• Title/Summary/Keyword: 자기결정 이방성

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Crystal Structure and Low Temperature Magnetic Properties of Melt-Spun $Sm_{2}Co_{7}B_{3}$ Compound (급냉응고된 $Sm_{2}Co_{3}B_{7}$ 화합물의 결정구조와 저온 자기특성)

  • Yang, C.J.;Lee, W.Y.;Choi, S.D.
    • Journal of the Korean Magnetics Society
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    • v.3 no.4
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    • pp.284-288
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    • 1993
  • Low temperature magnetic properties and crystal structures of melt-spun $Sm_{2}Co_{7}B_{3}$ compound were characterized. The magnetic measurements in the temperature range 77 K~450 K indicated that a spin-reorientation took place at about 150~160 K. A large anisotropy was observed(Ha=135 kOe at 300 K, 725 kOe at 77 K) for $Sm_{2}Co_{7}B_{3}$ although the magnetic moment is rather low. The crystal structure of the $Sm_{2}Co_{7}B_{3}$ compound was analyzed in detail by Rietveld analysis of powder diffraction pattern, and it was revealed that B(4h) atoms are not placed in the Sm(2e) layer but in between the Sm(2e) and Co($6i_{1}$) layers.

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MnIr Thickness Dependence of Torque Signals in CoFe/MnIr Thin Films (CoFe/MnIr 박막 재료에서 MnIr의 두께에 따른 토오크 신호 분석)

  • Kim, Dong Young;Yoon, Seok Soo
    • Journal of the Korean Magnetics Society
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    • v.24 no.5
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    • pp.140-145
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    • 2014
  • We analyzed the MnIr thickness dependence of torque signals measured in exchange coupled CoFe/MnIr ($t_{AF}$) bilayers. The measured torque signals were compared with calculated ones by Stoner-Wohlfarth model. The exchange coupling anisotropy $J_c$ was considered for the model calculation between ferromagnetic (F) and antiferromagnetic (AF) layers with uniaxial anisotropy constant of $K_F$ and $K_{AF}$, respectively. The rotational losses were appeared in the range of $0.5t_c$ < $t_{AF}$ < $t_c$ ($=J_c/K_{AF}$) by the unpinned AF layer. While, the unidirectional anisotropy ($J_k$) was caused by the pinned AF layer at $t_{AF}$ > $t_c$. The critical thickness of MnIr layer was $t_c$ = 3.4 nm in CoFe/MnIr bilayers. The rotational losses behavior as shown in $t_{AF}$ = 3 nm sample were explained by the random orientation of the easy axis of AF grains. The unidirectional anisotropy obtained from torque signal of $t_{AF}$ = 10 nm sample was $J_k=0.63J_c$. Thus, the unidirectional anisotropy can be enhanced up to $J_k=J_c$ by aligning the AF easy axis.

EFFECTS OF Nb ON MAGNETIC AND MICROSTRUCTURAL PROPERTIES OF FePt ALLOY FILMS

  • Kim, Min-Kyu;Kim, Young-Keun;Lee, Seong-Rae
    • Proceedings of the Korean Magnestics Society Conference
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    • 2002.12a
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    • pp.176-177
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    • 2002
  • Ll$_{0}$ 규칙 구조를 가지는 동일조성의 FePt는 높은 결정자기이방성에너지로 인해 차세대 고밀도 자기기록매체 재료로서 현재 활발히 연구가 진행되고 있다. 100 Gbit/in$^2$를 목적으로 할 때 결정립의 크기는 10nm 이하가 되어야 한다. [1] 더 나아가 향후 1Tb/in$^2$의 초고기록밀도를 가지는 미디어 재료로서 열적 안정성을 극복하기 위한 측면에서 이용될 수 있다.[2] 이러한 Ll$_{0}$ 규칙 구조를 얻기 위해서 증착된 FePt 합금 박막을 50$0^{\circ}C$이상에서 열처리를 하여야 한다.(중략)

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Variation of Magnetic Properties of Fe/CoNbZr with Multilayer Structure and Annealing Condition (Fe/CoNbZr 다층박막의 구조 및 열처리 조건에 따른 자기적 특성)

  • 이성래;김은학;김영근
    • Journal of the Korean Magnetics Society
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    • v.11 no.2
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    • pp.45-49
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    • 2001
  • Effects of multilayer structure and annealing condition on the soft magnetic properties of sputtered Fe/CoNbZr multilayers were investigated. We observed a minimum coercivity (1.1 Oe) at 5 nm thick Fe layer and the maximum permeability (2300) at 15 nm Fe layer and high saturation magnetization in the as-deposited state. As a result of increase of Fe grain size, coercivity increases with increasing Fe layer thickness. Degradation of ${\mu}$ at the thin Fe layer region may be due to the intermixed phase of high magnetostriction, such as CoFe. Optimum annealing condition was obtained through annealing at 300 $^{\circ}C$ for 40 min (${\mu}$=2500, H$\sub$c/=0.35 Oe). Enhancement of permeability was observed in the temperature range of 250∼300$^{\circ}C$. These results may closely be related with lowering the anisotropy energy by lattice deformation (0.4%) and enhanced uniaxial anisotropy.

