• 제목/요약/키워드: 열연화

검색결과 34건 처리시간 0.027초

젤방상, 열연신 방법에 의한 고강력, 고탄성률 섬유고분자재료의 개발 (Development of high Strength and Hign Modulus Polymeric Mateials by Using Gel SPinning and Hot Drawing)

  • 정호규
    • 유변학
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    • 제7권2호
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    • pp.158-167
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    • 1995
  • 농도 5w%의 초고분자량 폴리에틸렌(분자량:1.5$\times$106)을 상온으로 냉각시켜 벨을 만 들고 이를 방사하여 섬유를 제조하였다. 이때 방사구를 나온 섬유를 $0^{\circ}C$에서 9$0^{\circ}C$까지의 냉 각조를 통과시켜 젤화/결정화 온도를 다르게 하였다. 최대 연신비는 온도가 $0^{\circ}C$에서 7$0^{\circ}C$까 지 증가함에 따라서 증가하고 9$0^{\circ}C$에서 젤화/결정화시킨 섬유의 경우에는 감소한다. 시차주 사열분석, 배향, 인자, 복굴절률, 절단강도와 탄성률을 측정하여 섬유의 물성에 대해 고찰하 였다. 연신비의 증가에 따른 결정화도, 용융 온도, 복굴절률의 증가는 높은 온도에서 젤화/ 결정화시킨 섬유인 경우가 더 뚜렷했다.

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열연화시킨 근관충전방법에 따른 근단폐쇄성에 관한 연구 (A COMPARISON OF THE APICAL SEALING ABILITY OF OBTURATION TECHNIQUES BY THERMALLY SOFTENED GUTTA PERCHA)

  • 백승호
    • Restorative Dentistry and Endodontics
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    • 제23권2호
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    • pp.607-617
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    • 1998
  • The purpose of this study was to evaluate the apical sealing ability of lateral condensation method, vertical condensation method, and MicroSeal obturation system. Sixty-four extracted anterior teeth were instrumented to #40 using Profile. Three groups of 20 teeth were obturated by lateral condensation technique, vertical condensation technique, and and MicroSeal obturation system. Control group were not obturated. Teeth were immersed in resorcinol-formaldehyde resin for 5 days at $4^{\circ}C$, and the resin was allowed to polymerize completely for 4 days at room temperature. Teeth were ground horizontally at 1,5mm(level 1), 2.5mm(level 2), and 3.5mm(level 3) from the anatomic apex and examined with a stereomicroscope at X40 magnification. The photographs were taken a at X40 magnification of the filling in each level and scanned. The leakage area, which was filled with the resin, was measured at each of the three levels. Each ratio of leakage was evaluated by calculating the ratio of thearea of the resin to the total area of the canal and was analyzed statistically. The results were as followed: 1. Vertical condensation group had significantly higher percentage of the area which was obturated by gutta percha than other two technique at each level. 2. At the level 1, there was the greatest leakage in the lateral condensation group, but there was no statistically significant(P>0.05) 3. At the level 2, there was the least leakage in the MicroSeal group, and the most leakage in the lateral condensation group. There was statistically significant difference between the MicroSeal group and the lateral condensation group(P<0.05). 4. At the level 3, there was least leakage in the vertical condensation group, and the most leakage in the lateral condensation group. There was statistically significant difference between the vertical condensation group and the lateral condensation group(P<0.05).

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Microseal 열연화 근관충전법의 치근단 밀폐효과에 관한 연구 (THE EFFECT OF MICROSEAL OBTURATION TECHNIQUE ON THE APICAL SEAL OF ROOT CANALS)

  • 최중조;홍찬의
    • Restorative Dentistry and Endodontics
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    • 제24권2호
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    • pp.356-363
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    • 1999
  • The purpose of this study was to compare the apical sealing effect of Microseal obturation technique with lateral condensation technique in 26 recently extracted single rooted teeth. The root canals were instrumented using step-back technique and obturated with laterally condensed gutta-percha or Microseal. Teeth were suspended in methylene blue dye for 2 days and then longitudinary splited. The apical microleakage and the adaptability of gutta-percha to the root canal wall were examined under a stereomicroscope at ${\times}20$ magnification. The results were as follows: 1. The mean leakage was 1.38${\pm}$1.18 mm for laterally condensed gutta-percha group, and 0.71${\pm}$0.57 mm for Microseal gutta-percha group. But there was no statistical difference between two groups. 2. In Microseal gutta-percha group, they showed no gap between the master cone and Microseal gutta-percha, and showed homogeneous mass. 3. In contrast, laterally condensed gutta-percha group showed some gaps not only between gutta-percha cones, but also between gutta-percha cones and the canal walls, and the gaps were filled with some sealer. And also this group showed some amout of sealer on the root canal walls, Within the limits of the results of this experiment, Microseal gutta-percha obturation technique demonstrated relatively favorable apical sealing effect and shorter obturation time. Thus, it is thought that this obturation technique is a acceptable method for clinical use but further studies on this matter should be conducted.

