• Title/Summary/Keyword: 입자위치

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분무진공동결건조기 개발

  • Ryu, Gyeong-Ha;Ban, Byeong-Min;Kim, Jae-Hyeong;Son, Sang-Ho
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.02a
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    • pp.258-258
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    • 2013
  • 최근 건조 제품의 양질화, 고급화 및 편의화가 요구되어 이를 충족시키기 위한 새로운 건조방법이 계속 개발 되어 왔다. 이러한 방법들 중에서 저온과 진공하에서 건조가 이루어지는 진공 동결 건조는 가장 완벽한 건조 방법으로 최근 실용화 되고 있다. 진공동결건조란 건조의 한 종류로 수분을 함유한 시료를 동결시킨 후 진공펌프를 이용하여 수증기압을 3중점 이하로 낮추어 얼음을 직접 증기로 만드는 승화의 원리에 의해서 얻어진다. 분무진공동결건조의 특징은 (1) 물리적구조의 보존성, (2) 화학적인 안정성, (3) 생물학적인 활동의 보존성, (4) 제품의 높은 복원성 및 재생성이다. 따라서 분무진공동결건조 기술은 크게 진공, 분무, 동결, 건조, 멸균 등과 같은 요소기술의 복합기술이라 할 수 있다. 분말을 제조하기 위해서 진공동결건조 후 분쇄하는 방법을 사용하나 본 방법에서는 정밀화학품 제조를 위해서 분무진공동결건조 방식을 사용한다. 이를 통하여 적당한 크기인 5~10 um의 입경 제조가 가능하고, 공기동력학적인 입경이 기존 방식에 비해 작아서 허파까지의 운반효율이 1.5~2배 우수하다. 화학, 의학 분야에서의 분무동결 건조는 주로 민감한 제품, 즉 생물학적 고유성의 손상 없이 물을 제거하는데 사용되어 영구적으로 저장 가능한 상태로 보관할 수 있으며 물의 첨가로 원상태로 복구할 수 있어서 매우 각광을 받고 있다. 의약용 냉동건조 제품은 항생물질, 박테리아, 혈청, 백신, 검사 약물, 단백질을 포함하는 생물공학 제품들, 세포, 섬유, 화학제품 등이 있으며 주로 vial 또는 ampule 상태로 건조가 이루어진다.본 연구에서는 원료를 $-194^{\circ}C$의 액체질소에 분무시켜 동결된 미립자를 형성한 후 진공 및 저온상태에서얼음의 승화(sublimation)에 기반한 1차 건조와 수증기 탈착(desorption)에 기초한 2차 건조 과정으로 구성된 분무진공동결건조기를 개발하였다. 분무동결 과정의 해석을 통해 2유체식 노즐을 통해 분무된 미세 입경의 액적이 액체 질소 표면까지 도달하는 회수률, 분무 노즐의 위치, 운전 조건 및 용기의 설계의 최적화를 수행하였다. 초기 액적속도, 분무노즐의 높이, 흡입구 추가에 따른 액적 유동 및 회수의 특성을 제시하였으며 이를 통한 분사시스템 고도화 가능성을 제시하였다. 구형의 미세 입자가 적층된 제품의 동결건조 공정의 해석은 흡착승화 모델(sorption sublimation model)을 기반으로 다음과 같은 열전달, 물질전달, 상변화 모델을 고려하여 유도되었다. 분무노즐 및 냉동/진공 배기계 시작품을 개발하여, 표면의 고다공도를 갖춘 입경 3~20 m 정도의 시료를 얻을 수 있으며, 동역학적 입경 5 m 충족함을 확인하였다.

