• Title/Summary/Keyword: 열분석적 특성

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Analyzing the status of theoretical framework by subfields in library and information science research articles (문헌정보학 연구논문의 이론체계 현황분석 연구)

  • Kim, Sung-Jin;Jeong, Dong-Youl
    • Journal of the Korean Society for information Management
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    • v.23 no.2
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    • pp.21-37
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    • 2006
  • Based upon the assumption that both theory building and theory use are intertwined to construct a cohesive body of knowledge in the filed, this study attempts to identify the state of theoretical framework by examining the number and the quality of theoretical articles by subfield. Theoretical article is characterized as an incident in which in which the author contributes to the development or the use of theory in his/her own paper. Theoretical incidents were identified by a content analysis of 1,661 articles in four LIS journals from 1984 to 2003. The findings suggest that the four subfields, such as information seeking/use, information retrieval, library management, and scholar communication had great contributions to both theory building and theory use. Also, two research areas such as bibliometrics and professionals are very likely to be theoretical. Further, the analysis of the name of theories used by subfields could give an insight into the understanding of how the theoretical frameworks of each subfield are related.

Fabrication and the Electrochemical Characteristics of Petroleum Residue-Based Anode Materials (석유계 잔사유 기반 음극재 제조 및 그 전기화학적 특성)

  • Kim, Daesup;Lim, Chaehun;Kim, Seokjin;Lee, Young-Seak
    • Applied Chemistry for Engineering
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    • v.33 no.5
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    • pp.496-501
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    • 2022
  • In this study, an anode material for lithium secondary batteries was manufactured using petroleum-based residual oil, which is a petroleum refining by-product. Among petroleum-based residual oils, pyrolysis fuel oil (PFO), fluidized catalyst cracking-decant oil (FCC-DO), and vacuum residue (VR) were used as carbon precursors. The physicochemical characteristics of petroleum-based residual oil were confirmed through Matrix-assisted laser desorption/ionization Time-of-Flight (MALDI-TOF) and elemental analysis (EA), and the structural characteristics of anode materials manufactured from residual oil were evaluated using X-ray crystallography (XRD) and Raman spectroscopic techniques. VR was found to contain a wide range of molecular weight distributions and large amounts of impurities compared to PFO and FCC-DO, and PFO and FCC-DO exhibited almost similar physicochemical characteristics. From the XRD analysis results, carbonized PFO and FCC-DO showed similar d002 values. However, it was confirmed that FCC-DO had a more developed layered structure than PFO in Lc (Length of a and c axes in the crystal system) and La values. In addition, FCC-DO showed the best cycle characteristics in electrochemical characteristics evaluation. According to the physicochemical and electrochemical results of the petroleum-based residual oil, FCC-DO is a better carbon precursor for a lithium secondary battery than PFO and VR.

A Study on Fatigue Design Automation of Plug- and Ring-type Gas-welded Joints of STS301L Taking Welded Residual Stress into Account (용접잔류응력을 고려한 STS301L 플러그 및 링 용접부의 피로설계 자동화에 관한 연구)

  • Baek, Seung-Yeb;Yun, Ki-Ho
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.34 no.9
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    • pp.1137-1143
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    • 2010
  • This paper presents a fatigue design method for plug- and ring-type gas-welded joints, which takes into account the effects of welding residual stress. To develop this method, we simulated the gas-welding process by performing nonlinear finite element analysis (FEA) To validate the FEA results, numerically calculated residual stresses in the gas welds were then compared with experimental results obtained by the hole-drilling method. To evaluate the fatigue strength of plug- and ring-type gas-welded joints influenced by welding residual stresses, the use of stress amplitude $(\sigma_a)_R$, which includes the welding residual stress in gas welds, is proposed $(\sigma_a)_R$ on the basis of a modified Goodman equation that includes the residual stress effects. Using the stress amplitude $(\sigma_a)_R$ at the hot spot point of gas weld, the relations obtained as the fatigue test results for plug and ring type gas welded joints having various dimensions and shapes were systematically rearranged to obtain the $(\sigma_a)_R-N_f$ relationship. It was found that more systematic and accurate evaluation of the fatigue strength of plug- and ring-type gas-welded joints can be achieved by using $(\sigma_a)_R$.