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Easy Filling 및 Quick Obturation System을 이용한 열연화 충전법의 치근단 밀폐도 평가 (A COMPARISON OF THE APICAL SEAL PRODUCED BY EASY FILLING SYSTEM AND QUICK OBTURATION SYSTEM)

  • 신정인;금기연;이승종
    • Restorative Dentistry and Endodontics
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    • 제25권2호
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    • pp.202-211
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    • 2000
  • The aim of this study was to compare the apical sealing ability of a new thermoplasticized gutta-percha filling technique, the Easy Filling and the Quick Obturation system with lateral condensation technique and Thermafil system to evaluate their clinical acceptabilities. Fifty-two extracted single-rooted teeth were instrumented to #35 using the .04 taper ProFile system. Four groups of 12 teeth were obturated by lateral condensation technique. Thermafil system and two new thermoplasticized gutta-percha techniques, the Easy Filling system and Quick Obturation system (Meta Dental co. Ltd. Korea), respectively. Four teeth served as controls. After the teeth were immersed in 2% methylene blue dye for 48 hours, they were resected horizontally at 1mm to 5mm level from the anatomical apex using a low-speed microtome. Each section was examined under a stereomicroscope at ${\times40}$ magnification and photographed. After each image was scanned, the leakage area was measured at each level using Brain 3 (Nosdia Tech., Korea) software. Leakage ratio was calculated for each group and was analyzed statistically to come up with the following results: 1. At 1mm level, the Quick Obturation system had the largest amount of apical leakage and it was statistically significant when compared with the lateral condensation group and the Thermafil group (p<0.05). 2. At 2mm and 3mm level, there were no significant difference of apical leakage among all four groups (p>0.05), and from 4mm level, no apical dye penetration was observed in all the groups. In conclusion, the apical seal produced by Easy Filling system and the Quick Obturation system was comparable to lateral condensation technique and Thermafil system except for the 1mm level. More improvement of the apical seal can be expected as the operator becomes skillful with the new techniques.

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마멸에 의한 온간단조의 금형수명 예측에 관한 연구(II) -금형 마멸 모델의 적용- (A Study on Predictin of Die Life of Warm Forging by Wear(II) -Application of Suggested Die Wear Model-)

  • 강종훈;박은우;제진수;강성우
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 1998년도 춘계학술대회논문집
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    • pp.94-99
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    • 1998
  • In bulk metal forming processes prediction of tool life is very important for saving production cost and achieving good material properties. Generally the service life of tools in metal forming process is limited to a large extent by wear, fracture and plastic deformation of tools. In case of hot and warm forging processes, tool life depends on wear over 70%. In this study finite element analyses are applied to warm forging and hot forging by adopting suggested wear model. By comparision of simulation and real profile of die, suggested model is verified

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마멸에 의한 온간단조의 금형수명 예측에 관한 연구(I) -금형 마멸 모델의 정립- (A Study on Prediction of Die Life of Warm Forging by Wear(I) -Construction of Die Wear Model-)

  • 강종훈;박인우;제진수;강성수
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 1998년도 춘계학술대회논문집
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    • pp.88-93
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    • 1998
  • The service life of tools in metal forming process is to a large extent limited by wear, fatigue fracture and plastic deformation. In warm forging processes wear is the predominant factor for operating lives of tools. To predict tool life by wear, Archard's wear model is generally applied. Usually hardness of die is considered to be a function of temperature in Archard's wear model. But hardness of die is a function of not only temperature but also operating time of die. To consider softening of die by repeated operations, it is necessary to express hardness of dies by a function of temperatures and operating time. By experiment of reheating of dies, die softening curves were obtained. Finally modified Archard's wear model in which hardness of die was expressed as a function of main tempering curve was proposed.

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고강도 열연강판의 경량 자동차 샤시부품 개발 (Application Technology of high strength hot-rolled steels for automotive lightweight chassis parts)

  • 김종철;권태우;전진화;손경선
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2005년도 추계학술대회 논문집
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    • pp.43-45
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    • 2005
  • For application of advanced high strength hot-rolled steels (i.e. DP590, DP780) to automotive lightweight chassis parts, various technologies from design to forming test, optimization of welding condition and investigation of coating properties were tried. The target part of this study was automotive rear sub frame and we could make $16.8\%$ weight reduction by reducing the material thickness and optimizing the design. In addition, the formability and weldability of the newly developed AHSS, DP780, were evaluated.

