• Title/Summary/Keyword: 입계

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Fabrication and Properties of $(Pb_{1-x}C_{ax})((Co_{\frac{1}{2}}W_{\frac{1}{2}})_yTi_{1-y})O_3+(MnO_2, NiO)$ piezoelectric ceramic (압전세라믹 $(Pb_{1-x}C_{ax})((Co_{\frac{1}{2}}W_{\frac{1}{2}})_yTi_{1-y})O_3+(MnO_2, NiO)$)

  • Mun, Dong-Jin;Do, Si-Hong;Jang, Ji-Won
    • The Journal of the Acoustical Society of Korea
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    • v.6 no.4
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    • pp.55-63
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    • 1987
  • Modified $PbTiO_3$ piezoelectric ceramics added with 0.2, 0.25, 0.3 mol of $CaCO_3$ and 0.04 mol of $(Co_{\frac{1}{2}}W_{\frac{1}{2}})$ and 0.05 mol of $MnO_2$ and NiO have been fabricated. These ceramics can be poled sufficiently within 10 minutes at $100^{\circ}C$ under about d.c. field of 40 kv/cm. Detailed measurement was performed on dielectric constants, cutie temperatures, elastic and piezoelectric properties and coupling factors for the fabricated ceramics. The most value of the piezoelectric coupling factors was coupling factor of thickness mode kt and its value for 0.25 mol of Ca was about $45\%$. Dielectric constants of $\varepsilon_{33}^T$ and $\varepsilon_{11}^T$ for 0.25 mol of Ca were 242 and 260, and coupling factor ratio (kt/Kp) and Qm were 6 and 357 respectively.

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Calculation Model of Time Varying Loudness by Using the Critical-banded Filters (임계 대역 필터를 이용한 과도음의 라우드니스 계산 모델)

  • Jeong, Hyuk;Ih, Jeong-Guon
    • The Journal of the Acoustical Society of Korea
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    • v.19 no.5
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    • pp.65-70
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    • 2000
  • It is blown that the loudness is one of the most important metrics in assessing the sound quality and a calculation method for loudness has been standardized for steady sounds. In this study, a new loudness model is suggested for dealing with the transient sound for a unified analysis of various practical sounds. A signal processing technique is introduced for this purpose, which is required for the band subdivision and the prediction of band-level change of transient sounds. In addition, models for the post-masking and the temporal integration are adopted in the analysis of the loudness of transient sounds. In order to solve the problem of the conventional loudness model in the pure-tone signal processing, a critical band filter is employed in the analysis, which consists of 47 critical filters having a filter spacing of a half of the critical bandwidth. For testing the effectiveness of the present model, the predicted responses are compared with the experimental data and it is observed that they are in good agreements.

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Magnetic Properties of Magnetic Core Materials for PLC as a Funtion to Additives (PLC용 자심재료의 협가제에 따른 자기적 특성의 변화)

  • An, Yong-Woon;Kim, Jong-Ryung;Oh, Young-Woo
    • Journal of the Korean Magnetics Society
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    • v.13 no.6
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    • pp.246-250
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    • 2003
  • The electromagnetic properties of Ni$\_$0.8/Zn$\_$0.2/Fe$_2$O$_4$ having stable characteristics in high frequency range were investigated as functions of Bi$_2$O$_3$, CaO contents. Power loss increased in proportion to the amount of Bi$_2$O$_3$ up to 0.3 wt% and decreased over 0.3 wt%. Also, permeability increased with Bi$_2$O$_3$ contents. The lowest power loss and highest resonance frequency were obtained to the specimens added Bi$_2$O$_3$ of 0.7wt% and CaO of 0.3 wt% due to creation of resistivity layers in the grain boundaries originated by the solid solution of Bi$_2$O$_3$ and CaO.

Effect of Cu/Al powder mixing on Dy diffusion in Nd-Fe-B sintered magnets treated with a grain boundary diffusion process (입계확산처리된 Nd-Fe-B 소결자석에서 Dy의 확산에 미치는 Cu와 Al 분말의 혼합 효과)

  • Lee, Min Woo;Jang, Tae Suk
    • Journal of Powder Materials
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    • v.23 no.6
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    • pp.432-436
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    • 2016
  • We investigate the microstructural and magnetic property changes of $DyH_2$, $Cu+DyH_2$, and $Al+DyH_2$ diffusion-treated NdFeB sintered magnets with the post annealing (PA) temperature. The coercivity of all the diffusion-treated magnets increases with increasing heat treatment temperature except at $910^{\circ}C$, where it decreases slightly. Moreover, at $880^{\circ}C$, the coercivity increases by 3.8 kOe in Cu and 4.7 kOe in Al-mixed $DyH_2$-coated magnets, whereas this increase is relatively low (3.0 kOe) in the magnet coated with only $DyH_2$. Both Cu and Al have an almost similar effect on the coercivity improvement, particularly over the heat treatment temperature range of $790-880^{\circ}C$. The diffusivity and diffusion depth of Dy increases in those magnets that are treated with Cu or Al-mixed $DyH_2$, mainly because of the comparatively easy diffusion path provided by Cu and Al owing to their solubility in the Nd-rich grain boundary phase. The formation of a highly anisotropic $(Nd,\;Dy)_2Fe_{14}B$ phase layer, which acts as the shell in the core-shell-type structure so as to prevent the reverse domain movement, is the cause of enhanced coercivity of diffusion-treated Nd-Fe-B magnets.