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A Study on Anisotropy of Magnetic Susceptibility of Clastic Sedimentary Rocks in the Gyeongsang Basin (경상분지 쇄설성 퇴적암의 대자율 이방성 연구)

  • Choi, Eun-Kyeong;Kim, Sung-Wook;Hwang, Woong-Ki;Kwon, Hyun-Wook;Kim, Tae-Hyung
    • Journal of the Korean Geotechnical Society
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    • v.34 no.8
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    • pp.5-14
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    • 2018
  • The grain size of clastic sedimentary rocks classifies the rock types and also causes of anisotropy of the rock. The anisotropy is one of the most important factors that dominates the strength and weathering behavior of rocks. The anisotropy of clastic sedimentary and igneous rocks in the Gyeongsang Basin including Yeongju, Daegu, and Busan were analyzed by magnetic susceptibility expressed by the degree of anisotropy and shape parameter. As the results of the study, the sandstone deposited under lacustrine environment unaffected by the external force shows 1.03 degree of anisotropy. The degrees of anisotropy of the rocks affected by faults and fault rocks show 1.06 and 1.14, respectively. The magnetic susceptibility of rocks is to decrease with the distance from the fault. A fresh mudstone and shale formed by fines show a similar magnitude of the degree of anisotropy to fault rock and correspond to oblate shape parameter due to their sedimentary structure. Due to these reasons, we need attention in design, construction, and maintenance of a structure constructed in mudstone and shale.

Evaluation Methods of Homogeneity for Feedstocks and Effect of Homogeneity on the Magnetic Properties of Plastic Magnets (플라스틱 자석 혼합물의 균질도 평가방법과 균질도가 자기특성에 미치는 영향)

  • 이석희;최준환;문탁진;정원용
    • Journal of the Korean Magnetics Society
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    • v.8 no.2
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    • pp.86-92
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    • 1998
  • Homegeneous feedstock is necessary to make plastic magents with uniform magnetic properties, therefore the optrimized mixing route and the homogeneity evaluation method are demanded. In this paper, method of homogeneity evaluation and effect of homogeneity on the magnetic prperites were investigated using Sr-ferrite /EVA plastic magnets. The feedstocks with different homogeneity were prepared using batch mixer and single screw extruder. The homogeneities of feedstocks were tested by torgue sensor, capilary rheometer, and measurement of magnetic properties. Mixing torque measurement using torque sensor was an effective method to determine the critical powder loading, but it was nor suitable to suitable to determine the feedstock mixing quality. Particle alignment measurement of a plastic magent was very accurate to evaluate the homogeneity, but expensive equipments were required to make and measure the samples. Pressure measurement using capillary rheometer was a very effective and easy method with high accuracy. Homogeneous feedstock increased the particle alignment of plastic magnet. Remanet flux density and maximum energy product increased linearly and quadratically with increasing particle alignment, respectively.

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Origin of Variation of the Initial Permeability of Manganese-Zinc Ferrite Polycrystals with Additives (Mn-Zn 페라이트 다결정의 첨가물에 따른 초투자율의 변화 기구)

  • Byeon, Sun-Cheon;Byeon, Tae-Yeong;Go, Gyeong-Hyeon;Hong, Guk-Seon
    • Korean Journal of Materials Research
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    • v.7 no.9
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    • pp.758-762
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    • 1997
  • 52mol% Fe$_{2}$O$_{3}$, 26mol% MnO의 조성에서 calcium과 vanadium의 동시첨가에 의한 투자율의 변화원인을 살펴보았다. 초투자율은 첨가물의 농도가 커짐에 따라 감사하였으나 소결체의 밀도나 입자크기는 증가하였으므로 초투자율의 변화는 미세구조의 변화로는 설명되지 않았다. 전기비저항은 첨가물의 농도가 증가함에 따라 증가하였으며 이는 입계의 고저항층의 생성과 vanadium ion에 의한 Fe$^{2+}$이온의 산화로 설명되었다. 첨가물의 농도가 증가함에 따라, 초투자율의 제 2차 최대치가 나타나지 않는 것과 초투자율이 감소하는 것으로부터, 결정자기이방성 상수의 값은 음으로 커짐을 알 수 있었다. 투자육의 온도의존성과 비저항의 변화로부터, 첨가물의 농도에 따른 상온 초투자율의 감소는 Fe$^{2+}$ 이온 농도의 감소에 따른 결정자기이방성 상수의 증가에 의한 효과와 입계에 유리질이 생겨 자벽이 쉽게 이동하지 못하는 효과 때문인 것으로 판단되었다.