Mechanical Properties of Thermally Compressed Domestic Softwoods (국내산 침엽수 열압밀화재의 역학적 특성)

  • Hwang, Sung-Wook;Cho, Beom-Geun;Lee, Won-Hee
    • Journal of the Korean Wood Science and Technology
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    • v.42 no.6
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    • pp.666-674
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    • 2014
  • In this study, we investigated mechanical properties of Korean softwoods after applying thermal compression. Density of compressed woods was notably increased with thermal compression. In case of 50% compression set, density of Korean pine (Pinus koraiensis), Japanese red pine (P. densiflora), and Larch (Larix kaempferi) wood was increased by 71%, 74%, and 76%, respectively, when compared to the control group. The strength of woods was increased and quality of the woods became homogeneous with an increases in the compression set. On the 50% compression set, the compressive strength, bending strength, and hardness of Korean pine wood was increased by 76%, 83%, and 55%, respectively compared to the control group. Longitudinal compressive strengths of Japanese red pine wood increased by 69%, 130%, and 76%, respectively and those of Larch wood increased by 77%, 120%, and 44%, respectively. In thermal compression wood, mechanical properties of Larch wood was the highest, while those of Korean pine wood were the lowest. However, Japanese red pine wood showed the highest in the increase rate of mechanical properties after the thermal compression.

Development of Piezoelectric Transformer Using The Single Crystal of LiTaO3 (LiTaO3 단결정을 사용한 압전변압기의 개발)

  • Hwang, Sung-Phil;Kim, Moo-Joon;Ha, Kang-Lyeol;Kang, Gab-Joong
    • Journal of Sensor Science and Technology
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    • v.11 no.3
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    • pp.132-137
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    • 2002
  • The single crystal of $LiTaO_3$ ($x-112^{\circ}$ y) has very stable thermal characteristics in a piezoelectric transformer. In this paper, a piezoelectric transformer made of the crystal is newly designed and its operating characteristics are analyzed. The length of the transformer is determined as twice as its width for Lame'-mode because the single crystal of $LiTaO_3$ has low electro-acoustic efficiency. The electric and vibrational characteristics of the transformer is simulated by the PSpice program, and its results are compared to experimental ones. As the results, the ratio of output voltage to input shows large than 10 at 290.83[kHz], which is the frequency coupled the 2nd harmonic for length and the fundamental for width of the Lame'-mode transformer.

Long Memory and Cointegration in Crude Oil Market Dynamics (국제원유시장의 동적 움직임에 내재하는 장기기억 특성과 공적분 관계 연구)

  • Kang, Sang Hoon;Yoon, Seong-Min
    • Environmental and Resource Economics Review
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    • v.19 no.3
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    • pp.485-508
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    • 2010
  • This paper examines the long memory property and investigates cointegration in the dynamics of crude oil markets. For these purposes, we apply the joint ARMA-FIAPARCH model with structural break and the vector error correction model (VECM) to three daily crude oil prices: Brent, Dubai and West Texas Intermediate (WTI). In all crude oil markets, the property of long memory exists in their volatility, and the ARMA-FIAPARCH model adequately captures this long memory property. In addition, the results of the cointegration test and VECM estimation indicate a bi-directional relationship between returns and the conditional variance of crude oil prices. This finding implies that the dynamics of returns affect volatility, and vice versa. These findings can be utilized for improving the understanding of the dynamics of crude oil prices and forecasting market risk for buyers and sellers in crude oil markets.

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Analysis of Local Government Social Welfare Finance - A case study of GuRoGu budget(2000~2007) - (기초지방자치단체 사회복지 재정 분석 - 서울시 구로구 예산서(2000년~2007년) 사례 -)

  • Joung, Won-Oh;Kim, Sung-Kee
    • Korean Journal of Social Welfare Studies
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    • v.40 no.2
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    • pp.33-58
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    • 2009
  • The main purpose of this study is to explore the structure of local government social welfare finance and tendency of changing structure and what affects the change. We select GuRoGu budget from 2000 to 2007 as one of local governments in Korea to perform the study goal. After we analyzed the contents of the budget, we have developed the framework of analysis for reclassifying local government welfare budget. First of all, we find utility of the framework of analysis which classify local government social welfare budget as target groups, properties, and the source of the finance. Secondly, the structure of local government welfare finance has changed for 8 years. The rate of finance for direct service has risen more than that for indirect service, and the rate of finance providing material(or service) type has risen more than that of providing monetary type. The rate of the finance from central government has grown up rapidly, whereas that from local government has fallen off. The hypotheses that the rate of financial self-reliance and the increase rate of social welfare expenditure to the previous year play a significant role to the rate of social welfare expenditure are not clear in our study. But we find the central government's effects to the local government welfare budget has grown up. So, we propose if we analyze the hypothesis of incrementalism, we must divide the effects of the previous year expenditure from the effects of central government's policy.

