• Title/Summary/Keyword: 오토클레이브

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Synthesis and $CO_2$ Separation Characteristics of ZSM-5 Zeolite Composite Membranes (ZSM-5 제올라이트 복합분리막의 제조 및 $CO_2$ 분리 특성)

  • 현상훈;송재권;김준학
    • Proceedings of the Membrane Society of Korea Conference
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    • 1997.04b
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    • pp.29-29
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    • 1997
  • ZSM-5계 제올라이트는 직경이 약 6${\AA}$인 균일한 3차원 채널 형태의 기공을 형성하므로 이를 이용한 기체 분리막은 분자체가름(molecular sieving)이나 미세기공확산(micropore diffusion) 및 표면확산(surface diffusion) 메커니즘에 의해 최근 지구 온난화의 주범으로 지목되고 있는 CO$_2$ 기체에 대해 높은 분리 효율을 기대할 수 있으므로 ZSM-5 복합분리막의 제조 및 기체 투과 특성과 CO$_2$ 분리 특성에 대해 연구하였으며 다음과 같은 결과를 얻을 수 있었다. 콜로이달 실리카 졸에 질산 알루미늄, 수산화 나트륨 및 TPABr을 첨가한 혼합졸과 물유리를 증류수로 희석한 후 TPBr을 첨가한 용액을 각각 150~180${\AA}$의 온도 범위의 오토클레이브에서 수열 처리하여 ZSM-5와 실리카라이트를 합성하였다. 합성 제올라이트의 결정 구조는 사방정이었으나 450${\AA}$에서 하소하였을 때에는 단사정으로 전이됨과 동시에 채널 속을 채우고 있던 TPABr이 제거되면서 제올라이트의 3차원 채널 형태의 기공 구조가 생성되었다. 제올라이트 결정의 형상과 크기는 실리카 공급원과 반응용액/졸의 농도에 따라 매우 민감하게 변화되었다. 하소 제올라이트의 비표면적은 약 360 m$^2$/g 이었다. 합성 제올라이트의 표면은 소수성인 반면에 높은 CO$_2$ 흡착능을 갖고 있어서 CO$_2$ 분리용 막의 재료로써 적합하였다.

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A Study on the Reliability of Cooling Water Systems Using R436B (대체냉매 R436B를 적용한 정수기 냉각수 시스템 신뢰성 평가에 관한 연구)

  • Nam, Hyun-Kyu;Bai, Sangeun;Bai, Cheol-Ho;Ko, Jung-Su;Jin, Byung-Joo;Oh, Ju-Chul
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.25 no.8
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    • pp.438-442
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    • 2013
  • The alternative refrigerant R436B is applied, to assess the application feasibility for a commercial cooling water system. The characteristic stability was verified by Sealed glass tube test and Autoclave test. R436B is chemically stable with the compressor material. The Oil miscibility test shows the usual compressor oil mixed well with R436B. Through the life acceleration test, the cooling performance is maintained. Though slight changes in oil and capillary tube diameter were found, they were within the permitted range. R436B should be applied to commercial cooling water systems as a simple replacement for the usual refrigerant.

Thermal Deformation of Carbon Fiber Reinforced Composite by Cure Shrinkage (탄소섬유강화 복합재료 성형시 화학수축에 의한 변형연구)

  • Choi, Eun-Seong;Kim, Wie-Dae
    • Composites Research
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    • v.31 no.6
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    • pp.404-411
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    • 2018
  • As the autoclave process progresses in a given cure cycle, residual stress in the composite product is induced by cure shrinkage of the resin. As a result, It generates the thermal deformation such as spring-in and warpage, and the inaccuracy of the final product increases. It is important to predict thermal deformation in aerospace parts which require precise fabrication. The research has been done on predicting and grasping curing process of composite material. In this study, the cure mechanism of composite materials according to the process is predicted through finite element analysis, and the effect of cure shrinkage on thermal deformation generated by the process is analyzed.

A Study on the Development of Integrated Folding Composite Wing Using Optimal Design and Multiple Processes (최적설계 및 다중공정을 적용한 일체형 접이식 복합재료 날개 개발 연구)

  • Lee, Jong-Cheon
    • Journal of Aerospace System Engineering
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    • v.12 no.3
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    • pp.70-78
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    • 2018
  • This research was carried out to develop an integrated folding wing made from carbon composite materials. Design requirements were reviewed and composite wing sizing was conducted using design optimization with commercial software. Three composite manufacturing processes including hot-press, pultrusion, and autoclave were evaluated and the most suitable processes for the integrated wing fabrication were selected, with consideration given to performance and cost. The determined manufacturing process was verified by two design development tests for selecting the design concept. Stiffness and strength of the composite wing were estimated through structural analyses. The test loads were calculated and static tests about design limit load and design ultimate load were performed using both wings. As a result, the evaluation criterions of the tests were satisfied and structural safety was verified through the series of structural analyses and testing.

Study on Mechanical Properties of CFRP Composite Orthogonal Grid Structure (CFRP 복합재료 직교 격자 구조의 기계적 특성 연구)

  • Baek, Sang Min;Lim, Sung June;Kim, Min Sung;Ko, Myung Gyun;Park, Chan Yik
    • Composites Research
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    • v.31 no.2
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    • pp.69-75
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    • 2018
  • In this study, a grid panel structure in which the woven CFRP composites were stacked in the orthogonal array was proposed and the mechanical properties were analyzed and studied. The grid parts were fabricated by cutting prepregs and laminating them. The grid panel structure was fabricated by co-curing with lower laminate plate in auto-clave process. The behavior of the proposed grid panel structure was evaluated by tests under tensile, compressive, shear, and bending loads. The effect of increasing the stiffness of the orthogonal grid structure was verified through these tests. In addition, the finite element model was constructed and compared with the test results, confirming the validity and reliability of the test and analysis.