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Material Characteristics and Clay Source Interpretation of Crucibles in Baekje Kingdom Excavated from the Ssangbukri Site in Buyeo, Korea (부여 쌍북리 유적 출토 백제 도가니의 재료학적 특성과 원료의 산지해석)

  • Kim, Ji-Young;Park, Jin-Young;Park, Dae-Sun;Lee, Chan-Hee
    • Journal of Conservation Science
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    • v.26 no.1
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    • pp.1-12
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    • 2010
  • The crucibles of Baekje Kingdom from the Ssangbukri Site which were used for glass and metal melting had light brown, grayish blue and grayish brown colored bodies. In thin section, the crucibles contained numerous quartz grains and pottery fragments. The surface was covered with fine grained quartz for thermal resistance. Based on decomposition of mica group minerals and formation of mullite detected by X-ray diffraction analysis, it was inferred that all crucibles have been fired over $1,000^{\circ}C$. It was also found that firing temperature has exceeded $1,100^{\circ}C$ in some crucibles because feldspar was not detected. The maximum temperature was assumed at $1,200^{\circ}C$. The magnetic susceptibility values and geochemical characteristics sorted out the crucibles into two groups that differed from the characteristics of the local soils. This reflected geological setting of the site where the alluvium was formed from two kinds of surrounding rock masses, granite gneiss and biotite granite. However, the local soils had similarities with the crucibles in weathering degree and geochemical behavior of major elements. In consequence, it was considered that the raw clay of the crucibles was supplied from the local area of the site.

Development of Decompressed Dryer for Mushroom (버섯의 감압건조기 개발)

  • 김영민;김유호;조영길;최희석;조광환
    • Proceedings of the Korean Society for Agricultural Machinery Conference
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    • 2003.07a
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    • pp.267-272
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    • 2003
  • 본 연구에서는 버섯의 건조시간을 줄여 건조 후 버섯의 품질을 향상시키기 위하여 버섯의 감압건조기를 개발하였으며 연구 결과는 다음과 같다. 가. 버섯의 감압건조기의 시작기를 제작하였고, 시작기의 구조는 건조실, 감압블로워, 흡ㆍ배기구 솔레노이드 밸브, 제습장치, 송풍기, 전기히터로 구성되어 있으며, 건조실의 내부 압력이 표준대기압-900hPa, 열풍온도는 상온에서 5$0^{\circ}C$까지 조절할 수 있도록 제작하였다. 나. 시작기를 이용하여 표고버섯을 대상으로 건조특성시험을 실시한 결과, 열풍온도 5$0^{\circ}C$, 건조실 내부압력 900-940hPa에서 건조시간은 11.5h으로 대기압과 비교하여 6.5h 단축되는 것으로 나타났다. 또한, 건조 전ㆍ후의 색차, 수축률, 복원률의 품위가 우수한 것으로 나타났으며 F-test 유의성 검증 결과, 5%의 유의수준에서 갓주름의 색차, 갓직경의 수축률, 복원률에서 유의차가 있는 것으로 나타났다. 다. 열풍온도 5$0^{\circ}C$, 건조실 내부압력 900-940hPa로 표고버섯과 아가리쿠스에 대하여 건조성능시험을 실시한 결과, 표고버섯의 경우 건조시간은 13h으로 열풍식 농산물 건조기와 비교하여 건조시간이 4.5h 단축되는 것으로 나타났으며, 아가리쿠스의 경우 건조시간이 17.5h로 나타났다. 라. 성능시험 결과, 시작기가 열풍식 농산물건조기와 비교하여 건감률, 색택, 수축률, 복원률 등의 품위가 전반적으로 우수한 것으로 나타났다. 마. 시작기의 건조비용을 분석한 결과, 건조시간은 단축되었지만 시설투자비가 높아 건조비용이 표고버섯의 경우 2,461원/kg으로 열풍식 농산물건조기 보다 13% 높은 것으로 나타났지만, 추후 고품질 건조버섯 생산을 위한 기초자료로 활용이 가능할 것으로 판단된다.라갈수록 낮은 온도분포를 나타내고 있는 것은 상부에는 외부공기가 유입되면서 온도가 떨어지는 반면 하부에는 외부공기 유입이 적기 때문으로 사료된다. 또한 열풍실의 길이방향 위치별 온도 분포에서도 같은 현상으로 나타났고, 버너쪽과 송풍기쪽의 온도편차는 나타나지 않아 균일 건조를 기대할 수 있다. 마. 열풍온도를 45$^{\circ}C$로 설정하고 조사거리와 방사체 길이를 각각 119, 1,470mm로 하여 벼의 건조성능시험을 열풍건조기(대비구)와 비교시험 결과 시험구에서 건감률, 건조소요에너지가 각각 0.58%(w.b.), 470kcal/kg - water로 대비구보다 각각 건감율은 23% 높았고, 건조소요에너지는 2%의 절감되었다. 바. 건조기에서 발생되는 소음은 버너쪽 근처에서는 대비구 94.12㏈의 87%에 불과하였으나, 거리가 멀어질수록 차이는 크지 않았다. 이것은 버너에서 멀어질수록 외부적인 요인이 소음에 영향을 미쳤기 때문인 것으로 생각된다. 사. 시작기와 대비구간의 경제성에서 시작기의 구입가격이 20% 비싸기 때문에 시간당 고정비가 높았으나, 건조성능이 우수하여 건조비용이 69,350원/톤으로 대비구보다 14% 절감되는 것으로 나타났다.작용하는 것으로 사료된다.된다.정량 분석한 결과이다. 시편의 조성은 33.6 at% U, 66.4 at% O의 결과를 얻었다. 산화물 핵연료의 표면 관찰 및 정량 분석 시험시 시편 표면을 전도성 물질로 증착시키지 않고, Silver Paint 에 시편을 접착하는 방법으로도 만족한 시험 결과를 얻을 수 있었다.째, 회복기 중에 일어나는 입자들의 유입은 자기폭풍의 지속시간을 연장시키는 경향을 보이며 큰 자기폭풍일수록 현저했다. 주상에서 관측된 이러한 특성은 서브스톰 확장기 활동이 자기폭풍의 발달과 밀접한 관계가 있음을 시사한다.se that were all