Synthesis of DyF3 paste and Magnetic Properties of GBDPed Nd-Fe-B Magnets (DyF3 paste 제조 및 이를 이용한 Nd-Fe-B 입계확산 자석의 특성 연구)

  • Jeon, Kwang-Won;Cha, Hee-Ryoung;Lee, Jung-Goo
    • Journal of Powder Materials
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    • v.23 no.6
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    • pp.437-441
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    • 2016
  • Recently, the grain boundary diffusion process (GBDP), involving heavy rare-earth elements such as Dy and Tb, has been widely used to enhance the coercivity of Nd-Fe-B permanent magnets. For example, a Dy compound is coated onto the surface of Nd-Fe-B sintered magnets, and then the magnets are heat treated. Subsequently, Dy diffuses into the grain boundaries of Nd-Fe-B magnets, forming Dy-Fe-B or Nd-Dy-Fe-B. The dip-coating process is also used widely instead of the GBDP. However, it is quite hard to control the thickness uniformity using dip coating. In this study, first, a $DyF_3$ paste is fabricated using $DyF_3$ powder. Subsequently, the fabricated $DyF_3$ paste is homogeneously coated onto the surface of a Nd-Fe-B sintered magnet. The magnet is then subjected to GBDP to enhance its coercivity. The weight ratio of binder and $DyF_3$ powder is controlled, and we find that the coercivity enhances with decreasing binder content. In addition, the maximum coercivity is obtained with the paste containing 70 wt% of $DyF_3$ powder.

Analysis of SCC Behavior of Alloy 600 Nozzle Penetration According to Residual Stress Induced by Dissimilar Metal Welding (Alloy 600 노즐관통부의 이종금속용접 잔류응력에 따른 응력부식균열 거동 분석)

  • Kim, Sung-Woo;Kim, Hong-Pyo;Kim, Dong-Jin;Jeong, Jae-Uk;Chang, Yoon-Suk
    • Transactions of the Korean Society of Pressure Vessels and Piping
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    • v.6 no.2
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    • pp.34-41
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    • 2010
  • This work is concerned with the analysis of stress corrosion cracking(SCC) behavior of Alloy 600 nozzle penetration mock-up according to a residual stress induced by a dissimilar metal welding(DMW) in a nuclear reactor pressure vessel. The effects of the dimension and materials of the nozzle penetration on the deformation and the residual stress induced by DMW were investigated using a finite element analysis(FEA). The inner diameter(ID) change of the nozzle by DMW and its dependance on the design variables, calculated by FEA, were well consistent with those measured from the mock-up. Accelerated SCC tests were performed for three mock-ups with different wall thicknesses in a highly acidic solution to investigate mainly the effect of the residual stress on the SCC behavior of Alloy 600 nozzle. From a destructive examination of the mock-up after the tests, the SCC behavior of the nozzle was fairly related with the residual stress induced by DMW : axial cracks were found in the ID surface of the nozzle within the J-weld region where the highest tensile hoop stress was predicted by FEA, while circumferential cracks were observed beyond both J-weld root and toe where the highest tensile axial stress was expected.

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The High-Speed Extraction of Interest Region in the Parcel Image of Large Size (대용량 소포영상에서 관심영역 고속추출 방법에 관한 연구)

  • Park, Moon-Sung;Bak, Sang-Eun;Kim, In-Soo;Kim, Hye-Kyu;Jung, Hoe-Kyung
    • The KIPS Transactions:PartD
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    • v.11D no.3
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    • pp.691-702
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    • 2004
  • In this paper, we propose a sequence of method which extrats ROIs(Region of Interests) rapidly from the parcel image of large size. In the proposed method, original image is spilt into the small masks, and the meaningful masks, the ROIs, are extracted by two criterions sequentially The first criterion is difference of pixel value between Inner points, and the second is deviation of it. After processing, some informational ROIs-the areas of bar code, characters, label and the outline of object-are acquired. Using diagonal axis of each ROI and the feature of various 2D bar code, the area of 2D bar code can be extracted from the ROIs. From an experiment using above methods, various ROIs are extracted less than 200msec from large-size parcel image, and 2D bar code region is selected by the accuracy of 100%.