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팽윤습열연신에 의한 아크릴섬유의 고강도화에 관한 연구 (A study on the development of high strength for acryl fiber during uniaxial stretching by swell-wet process)

  • 이문수;송경헌
    • 자연과학논문집
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    • 제8권1호
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    • pp.145-151
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    • 1995
  • 건열일축연신법에 의한 합성섬유의 연신은 높은 유리전이온도 때문에 대략 $150^{\circ}C$이상의 온도에서 행하여 지고 있다. 그러나, 팽윤습열연신법은 유기용매를 팽윤제로 사용하여 미세구조를 변화시키기 때문에 낮은 온도에서 연신 할 수 있는 특징을 갖고 있다. 본 연구에서는 비교적 낮은 온도인 $70^{\circ}C$에서 팽윤습열 일축연신에 의한 100% 아크릴섬유의 고강도화에 대하여 연구하였다. 연신능력은 연신일에 의하여 계상하였으며, 이 연신일은 연신응력과 변형 그리고 초기영율에 의하여 좌우됨을 알 수 있었다. 연신은 아크릴 섬유의 고강도를 위해 필요한 요인임을 확인할 수 있었다. 또한, 아크릴 섬유의 고강도화를 위한 분자배향도 및 결정화도 증가에 따른 연신조건의 효과와 물성 변화에 대하여 비교. 검토하였다.

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Mo첨가 열연강판의 반복 열처리 제어압연에 관한 연구 (A Study on Repeat Heat Treating and Controlled Rolling of Mo-alloyed Plate Steels)

  • 이정훈;홍승찬;이경섭
    • 한국재료학회지
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    • 제9권7호
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    • pp.740-747
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    • 1999
  • 결정립 미세화는 강도와 인성을 동시에 향상시킬 수 있는 유일한 방법이다. 제어압연과 가속냉각은 공정 중에 재결정과 결정립 조대화 거동을 조절함으로써 기계적 성질을 향상시키는 효과적인 방법으로 알려져 있으며, 반복열처리에 의한 반복상변태는 결정립 미세화 방법 중의 하나이다. 본 연구에서는 제어압연과 반복열처리를 복합 적용하여 그 효과를 관찰하였다. Mo 첨가효과와 공정변수의 효과를 관찰하기 위해 Mo이 첨가된 저탄소강 시편을 준비하여 Gleeble로 가공열처리 모의실험을 하였다. Mo첨가는 결정립 조대화 온도를 상승시키고, 오스테나이트 재결정을 억제하는 효과를 나타내었다. 오스테나이트 결정립 미세화에 가장 효과적인 공정조건은 반복 열처리 제어압연을 두번 실시하는 것이고, 첫번째보다 두번째 압연율을 더 크게 하는 것이었다

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모조 근관의 크기와 충전 방법이 orthograde MTA apical plug의 미세누출에 미치는 영향 (EFFECTS OF CONDENSATION TECHNIQUES AND CANAL SIZES ON THE MICROLEAKAGE OF ORTHOGRADE MTA APICAL PLUG IN SIMULATED CANALS)

  • 남득림;박정길;허복;김현철
    • Restorative Dentistry and Endodontics
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    • 제34권3호
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    • pp.208-214
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    • 2009
  • 이 연구의 목적은 서로 다른 두 개의 근관 크기(#70, #120)를 가진 레진 모형에 MTA (minoral trioxide aggregate)를 서로 다른 두 가지 방법 (수기구 충전(HC), 초음파 보조 수기구 충전(UAHC))으로 정방위 충전하고 MTA apical plug의 미세 누출을 평가하는 것이다. 직선형 근관 형태를 가지며, #70과 #120의 치근단 크기를 갖는 레진 모형을 각각 30개씩 준비하였다. 이 시편들을 MTA의 적용 방법에 따라 각 군을 2개의 아군으로 다음과 같이 분류하였다 (n=15); C70: HC + 치근단 크기 #70, C120: HC + 치근단 크기 #120, U70: UAHC + 치근단 크기 #70, U120: UAHC + 치근단 크기 #120. MTA 충전을 완료한 후에, 24시간 동안 실온에서 100% 습도를 유지하여 경화시켰다. 근관의 상부는 열연화 충전 시스템(Obtura II)을 이용하여 충전하였다. 48시간 동안 100% 습도를 유지하여 실온에서 0.2% rhodamine B 용액을 이용해 미세누출 실험을 하였다. 이 연구결과 #70의 치근단 크기를 갖는 그룹 사이에서 UAHC가 HC에 비해 미세누출이 적은 것으로 나타났다(p<0.05). 이 연구 조건하에서는 초음파 진동을 동반한 정방위 MTA apical plug 형성 방법이, 특히 좁은 근관에서 더 효율적인 것으로 사료된다.