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Ecological Studies on the Sand Dollar, Astriclypeus manni (Verril 1867) - Feeding, Density and Locomotion (구멍연잎성게, Astriclypeus manni(VERRIL 1867)의 먹이섭취, 서식밀도 및 이동속도에 관하여)

  • 강도형;최광식
    • Korean Journal of Environmental Biology
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    • v.20 no.2
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    • pp.180-188
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    • 2002
  • Sand dollar, Astriclypeus manni (Echinodermata: Echinoidea) is widely distributed on subtidal sand flats all along the coast of Cheju Island. Limited information has been reported on their ecology despite their abundance. This study reports gut contents, density and locomotion of the sand dollars distributed on a subtidal sand flat on the north-east coast of Cheju Island. Microscopic examination of the gut contents indicated that A. manni feeds on inorganic and organic detritus as well as live organisms contained in the sediments. Inorganic particles included sand grains, sponge spicules and shells of benthic animals such as foraminifera, crustacean and molluscs. Mean diameter of sediment particles retained in the gut was $77.6\pm{22.2}\mu{m}$. Live organisms retained in the gut included foraminifera, harpacticoid copepods, nematodes, diatoms and unidentified egg. Spatial distribution pattern of the sand dollar was found to be random with a mean density of 0.4 individual $m^{-2}(\chi^2=85.16,\;p>0.05)$. Locomotion speed of the sand dollar measured in situ was 2.0 to 65.0 cm $hr^{-1}$. Locomotion speed and moving distance was somewhat higher in summer when food availability also higher.

Engineering Geological Analysis of Landslides on Natural Slopes Induced by Rainfall - Yongin$\cdot$Ansung Area - (강우에 의해 발생된 자연사면 산사태의 지질공학적 분석 - 용인$\cdot$안성지역을 대상으로 -)

  • Kim Kyeong-Su;Kim Won-Young;Chae Byung-Gon;Song Young-Suk;Cho Yong-Chan
    • The Journal of Engineering Geology
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    • v.15 no.2 s.42
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    • pp.105-121
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    • 2005
  • Most of the landslides triggered by intensive rainfall on natural slope occur serious damages of human beings and properties. There have been many landslides since 1991 in Gyeonggi province. The influential factors are rainfall, topography, geology and soil properties. There were 660 landslides occurred by intensive rainfall as much as 250mm at Yongin and Anseong area from Tuly 19th to luly 21st,1991 This study surveyed location, topography, geology, geometry of the landslide and rainfall at the area and analyzed occurrence characteristics of the landslides. Most of the landslides occurred on the soil layer above the bed rock. They showed changes of landslide types from translational slides at the head part to flow at the central part. The landslides have relatively small magnitude of which length is shorter than 50m. In order to identify characteristics of landslides dependent on soil conditions, geotechnical properties of soil were evaluated by laboratory tests using soil samples which were collected on slided area and not-slided area. Soil properties of the slided area show high percentage of coarse material such as gravel and sand. However, soil of the not-slided area is mainly composed of fine material such as silt and clay. Permeability coefficients of the slided area are higher than those of the not-slided area.