탄소와 질소 함량 변화에 따른 type 347 스테인리스강의 피로균열거동 연구

  • Min, Gi-Deuk;Kim, Dae-Hwan;Lee, Bong-Sang;Kim, Seon-Jin
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2009.05a
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    • pp.42.1-42.1
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    • 2009
  • 오스테나이트 스테인리스강은 우수한 내식성 및 기계적 특성으로 인해 구조용 재료로 널리 사용되고 있다. 표준원전 경수로의 경우 가압기 밀림관소재로 Nb 안정화 오스테나이트 스테인리스강인 type 347 스테인리스강이 사용되고 있다. 그러나 원전배관에서는 운전중 배관내 온도편차에 의한 열응역과 하중변화에 의한 기계적하중에 의해 피로손상을 받는다. 일반적으로 범용 오스테나이트 스테인리스강(AISI 304, 316)의 피로균열 성장거동에 대한 연구결과는 국내외적으로 다수 축적되어 있으나 type 347 탄소, 질소 함량에 따른 기계적 특성 및 피로균열성장 연구는 매우 미비하다. 따라서 본 연구에서는 탄소와 질소의 함량에 따른 기계적거동을 평가하고, 이에 따른 피로균열전파속도를 관찰하여 스테인리스강의 정확한 피로균열전파속도 곡선을 제시하고자 한다. 실험에 사용된 시편은 두께 5mm, 폭 25.4mm CT시편을 사용하였으며, 1mm의 예비균열을 주었다. 그리고 실험온도는 상온과 원전가동온도인 $316^{\circ}C$에서 실시하였으며, 주파수는 10Hz를 주었다. 실험결과 각 함량에 따른 type 347의 미세조직 관찰결과 기지내에 압연방향을 따라 조대한 석출물의 흐름이 관찰되었으며, 크기나 분포가 큰 차이를 보였다. C+N 함량이 낮은 시편은 주로 $0.1\;{\mu}m$ 이하의 미세한 입자들이 오스테나이트 기지조직의 입내와 입계에 고르게 분포되어 있었다. 그러나 C+N 함량이 높은 시편의 경우에는 $0.1\;{\mu}m$ 이하의 미세한 입자들과 함께 국부적으로 $1\sim10\;{\mu}m$의 조대한 입자들이 분포하고 있는 것이 관찰되었다. 그리고 질소의 함량이 높아짐에 따라 인장강도는 증가하였으며, 피로시험결과 고온에서 실험한 피로균열성장률 곡선이 상온보다 높게 나타남을 확인할 수 있었다. 그리고 질소가 적게 첨가되고 탄소의 함량이 많을수록 피로균열성장률은 ASME 곡선보다 낮게 나타났다.

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Effect of Ti Concentration on the Microstructure of Al and the Tunnel Magnetoresistance Behaviors of the Magnetic Tunnel Junction with a Ti-alloyed Al-oxide Barrier (Ti 첨가에 따른 Al 미세구조 변화 효과와 산화 TiAl 절연층을 갖는 자기터널접합의 자기저항 특성)

  • Song, Jin-Oh;Lee, Seong-Rae
    • Journal of the Korean Magnetics Society
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    • v.15 no.6
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    • pp.311-314
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    • 2005
  • We investigated the composition dependence of the tunneling magnetoresistance (TMR) behavior and the stability of the magnetic tunnel junctions (MTJs) with TiAlOx barrier and the microstructural evolution of TiAl alloy films. The TMR ratio increased up to $49\%$ at $5.33\;at\%$ Ti. In addition, a significant tunneling magnetoresistance (TMR) value of $20\%$ was maintained after annealing at $450^{\circ}C$, and the breakdown voltage ($V_B$) of and 1.35 V were obtained in the MTJ with $5.33\;at\%$ Ti-alloyed AlOx barrier. These results were closely related to the enhanced quality of the barrier material microstructure in the pre-oxidation state. Ti alloying enhanced the barrier/electrode interface uniformity and reduced microstructural defects. These structural improvements enhanced not only the TMR effect but also the thermal and electrical stability of the MTJs.

The Effect of Sintering Time in the Microstructure and Electric Conductivity of $(Gd_2O_3)_{0.05}(Y_2O_3)_{0.05}(ZrO_2)_{0.9}$ System ($(Gd_2O_3)_{0.05}(Y_2O_3)_{0.05}(ZrO_2)_{0.9}$계의 소결시간에 따른 미세구조와 전기전도도)

  • 임용무;장복기;신동선;김동근;김종빈;윤성도
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.11 no.12
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    • pp.1099-1107
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    • 1998
  • In this study, the microstructure and electric conductivity of 5mol% $Gd_2O_3$-5mol% $Y_2O_3-ZrO_2$ system(5G5YZ) with a variation of sintering time at $1600^{\circ}C$ were investigated. By the result of TEM analysis of 5G5YZ sintered for 12h, a microcrack was observed near grain boundary. The change of the sintering time did not affect the lattice conductivity, but the grain boundary contribution was varied with the sintering time. The grain boundary conductivity of the sample sintered for 1h showed the highest value. Furthermore, the activation energy of the total conductivity was independent upon the sintering time and showed approximately 1.01eV. The highest conductivity measured at $1000^{\circ}C$ was 0.0197S/cm with the sample sintered for 1h. Comparing to 0h’s, the thickness ration of grain boundary as a function of sintering time were 0.88, 1.11 and 1.29 for 1h, 5h and 12h, respectively. In case of the sample sintered for 1h, the thickness of the grain boundary showed the lowest value. The increase of the sintering time over 1h made the decrease of the electric conductivity as well as the increase of the grain growth and the thickness of the grain boundary. As a result, it seemed that the proper sintering time for 5G5YZ composition was 1h.

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