Microscopic Investigation on the Micro-Deformation of Draped Helmet Structure Made of fabric Composite (직물 복합재료를 이용한 드레이핑 헬멧의 미소 변형 관찰)

  • 장승한
    • Composites Research
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    • v.16 no.4
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    • pp.29-35
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    • 2003
  • In this paper. various tow parameters such as equivalent tow thickness, amplitude of longitudinal tow and tow intervals were investigated and compared with each other by using microscopic observation to find out the exact deformation patterns between both directions of the fabric structure(Longitudinal and Transverse Directions). And those observation results were compared with bias extension. biaxial tests results with dry fabric which has the same tow structure as the draped helmet materials and also compared with prepreg specimen which is cured by autoclave moulding without vacuum and pressure condition. Specimens for the observation were taken from draped helmet which is made of fabric composite(Five Harness Satin Weave). From the observation results, it was found that there are different deformation pattern between tow directions and effect of geometric condition on the deformation of the fabric materials during draping process was verified.

Evaluation of Void Content in Carbon Fiber/Epoxy Composites Manufactured by Different Manufacturing Process (제작공법을 달리한 탄소섬유/에폭시 복합재의 기공함유율 평가 기법)

  • Yoona, Sungho;Jang, Jungkeun
    • Journal of the Korean Society of Propulsion Engineers
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    • v.21 no.2
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    • pp.32-40
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    • 2017
  • In this study, the procedures for quantitative measurement of void contents of carbon fiber/epoxy composites were suggested. Two types of the composites were considered: autoclave cured composite and filament wound composite. Void contents of the composites were evaluated by the density of the composites and their constituents, which was determined from weights in the air and water, and the weight fraction and volume fraction of the constituents obtained from the digestion method and combustion method. The surfaces of filtered carbon fibers were examined by FE-SEM in order to investigate the validity of resin removal from the composites. According to the results, the resin in the composites could be fully removed by the digestion method and combustion method. Therefore, the weight fraction and volume fraction of the constituents, and void content of the composites could be quantitatively obtained by the suggested procedures.

Effect of Volume Fraction of Fibers on the Mechanical Properties of a Lightweight Aggregate Concrete Reinforced with Polypropylene Fibers (섬유 혼입률에 따른 섬유보강 경량골재 콘크리트의 역학적 특성)

  • Lee, Haeng-Ki;Song, Su-Yong
    • Journal of the Korea Concrete Institute
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    • v.18 no.6 s.96
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    • pp.743-748
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    • 2006
  • This paper presents results of an experimental study conducted to investigate the effect of volume fraction of fibers on the mechanical properties of a fiber-reinforced, lightweight aggregate concrete(FRLAC) that was produced without an autoclave process. The FRLAC enhanced the strength of lightweight, cellular concrete by adding polypropylene fibers and lightweight aggregates. To investigate the effect of volume fraction of fibers on the mechanical behavior of FRLAC and to determine the optimal volume fraction of fibers, a series of compression and flexural strength tests on FRLAC specimens with various fiber volume fractions(0%, 0.10%, 0.25%, 0.50%) were conducted. It was observed from the tests that a 0.25% volume fraction of fibers maximized the increase in the strength of FRLAC and the fibers controlled cracking in FRLAC.

A Study on Manufacture of Integrated Composite Wing with High Aspect Ratio (고 세장비 일체형 복합재 날개 제작 연구)

  • Joo, Young-Sik;Jun, Oo-Chul;Byun, Kwan-Hwa;Cho, Chang-Min;Han, Jin-Wook
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.41 no.2
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    • pp.127-133
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    • 2013
  • In this paper, the study for the manufacture of the integrated composite wing is performed. The wing has a pivoting structure and high aspect ratio to increase lift drag ratio. The wing is designed with carbon fiber composite because the wing needs to be light and have sufficient strength and stiffness to satisfy structural design requirements. The number of structural members is decreased by part integration to reduce manufacturing cost and the wing is manufactured with the integrated molding process by an autoclave. The material properties are identified by the coupon tests and the structural strength and stiffness are verified through the component tests.

Design of a Piezocomposite Generating Element and Its Characteristics (압전-복합재료 발전 소자의 설계 및 특성)

  • Tien, Minh Tri;Kim, Jong-Hwa;Goo, Nam-Seo
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.34 no.7
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    • pp.867-872
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    • 2010
  • Unused energy derived from sources in nature can be captured and stored for future use, for example, to recharge a battery or power a device; this process of capturing and storing energy is called energy harvesting. Extensive investigations are being carried out in order to use piezoelectricity to harvest the energy generated by body movements or machine vibrations. This paper presents a simple analytical model that describes the output voltage effectiveness of a Piezocomposite Generating Element (PCGE) from vibration and its experimental verification. PCGE is composed of carbon/epoxy, PZT, and glass/epoxy layers. During the manufacturing process, the stacked layers were cured at $177^{\circ}C$ in an autoclave, which created residual stresses in PCGE and altered the piezoelectric properties of the PZT layer. In the experiments, three kinds of lay-up configurations of PCGE were considered to verify the proposed prediction model and to investigate its capability to convert oscillatory mechanical energy into electrical energy. The predicted performance results are in good agreement with observed experimental ones.