Evaluation of Pollution Loads Removal Efficiency of Vegetation Buffer Strips Using a Distributed Watershed Model (분포형 유역모델을 이용한 식생여과대의 오염부하 저감효과 분석)

  • Park, Min-Hye;Cho, Hong-Lae;Koo, Bohn Kyoung
    • Journal of Environmental Impact Assessment
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    • v.25 no.6
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    • pp.369-383
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    • 2016
  • A distributed watershed model CAMEL(Chemicals, Agricultural Management and Erosion Losses) was applied to a part of grazing grassland and vegetation buffer strip(VBS) located in Daegwanryeong, Korea. A set of scenario analyses was carried out for grassland and VBS with various combinations of VBS widths, soil textures and ground surface slopes. The simulation results indicate that annual direct runoff decreases with wider VBS and the removal efficiency of pollutants generally decrease with steeper slopes. The removal efficiency of sediment is not significantly different with VBS widths. For gentle and medium slopes($10^{\circ}$, $20^{\circ}$), the removal efficiency of TOC and TN is not significantly different with VBS widths. As for a steep slope($30^{\circ}$), however, the removal efficiency of TOC and TN increases with narrower VBS. The removal efficiency of TP is generally high except for medium and steep slope of sandy loam where the removal efficiency of TP increases with wider VBS. This result of TP is contrary to the results of TOC and TN due to the adsorption characteristics of phosphorus associated with fine sediment particles. It is expected that CAMEL can be used for evaluating the effectiveness of VBS to reduce non-point source pollution discharges.

Distribution of $^{222}Rn$ Concentration in Seoul Subway Stations (서울지역 지하철역의 라돈농도 분포 특성)

  • Jeon, Jae-Sik;Kim, Dok-Chan
    • Journal of Korean Society of Environmental Engineers
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    • v.28 no.6
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    • pp.588-595
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    • 2006
  • Indoor radon($^{222}Rn$) concentrations of subway stations in Seoul area were measured to survey the environmental indoor radon levels and to identify sources of radon. The radon concentration of indoor air by method of long-term measuring with a-track detector were surveyed at 232 subway stations from 1998 to 2004. And the radon concentration in ground-water was measured with a method of alpha particle counting. To trace main source of radon, 8 out of 232 stations were selected and their radon concentrations in tunnel and on platform were analyzed. Total geometric mean and arithmetic mean of radon concentrations in all stations from 1998 to 2004 were $1.40{\pm}1.94pCi/L,\;1.65{\pm}1.07$ respectively. Geometric means of radon concentrations on platform and concourse were $1.54{\pm}1.96pCi/L,\;1.23{\pm}1.88pCi/L$ respectively, with higher concentration at the platform than at the concourse. The geological structure was significantly correlated to the indoor radon concentration in subway stations region. Radon concentrations of adjacent tunnel and ground-water of subway station was significantly correlated to the indoor radon concentration in subway stations. And There was a significant difference in radon concentration, depending on the depth levels in platform of subway stations(p<0.05).

Acoustic Characteristics of Sand Sediment with Circular Cylindrical Pores in Water (수중 원통형 다공성 모래퇴적물의 음향특성)

