조사하였다. Torque sensor에 의해 측정한 본 연구에 사용된 이방상 Nd-Fe-B계 자성분말의 최대 분말함량은 70.7vol%이었다. Compound의 자성분말 함량이 증가함에 따라 레진본드자석의 잔류자속밀도와 최대자기에너지적은 증가하여 54vol%에서 최대값을 보인후 다시 감소하였고, 보자력은 변화가 없었다. 54vol% 자성분말 함량 이상에서 잔류자속밀도와 최대자기에너지적이 다시 감소하는 것은 사출성형시 자성분말의 배향도 저하에 기인한다. 이것은 compound의 자성분말 함량이 증가함에 따라 compound의 유동성이 저하되어 사출성형시 자성분말의 이방화를 어렵게 만들기 때문이다. 사출성형 온도가 증가함에 따라 레진본드자석의 자기적 특성은 증가하였다. 이는 성형온도가 증가함에 따라 compound의 유동성이 향상되어 자성분말의 배향도가 증가되었기 때문이다. 따라서 사출성형에 의해 이방성 Nd-Fe-B계 레진본드자석 제조시 자기적 특성을 향상시키기 위해서는 compound의 자성말 함량 뿐만 아니라 compound의 유동성이 중요하게 고려되어야 한다.

• Journal of Adhesion and Interface
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• v.15 no.4
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• pp.161-168
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• 2014

New self-assembled discotic liquid crystals have been prepared through single hydrogen bonding between phenol and pyridine moieties, and their liquid crystalline properties were investigated. For the construction of discotic structure, we used phloroglucinol as a core molecule and trans-4-alkoxy-4'-stilbazoles with systematically varied alkyl chain lengths as peripheral units. FTIR results showed that the intermolecular hydrogen bonds between core and peripheral molecules are successfully formed, and the stability of the hydrogen bond is strongly influenced by molecular ordering. Discotic complexes exhibited different liquid crystalline phases depending on the length of alkyl chains around the discotic mesogen. The discotic complexes with longer alkyl chains showed hexagonal columnar mesophases, while the other complexes formed nematic columnar mesophases. These results indicated that the type of mesophase structure was strongly dependent on the alkyl chain length around the aromatic core.

• Elastomers and Composites
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• v.34 no.1
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• pp.45-52
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• 1999

This paper describes how the gold particles self assemble on the specific phase on the microphase separated block copolymer thin film and form a well ordered patterns. For this study, polystyrene-polybutadiene-polystyrene (PS-PB-PS) triblock copolymer (30wt % PS) thin films (${\sim}100nm$) having a cylindrical morphology were cast from 0.1wt% toluene solution to be used as polymer thin film templates. The films having either vertical PS cylinders or in-plane PS cylinders in PB matrix from each different solvent evaporation condition were obtained. Cross-sectional transmission electron microscopy(TEM) was used to study the surface and bulk morphologies of block copolymer thin films. Small amount of gold particles was evaporated on a block copolymer thin film template to obtain a nano-scale pattern. When an as-cast thin film template was used, gold particles preferentially self assemble on the low surface tension PB phase and a relatively well ordered pattern in nano-scale was produced. However, after the formation of a low surface energy PB rich layer upon annealing, a gold self-assembled pattern was not observed.

• Journal of the Korean Orthopaedic Association
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• v.53 no.6
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• pp.530-539
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• 2018

Purpose: We aimed to evaluate the magnetic resonance imaging (MRI) findings of congenital postaxial polydactyly of the foot. Materials and Methods: Three-hundred and forty-seven feet of 288 patients who underwent congenital postaxial polydactyly or polysyndactyly correction were divided into five subtypes according to the radiographic shapes of deformity origins (widened metatarsal head, bifid, fused duplicated, incompletely duplicated, or completely duplicated). MRIs were assessed to determine whether they unrevealed areas were fused or separated. MRI was also used to assess cases with radiographic phalangeal aplasia. Results: Huge variations were noted in MRIs. Fusion or separation at the base or head between original and extra digits were observed, and MRI effectively depicted phalangeal aplastic areas. Conclusion: MRI evaluations of congenital postaxial polydactyly of the foot are useful for determining the anatomical statuses which were not visualized by plain radiography (level of evidence: 3).

