• Title/Summary/Keyword: 열처리 시간

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Proton implantation mechanism involved in the fabrication of SOI wafer by ion-cut process (Ion-cut에 의한 SOI웨이퍼 제조에서의 양성자조사기구)

  • 우형주;최한우;김준곤;지영용
    • Journal of the Korean Vacuum Society
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    • v.13 no.1
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    • pp.1-8
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    • 2004
  • The SOI wafer fabrication technique has been developed by using ion-cut process, based on proton implantation and wafer bonding techniques. It has been shown by TRIM simulation that 65 keV proton implantation is required for the standard SOI wafer (200 nm SOI, 400 nm BOX) fabrication. In order to investigate the optimum proton dose and primary annealing condition for wafer splitting, the surface morphologic change has been observed such as blistering and flaking. As a result, effective dose is found to be in the 6∼$9\times10^{16}$ $H^{+}/\textrm{cm}^2$ range, and the annealing at $550^{\circ}C$ for 30 minutes is expected to be optimum for wafer splitting. The depth distribution of implanted hydrogen has been experimentally confirmed by ERD and SIMS measurements. The microstructure evolution in the damaged layer was also studied by X-TEM analysis.

Degradation Evaluation of Aged 1Cr-1Mo-0.25V Steel Using Coercive Force (보자력을 이용한 1Cr-1Mo-0.25V강 인공시효재의 열화도 평가)

  • Ryu, K.S.;Nahm, S.H.;Kim, Y.I.;Yu, K.M.;Son, D.R.
    • Journal of the Korean Society for Nondestructive Testing
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    • v.19 no.4
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    • pp.288-293
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    • 1999
  • The integrity of the turbine rotors can be assessed by the coercive force and Vickers hardness of the aged rotors at service temperature. The coercive force measurement system was constructed in order to evaluate material degradation nondestructively. The test specimen was 1Cr-1Mo-0.25V steel used widely for turbine rotor material, and then the seven kinds of specimens with different degradation levels were prepared by the isothermal heat treatment at $630^{\circ}C$. The coercive force of the test materials was measured at room temperature. Vickers hardness and coercive force decreased with the increase of degradation. The relationship between Vickers hardness and coercive force was investigated. The degradation of test material may be determined nondestructively by the relationship between Vickers hardness and coercive force.

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Serovars of Xanthomonas campetris pv. oryzae Collected from Korea and Serological Diagnosis of Bacterial leaf Blight (우리나라 벼 흰빛잎마름병균 (Xanthomonas campestris pv. oryzae)의 혈청학적 분류 및 진단)

  • Choi J. E.;Lee D. K.;Seo J. H.
    • Korean Journal Plant Pathology
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    • v.1 no.1
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    • pp.61-66
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    • 1985
  • Seventy-one strains collected from Korea were classified into three serovars (designated A, B-I and B-II) by using agar gel diffusion test with the antisera produced against Xanthomonas campestris pv. oryzae isolates Q7472 and Q7502. Of 71 isolates tested, 65 isolates belonged to serovar A, 5 isolates were serovar B-I, and one isolate was serovar B-II. The isolates of serovar B-I and B-II could be distinguished clearly from those of serovar A showing marked autoagglutination. Xanthomonas campestris pv. oryzae was serologically diagnosed in rice leaves by agar gel diffusion tests, possibly being distinguished from Xanthomonas campestris pv. olyzicola and E. herbicola. The pathogen could be also serologically detected from the extracts of diseased leaves, squeezed immediately, heated at $100^{\circ}C$ or incubated in PSA. Serological detection of Xanthomonas campestris pv. oryzae is a more reliable and less time-comsuming method.

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Synthesis of β-tricalcium Phosphate by Using an Eggshell (달걀껍질을 이용한 생체용 β-tricalcium Phosphate 분말의 합성)

  • Kwon, Myoung-Do;Oh, Sun-Ho;Lee, Sang-Jin
    • Journal of the Korean Ceramic Society
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    • v.39 no.11
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    • pp.1103-1107
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    • 2002
  • Biocompatible ${\beta}$-Tricalcium Phosphate(${\beta}$-TCP) powder was successfully synthesized by using a re-cycled eggshell and phosphoric acid. The crystallization behavior of the synthesized powder was dependent on the mixing ratio between the eggshell and phosphoric acid, the starting condition of the eggshell and calcination temperature. The ${\beta}$-TCP was stably synthesized in the 1:1.3~1:1.5 (wt%) mixing ratios of calcined eggshell and phosphoric acid. The synthesis was achieved at about $900{\circ}$ for 1h in an air atmosphere. The crystalline development and microstructure of the synthesized powder were examined by X-ray diffractometer and scanning electron microscopy.

Effect of strontium ions on K2O-TiO2-SiO2 glass soaked in molten Sr(NO3)2 (Sr(NO3)2 용융염에서 이온교환이 K2O-TiO2-SiO2 glass에 미치는 영향)

  • Park, No-Hyung;Yoo, Eun-Sung;Lee, Hoi-Kwan;Huh, Hoon
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.21 no.5
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    • pp.214-217
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    • 2011
  • A fresnoite glass-ceramics has been investigating considerably because of the second order nonlinearity as well as its permanent optical nonlinearity. However, the chemical compositions of transparent glass-ceramics examined in the previous studies have been limited to adjust the composition close to fresnoite stoichiometrically. In this study, to investigate the effect of strontium ions in glass-ceramics on second order nonlinearity, $K_2O-TiO_2-SiO_2$ (KTS) glasses soaked in molten $Sr(NO_3)_2$ were prepared. Crystalline phases of the soaked glasses were measured by X-ray diffraction (XRD) as soaking times and additional heat treatment. The exchange of strontium ions into the glass was verified by Field Emission Scanning Electron Microscope (FE-SEM). And the phenomena of second order harmonic generation (SHG) was observed using Nd-YAG laser.