  • 윤석왕;이용주;노희설
    • The Journal of the Acoustical Society of Korea
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    • v.21 no.2
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    • pp.110-119
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    • 2002
  • Acoustic characteristics of water sediment were experimentally studied in laboratory. Water saturated sand sediment less than the grain size of 0.5 mm diameter is uniformly distributed in an acryl box (100 mm×100mm×42mm) with material thickness 1 mm. Pores in the acryl box are modeled as the structure of cylindrical pore tubes (diameter 3 mm and length 42 mm) filled with water. Cylindrical pore tubes have porosities 0%, 5%, 11%, 18% and 26 % controlled by the tube numbers. Transmitted acoustic waves through sand sediment specimen are analyzed as the functions of porosity and frequency from 0.3 MHz to 4 MHz. Transmitted acoustic waves are mixed with the first-kind wave from whole specimen and the second-kind wane from cylindrical pore tubes. For the center frequency 1 MHz, the first kind wave is dominant but for the center frequency 2.25 MHz, the second kind wave is dominant. In the case of the first-kind wave, as the porosity increases, the transmission coefficient decreases and the sound speed decreases to the sound speed of water. As the frequency increases, the transmission coefficient decreases but the sound speed is almost constant. In the case of the second-kind wave, as the porosity increases, the transmission coefficient increases but the sound speed is almost constant. The transmission coefficient and the sound speed are almost constant as a function of frequency.

THE RELATIVE CONTRIBUTIONS OF ELECTRIC FIELD AND IONOSPHERIC CONDUCTANCE TO THE AURORAL ELECTROJETS (오로라 제트전류에 대한 전기장과 전기전도도의 상대적 기여도)

  • 조은아;안병호;문용재
    • Journal of Astronomy and Space Sciences
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    • v.17 no.1
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    • pp.87-98
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    • 2000
  • We examine the relative contributions of the electric field and ionospheric conductance to the auroral electrojets. For this purpose we used magnetometer data obtained from the International Magnetospheric Study (IMS) meridian chains of observatories for March 17, 18, and 19, 1978. Based on the study by Allen & Kroehl (1975), we redefine the AU and AL indices by utilizing the magnetic disturbance data obtained from the AE stations located within limited magnetic local time (MLT) sectors; i.e., $1500\leq MLT\leq1800$ and$0000\leq MLT\leq0300$, respectively. The current densities of the eastward and westward electrojets are calculated based on the AU and AL indices thus defined. Under the assumption that the Hall conductance at the dusk sector is mainly caused by the solar EUV radiation, we estimate the electric field contributin to the AU index. Assuming further that electric field distributins at dawn and dusk sectors are comparable, it is also possible to estimate the contribution of the Hall conductance associated at the dusk sector is mainly caused by the solar EUV radiation, we estimate the electric field contribution to the AU index. Assuming further that electric field distributions at dawn and dusk sectors are comparable, it is also possible to estimate the contribution of the Hall conductance associated with auroral particle precipitation to the AL index. From this study it is noted that the electric fields and Hall conductances thus estimated show significant correlations with the AU and AL indices, respectively, suggesting that the AU and AL indices are closely associated with the directly driven and loading-unloading processes of substorms.

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Characteristics of Precipitates and Geochemistry of Mine and Leachate Water in Janggun Mine (장군광산 갱내수와 침출수의 지화학적 및 침전물의 특성 연구)

  • Kim, Jun Yeong;Jang, Yun Deug;Kim, Yeong Hun;Kim, Jeong Jin
    • Journal of the Mineralogical Society of Korea
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    • v.27 no.3
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    • pp.125-134
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    • 2014
  • The Janggun mine (Longitude $E129^{\circ}$ 03' 40", Latitude $N36^{\circ}$ 51' 19") was once operated as an underground mine and recently significant amount of mine and leachate water has been discharged from the mine adits and tailing dumps. Mine and leachate waters are characterized by neutral to weakly basic pH values (6.81-9.59). Major cations and anions have concentrations between 6.70-129.80 mg/L of Mg, 289.29-661.02 mg/L of Ca, 4.74-14.38 mg/L of Mn and 1205.00-2448.69 mg/L of $SO{_4}^{2-}$. Brownish yellow precipitates that found in the stream bottom consist of poorly crystallized 2-line ferrihydrite ($Fe_2O_3{\cdot}0.5H_2O$. Scanning electron microscope (SEM) photographs show that brownish yellow precipitates consisted of micro-sized granular particles of about $0.1{\mu}m$ in diameter. Semi-quantitative energy dispersive spectrometry (EDS) analyses show that these samples contained mainly Fe with minor Mn, Ca, Si and As.