• Proceedings of the Korean Society of Precision Engineering Conference
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• 2004.05a
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• pp.158-158
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• 2004

본 연구에서는 이부프로펜(Ibuprofen)분말을 마이크론(Micron) 크기의 입자로 만들기 위하여 극저온 볼 밀링 공정(Cryogenic Ball Milling Process)을 사용하였다. 극저온 볼 밀링 공정은 약 -18$0^{\circ}C$의 질소 분위기에서 6시간 동안 실행되어 졌다 이부프로펜 분말 형상의 변화는 SEM(Scanning Electronic Microscope)촬영을 통하여 관찰하였으며, 분말의 입자 크기와 분포는 입도 분석기(Particle Size Analysis)를 사용하여 극저온 볼 밀링 공정 전ㆍ후의 변화를 관찰하였다(중략)

• Proceedings of the Korea Water Resources Association Conference
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• 2021.06a
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• pp.259-259
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• 2021

하상을 구성하는 사립자들이 흐름에 의해 움직이기 시작하는 상태를 한계운동이라 하며, 한계운동이 시작될 때의 흐름조건을 한계조건이라 한다. 흐름에 부유되어 이동하는 부유사의 농도분포를 정확하게 산정하기 위해서는 하상재료의 침식율을 정확하게 산정하는 것이 필요하다. 특히 하상재료에 다양한 크기의 하상재료가 혼합되어 있을 때에는 차폐효과(Hiding-Exposure Effect)에 대한 고려가 필요하다. 여기서 차폐효과란, 동일한 크기의 사립자들로 구성된 균질 하상에 비해 비균질 하상에서 굵은 사립자가 흐름에 더 많이 노출되어 한계소류력이 감소하고, 잔 사립자의 한계소류력이 굵은 사립자로 인해 증가하는 현상을 의미한다. 하상토의 차폐효과는 Shields (1936)에서 제안된 무차원 한계소류력을 각 사립자의 크기별로 산정 한 후 보정계수를 곱해 고려해주는 것이 일반적이다. 이에 본 연구에서는 하상재료의 차폐효과가 부유사의 연직방향 농도분포에 미치는 영향을 살펴보았다. 연구를 수행하기 위해 하상토의 입도분포를 바탕으로 차폐효과를 고려하고 연직방향으로의 유사농도를 계산하는 유사이동모형을 개발하였다. 수치모형의 검증은 실험실 실험자료와의 비교를 통해 수행되었다. 수치모의 결과로부터 차폐효과를 고려하지 않는 경우에는 하상에서의 침식율이 과다하게 산정되는 것으로 나타났으며, 불균질한 하상재료로 구성된 하천에서 부유사의 연직방향 유사농도를 정확하게 계산하기 위해서는 차폐효과에 대한 고려가 필요하다는 결론이 도출되었다.

• Korean Journal of Materials Research
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• v.7 no.12
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• pp.1027-1032
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• 1997

본 연구에서는 용사용WC-17%Co 복합분말을 분무건조법으로 제조하고 열처리 온도(85$0^{\circ}C$, 100$0^{\circ}C$, 115$0^{\circ}C$, 130$0^{\circ}C$)에 따른 조립분말의 미세구조, 입도분포, 유동도, 및 결정상변화를 고찰하였다. 분무건조상태의 입형은 구형이었으며, 입도분포, 평균입자크기, 유동성은 각각 20.6-51.7$\mu\textrm{m}$, 27.2$\mu\textrm{m}$, 0.26 sec/g 이었다. 열처리에 의하여 조립분말은 치밀화되어 130$0^{\circ}C$ 열처리 후에는 입도분포와 평균입자크기가 각 각 6.9-37.9$\mu\textrm{m}$과 17.8$\mu\textrm{m}$로 감소하였으며, 유동성은 0.12 sec/g로 향상되었다. 열처리중에 WC와 Co의 상화확산에 의하여 Co$_{6}$W$_{6}$C및 Co$_{3}$W$_{3}$C이 생성되었으며, 두 상이 나타나는 임계온도는 115$0^{\circ}C$이었다.

• Polymer(Korea)
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• v.26 no.3
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• pp.307-315
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• 2002

Major factors affecting the impact resistance of high impact polystyrene (HIPS), the rubber-toughened grade of polystyrene, are rubber-phase particle size and size distribution, molecular weight, morphology, and degree of grafting. Accordingly, it is important to control or investigate these factors. In this study, the effect of solvent content was analyzed by the morphology and particle size distribution of rubber phase, and final properties in bulk-solution polymerization of HIPS. The prepolymerization time was, first, determined by measuring the evolution of particle size distribution of dispersed phase to explain the phase inversion with time. As the solvent content increased, the size of rubber particle increased and then gradually decreased. Rubber-phase morphology was likely to have higher degree of grafting as the solvent content increased. Rheological and mechanical properties decreased as the solvent content increased because of the decrease of matrix molecular weight due to the chain transfer reaction to solvent and the existence of residual solvent. Nevertheless, the impact resistance seemed to increase when the rubber particle size increased.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.18 no.7
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• pp.714-719
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• 2017

The controlled synthesis of inorganic materials with a specific size and morphology is an important factor in the development of new materials in many fields, such as nanoparticles, medicine, electronics, semiconductors, pharmaceutical sand cosmetics. Solution crystallization is one of the most widely used separation processes in the chemical and pharmaceutical industries. Calcium carbonate has attracted a great deal of attention in industry because of its numerous applications. The mean crystal size, crystal size distribution and morphology are important factors in the continuous crystallization process. In this study, the continuous crystallization of calcium carbonate by the calcium chloride process was investigated. The mean crystal size and crystal size distribution data were obtained by a particle size analyzer. The morphological imaging of the crystalswasper formed by SEM. Under steady state operation, the mean crystal size change was small, but increasing the input concentration and mixing rate increased the crystal size. In this operation, some aragonite was found, but the main crystal phase was calcite.