Application of Quantitative X-ray Diffraction Analysis for Unburned Coal Content on Coke-Char-Sinter Mixtures (고온에서 발생한 코크스-미연소탄-소결광의 혼합물 중 미연소탄의 정량화를 위한 분말 X-선 회절법 적용)

  • 김재명;정진경;김성만;허완욱;김형순
    • Journal of the Korean Ceramic Society
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    • v.40 no.5
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    • pp.481-487
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    • 2003
  • A technique for determination of proportions of char, coal ana coke is needed in order to monitor pulverized coal injection performance in operating blast furnace. Quantitative X-ray powder diffraction analysis can be applied to the problem providing that structural information on carbonaceous materials, coal, char, coke and their mixture are known. Chars were prepared from a coal at different temperatures (1000∼1400$^{\circ}C$) and were characterised by X-Ray powder Diffraction (XRD). The XRD result gave crystallite size (height Lc and diameter, La), aromaticity, number of (002) plane in carbon, and d-spacing. As a result, with increasing heat treat temperature of char, Lc$_{(002)}$, La$_{(10)}$ and number of (002) plane in carbon were increased, and d-spacing and FWHM(Full With Half Maximum) were decreased. Result of prediction of amount of char from the mixtures (char, coke and ore) based on the Lc$_{(002)}$ information of two mixtures (coke and char) showed very close values expected.

Digestive, Physical and Sensory Properties of Cookies Made of Dry-Heated OSA-High Amylose Rice Starch (변성 고아미 쌀전분을 이용한 쿠키의 소화율과 물리적 및 관능적 특성)

  • Han, Jung-Ah
    • Korean Journal of Food Science and Technology
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    • v.41 no.6
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    • pp.668-672
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    • 2009
  • Cookies containing wheat flour mixed with 10, 30 or 50% esterified with octenylsuccinic anhydride (OSA, 3%) and dry-heated ($130^{\circ}C$, 2 hr) high amylose rice (Goami 2) starch (DH-OSAR) were prepared and then their physical and digestive properties were evaluated. When the amount of added DH-OSAR increased, the hardness and brittleness of the cookies decreased, and L (brightness) value increased. For the digestive properties, the cookies containing 50% DH-OSAR significantly increased the amount of slowly digestible starch (SDS), and decreased the amount of rapidly digestible starch (RDS), resulting in the lowest expected Glycemic Index (eGI) among tested cookies. Although the cookies containing DHOSAR were inferior to the control, the addition of xanthan gum (0.5% based on total powder amount) significantly improved their textural and sensory properties. Specially, the cookies containing 50% DH-OSAR and the addition of 0.5% xanthan gum showed the lowest eGI value, maintaining the improved textural and sensory properties.

Preparation of Silica Sol by Partial Hydrolysis of TEOS and High Purity Silica Glass Fiber (TEOS의 부분가수분해에 의한 실리카 졸의 합성과 유리섬유 제조)

  • Yang, Hyun S.;Kwon, Oh H.;Lee, Jae D.;Rho, Jae S.;Kim, Young H.
    • Applied Chemistry for Engineering
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    • v.7 no.5
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    • pp.823-831
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    • 1996
  • At the ratio [$H_2O$]/[TEOS]=1.7, the silica sol was synthesized by partial hydrolysis in the presence of acid catalyst. After stabilizing the silica sol by trimethylsilylation, the molecular weight and viscosity of the sol obtained at various reaction times were examined to determine a best spinnability of the sol. Gel fibers were prepared from the sol solution after removing solvent in the solution, and the gel fibers were heated at $1,000^{\circ}C$. The prepared silica fibers were in the shape of circular cross-section and their tensile strength and $SiO_2$ purity were $83{\pm}20kg/mm^2$ and about 99.997%, respectively.

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Research Trends in Doping Methods on TiO2 Nanotube Arrays Prepared by Electrochemical Anodization (양극산화 기법으로 제조한 TiO2 나노튜브의 촉매 도핑 연구 동향)

  • Yoo, Hyeonseok;Choi, Jinsub
    • Applied Chemistry for Engineering
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    • v.26 no.2
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    • pp.121-127
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    • 2015
  • Nanotubular $TiO_2$ prepared by electrochemical anodization has been significantly used for various applications due to high aspect ratio structures showing a high chemical stability. Morphological properties of nanotubular titanium oxide are easily tailored by adjusting types and compositions of electrolyte, pH value, applied voltage, temperature and anodization time. Since their catalytic properties can be enhanced by doping foreign elements into $TiO_2$, metal as well as non-metal elements are doped into $TiO_2$ nanotubes using different methods. For example, single anodization, thermal annealing, precipitation, and electrochemical deposition have been applied to simplify the doping process. In this review, anodization of Ti to produce $TiO_2$ and doping methods will be discussed in detail.

A Linearization Model of the Stress Relaxation Curves for Fruits and Vegetables (과일 및 채소의 응력완화 직선화 모델)

  • Yoo, Myung-Shik;Song, Woo-Jin;Rho, Young-Ta;Pyun, Yu-Ryang
    • Korean Journal of Food Science and Technology
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    • v.24 no.3
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    • pp.226-231
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    • 1992
  • A generalized linearization model for stress relaxation curves of vegetative tissues was proposed as $[F_{(o)}t^n/(F_{(o)}-F_{(t)})=k_1+k_2t]$, taking into account internal structure changes under a constant strain. Where $F_{(o)}$ is the initial force, $F_{(t)}$ is the decaying force after time t, and $k_1$, $k_2$ and n are constants. This model was well fit to stress relaxation curves of a variety of raw and processed fruits and vegetables.

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