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Magnetic properties and the shapes of magnetic domain for $CoCr_{16.2}Pt_{10.8}Ta_4$ alloy films with the prior deposition of Ti layer ($CoCr_{16.2}Pt_{10.8}Ta_4$ 합금박막의 Ti 우선증착에 따른 자기적 특성과 자구형상변화)

  • 이인선;김동원
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.10 no.1
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    • pp.17-22
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    • 2000
  • A quaternary alloy film of $CoCr_{16.2}Pt_{10.8}Ta_4$was investigated for its magnetic properties and c-axis orientation with and without Ti underlayer. Additional elements such as Ta, Pt have been frequently introduced in CoCr alloy film for perpendicular recording as a means of improving magnetic performance. It has been reported that the addition of Pt and Ta in CoCr increase the coercivity and the magnetic isolation of columnar grains, respectively. However, CoCrPtTa perpendicular magnetic layer should be more increased its perpendicular magnetic anisotropy than at present for the application of ultrahigh recording density. The improvement of underlayers and substrate materials is one of the promised schemes to intensify the perpendicular magnetic anisotropy. In this study, the insertion of Ti underlayer shows the remarkable improvement of c-axis orientation compare with the direct deposition on the bare glass. The mechanism about this effect of Ti underlayer on CoCrPtTa is not to be clarified yet. Meanwhile, it is found that the magnetic domain of CoCrPtTa on 20 nm Ti underlayer has the continuous stripe pattern but the one of CoCrPtTa on 90 nm Ti underlayer shows the discrete mass type from the results of MFM investigation. This phenomenon is to be a distinct evidence that the improvement of perpendicular anisotropy by the adoption of Ti underlayer is originated from the reinforcement of the grain boundary segregation in CoCrPtTa alloy. Moreover, the transition of the M-H hysteresis pattern with the thickness of Ti underlayer indicates that the major contribution of Ti underlayer is not the magnetocrystalline anisotropy but the shape anisotropy due to the formation of uniform columnar grains by the nonmagnetic alloy segregation.

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Structure and Magnetic Properties of $(Sm_{0.5}RE_{0.5})Fe_{11}Ti$ Compounds ($(Sm_{0.5}RE_{0.5})Fe_{11}Ti$ 화합물의 구조 및 자기특성)

  • 김희태;김윤배;김창석;김택기;권혁무
    • Journal of the Korean Magnetics Society
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    • v.3 no.3
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    • pp.196-200
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    • 1993
  • $(Sm_{0.5}RE_{0.5})Fe_{11}Ti$ compounds have tetragonal $ThMn_{12}$-type structure and show the uniaxial magnetocrystalline anisotropy with the easy magnetization c-axis. Among the $(Sm_{0.5}RE_{0.5})Fe_{11}Ti$ series, RE=Sm shows the highest anisotropy field of 11200 kA/m(140 kOe). On the other hand, RE=Nd has the highest saturation magnetization of $122.3\;Am^{2}/kg$(122.3 emu/g) and RE=Gd the highest Curie temperature of $326^{\circ}C$.

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A study on microstructures of Fe-Hf-N thin films (Fe-Hf-N 박막의 미세조직에 관한 연구)

  • 김중희;김정남;오승탁;강계명;현창용;최종운
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2003.03a
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    • pp.139-139
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    • 2003
  • 기록매체의 고밀도 대용량화를 위하여 자기헤드의 고성능화가 필요하다. 현재 고성능 자기헤드로는 bulk 형 페라이트 헤드, 헤드 갭(Gap)부의 연자성 특성이 우수한 MIG(Metal-in-Gap) 헤드, core부 자성금속을 적층시킨 적층 자기박막헤드 등이 있다. 이들 중 최근 MIG 헤드가 타 자기헤드에 비하여 연자성 특성이 우수하며, 박막의 조직특성에 따라 헤드의 성능이 크게 좌우되는 것으로 보고되고 있어, 이에 따라 특성 및 조직제어에 관한 연구가 진행되고 있다. 고포화 자속밀도의 자기헤드 갭은 자기모멘트가 큰 Fe원소를 기지원소로, 미량의 첨가원소에 기인하는 포화 자속밀도의 조절과 이에 따른 미세구조의 제어에 있는 것으로 연구되고 있다 즉 고포화 자속밀도를 가지는 연자성 박막의 미세구조를 제어함으로서 결정자기이방성이 최소화된 재료에 관한 박막화로 있다.

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