• Proceedings of the Korean Vacuum Society Conference
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• 2013.02a
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• pp.374-375
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• 2013

Al/Ni 나노 멀티 포일은 상온에서 외부 방전 및 촉발에 따라 급속한 자기 발열 반응이 일어나는 특성을 보여, 외부 촉발을 통해 상온에서 온도를 높일 수 없는 접합이나 마이크로 수준의 미세 접합이 가능한 접합재료로서 활용이 상당히 기대되는 재료이다. 본 연구에서는 스퍼터링법을 이용하여 한 층이 20 nm 이하에서 Al과 Ni의 혼합 기준을 달리한 Al/Ni 나노 멀티 900층을 제조와 제조된 반응성 포일이 자기 발열 반응에 따른 미세구조에 대해 조사하였다. 박막의 증착은 3~10 mTorr의 공정압력 으로 Al 타겟 전류 1.7 A, Ni 타겟 전류 1.4 A로 하여 증착시간을 조절하여 제조하였다. SEM과 EDX를 통하여 Al/Ni 나노 멀티 포일의 성장구조와 각 원소의 함량을 조사하였다. XRD 미세결정구조 분석은 제조된 반응성 포일과 외부 촉발시킨 후 자기 발열 반응에 의해 형성되는 혼합 상에 대한 조사를 실시하였다. 혼합기준이 1:1의 Al/Ni 나노 멀티 포일에서 약 $980^{\circ}C$의 발열이 발생하는 것을 Pyrometer를 통해 측정하였으며, 자기 발열 반응 후의 혼합 상은 AlNi이 형성되었다. Ni rich 포일에서는 약 $730^{\circ}C$의 발열이 발생하였고, 혼합상으로 주로 AlNi이 형성되었고 Al3Ni2도 나타났으며, 반응에 참여하지 못한 Ni이 남아있는 것을 관찰하였다. Al rich 포일에서는 약 $720^{\circ}C$의 발열과 함께 AlNi, $AlNi_3$이 형성되었고 반응에 참여하지 못한 Al이 미세하게 나타났다.

• Journal of the Korean Magnetics Society
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• v.3 no.2
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• pp.87-93
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• 1993

Iron nitride (Fe-N) magnetic thin films were deposited using a DC magnetron sputtering system. Microstructures and magnetic properties were examined as a function of deposition power and nitrogen gas input ratio. The nitrogen content in the film was found to be the major factor determining the microstructure and the magnetic properties. The films deposited at low nitrogen input ratios have an $\alpha$-Fe structure of which the lattice is expanded due to the nitrogen atoms incorporated at the interstitial sites. As the nitrogen content in the film increases, the degree of lat-tice expansion increases and the value of saturation magnetization decreases linearly. The films with a high degree of lattice expansion give very low values of coercivity, which is attributed to the disturbance of colunmar growth and the decrease of surface roughness. Further increase in the nitrogen input ratio causes the phase transfonnation from $\alpha$-Fe to $Fe_{2-3}N$, resulting in the marked reduction in the saturation magnetization. The phase transformation occurs when, regardless of deposition conditions, the nitrogen content reaches at 15 at.% and the lattice is expanded by 5%.

• Journal of the Korean Magnetics Society
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• v.8 no.4
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• pp.210-215
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• 1998

$Nd_{15}Fe_{77}B_8$ and $Nd_{16}Fe_{76}B_8$ powders were prepared by mechanical alloying in Ar atmosphere, and their phases and magnetic properties were investigated with as a function of the annealing temperature. It was found that the mechanical alloyed $Nd_{16}Fe_{76}B_8$ powder for 450 hours was amorphous phase with a part of $\alpha$-Fe crystallites. The obtained powders at 700 $^{\circ}C$ for 30 minute resulted in two phase of $Nd_2Fe_{14}B$ and $NdB_6$ by the solid-state reaction. The mechanical alloyed $Nd_{16}Fe_{76}B_8$ powder for 450 hour and annealed at 700 $^{\circ}C$ for 30 minute was showed $_iH_c\;of\;9.91\;kOe,\; B_{max}\;of\;12.93\;kG,\;Br\;of\;7.6\;kG\;and\;(BH)_{max}\;10.1\;MGOe$.