• Proceedings of the Korea Society for Simulation Conference
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• 1996.05a
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• pp.10-14
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• 1996

본 논문은 토러스 망의 패킷 전송 효율을 평가하기 위해 각 노드가 에지당 2개의 입·출력 큐를 가지는 라우팅 알고리즘을 제시하고 시뮬레이션을 수행하여 그 결과를 분석하였다. 제시된 4가지 오름순차를 가지는 라우팅 알고리즘에 대해 시뮬레이션을 하기 위해 도착분포와 서비스분포는 지수분포를 갖도록하여 교착상태가 없는 패킷 전송 효율을 비교 평가하였다. 실험 결과로부터 무교착 상태로 패킷을 전달하기 위한 노드 큐의 크기를 알 수 있었고, 또한 입력 패킷 메시지의 분포에 따라 패킷의 전송 효율을 높이기 위한 버퍼의 크기를 예측할 수 있었다.

• Journal of the Korean GEO-environmental Society
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• v.21 no.11
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• pp.21-26
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• 2020

Natural soil is composed of particles of various sizes, and the shear behavior which is a kind of mechanical behavior of the soil is affected by the particle size distribution. In addition, since the natural soil contains a large mixture of coarse and fine grained soil, it is difficult to clearly understand the shear behavior of the soil. Therefore, a ring shear test was conducted on sandy soils that has various particle size distribution in order to identify the effect of the distribution on shear characteristics of soils. At this time, sand and silt were used for coarse and fine grained soils, respectively, to make sandy soils by changing the silt content. Also the water was supplied during the test to confirm shear characteristics of sandy soils with various particle size distributions. The result shows that the shear strength increases as the silt content increases, and the strength decreases as the silt content increases over the sand. Besides, residual shear strength gradually decreases because of the silt content when the water is supplied.

• Korean Journal of Materials Research
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• v.6 no.4
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• pp.357-363
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• 1996

다공성 알루미나 지지체를 이용하여 졸에 침지하는 미세한 기공으로 이루어진 티타니아 여과막을 제조하였다. 티타니아 졸은 현\ulcorner액 재안정화 공정으로 제조하였고, pH 1.23-1.32범위에서 졸의 평균입지크기는 15nm 이하였다. 이 여과막은 $600^{\circ}C$에서 1시간 열처리한 경우 평균입도는 30-40nm로서 입도 분포가 좁은 양호한 여과막을 제조하였다. 이때 입자의 모양은 구형이었다. 열처리 온도가 $600^{\circ}C$보다 높아지면 여과막을 구성하는 입자 모양을 다각형으로 변하고 입도의 분포는 넓어졌다.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.18 no.1
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• pp.715-723
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• 2017

This study investigates the properties of a high-performance cementitious composite with partial substitution of stone dust for fine aggregate. The relationship between the properties and particle size distribution was analyzed using several analytical models. Experiments were carried out to examine the flowability, rheology, and strength of cement mortars with different stone-dust replacement ratios of 0-30 wt.%. The results showed improved flowability, lower rheological parameters (yield stress and plastic viscosity), and improved strength as the amount of stone dust increased. These results are closely related to the packing density of the solid particles in the mortar. The effect was therefore estimated by introducing an optimum particle size distribution (PSD) model for maximum packing density. The PSD with a higher amount of stone dust was closer to the optimum PSD, and the optimization was quantified using RMSE. The improvement in the PSD by the stone dust was proven to affect the flowability, strength, and plastic viscosity based on several relevant analytical models. The reduction in yield stress is related to the increase of the average particle diameter when using stone dust.

• Journal of the Korean Society of Food Science and Nutrition
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• v.40 no.5
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• pp.725-730
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• 2011

This study evaluated the quality characteristic of red pepper powders of Hanbando and Cheongyang cultivars by particle size. Two types of powder samples for pepper paste and Kimchi were prepared, and capsaicinoid contents, Hunter Lab color values, and ASTA values by particle size distribution were investigated. Particle size distribution was normal in the pepper paste powder; however, an abnormal distribution was shown for the Kimchi powder. In addition, the greatest particle sizes were $300{\sim}425\;{\mu}m$ in the pepper paste powder. In accordance with smaller particle size, redness (a-value), ASTA values, and capsaicinoid contents increased. Redness (a-value) by particle size was in the range of 15.13~31.34, and ASTA values were in the range of 53.35~96.87. Capsaicinoid contents by particle size were in the range of 1.90~6.05 mg/100 g for Hanbando and 156.65~235.10 mg/100 g for Cheongyang.