질소 첨가된 GeSe 비정질 칼코지나이드 박막을 이용한 OTS (Ovonic threshold switching) 소자의 switiching 특성 연구

  • An, Hyeong-U;Jeong, Du-Seok;Lee, Su-Yeon;An, Myeong-Gi;Kim, Su-Dong;Sin, Sang-Yeol;Kim, Dong-Hwan;Jeong, Byeong-Gi
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2012.05a
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    • pp.78.2-78.2
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    • 2012
  • 최근 PRAM의 집적도 향상 및 3차원 적층에 의한 메모리 용량 향상을 위해 셀 선택 스위치로서 박막형 Ovonic Threshold Switching (OTS) 소자를 적용한 Cross bar 구조의 PRAM이 제안된 바 있다. OTS 소자는 비정질 칼코지나이드를 핵심층으로 하는 2단자 소자로서 고저항의 Off 상태에 특정 값 (문턱스위칭 전압) 이상의 전압을 가해주면 저저항의 On 상태로 바뀌고 다시 특정 값 (유지전압) 이하로 전압을 감소시킴에 따라 고저항의 Off 상태로 복원하는 특성을 갖는다. 셀 선택용 스위치로 적용되기 위해서는 핵심적으로 On-Off 상태간의 가역적인 변화 중에도 재료가 비정질 구조를 안정하게 유지해야 하며 전기적으로는 Off 상탱의 저항이 크고 또한 전류값의 점멸비가 커야 한다. GeSe는 이원계 재료로서 단수한 구성에도 불구하고 OTS 소자가 갖추어야할 기본적인 특성을 가지는 것으로 알려져 있다. 본 연구에서는 GeSe로 구성된 OTS 재료에 경원소인 질소를 첨가하여 비정질 상태의 안정성과 소자특성의 개선 효과를 조사하였다. RF-puttering 시 Ar과 $N_2$의 혼합 Gas를 사용하여 조성이 $Ge_{62}Se_{38}$ ($N_2$ : 3%)인 박막을 제작하여 DSC를 통해 결정화온도(Tx)를 확인하였고, $N_2$ gas의 함유량이 각각 1 %, 2 %, 3 %인 $Ge_{62}Se_{38}$인 박막을 전극의 접촉 부 면적이 $10{\times}10\;{\mu}m^2$인 cross-bar 구조의 소자로 제작하여 Threshold switching voltage ($V_{th}$), Delay time ($t_d$), $I_{on}/I_{off}$ 그리고 Endurance 특성을 평가하였다. DSC 분석 결과 $N_2$ 가 3 % 첨가된 GeSe 박막은 Tx가 $371^{\circ}C$에서 $399^{\circ}C$로 증가되었다. $N_2$가 1% 첨가된 GeSe 소자를 측정한 결과 $V_{th}$의 변화 없는 가운데 $I_{on}/I_{off}$이 약 $2{\times}10^3$에서 $5{\times}10^4$로 향상되었다. Endurance 특성 역시 $10^4$에서 $10^5$번으로 향상되었다. $t_d$의 경우 비정질 상태의 저항 증가로 인해 약 50% 증가되었다. 이러한 $N_2$의 첨가로 인한 비정질 GeSe 박막의 변화 원인에 대한 분석 결과를 소개할 예정이다.

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Polyether Ether Ketone Membrane with Excellent Pure Permeability Using Thermally Induced Phase Separation Method and Morphology Analysis with Characterization (열유도 상분리법을 이용한 순수 투과 성능이 우수한 폴리에테르 에테르 케톤 분리막 제조와 모폴로지 분석 및 특성평가)

  • Kwang Seop Im;Seong Jun Jang;Chae Hong Lim;Sang Yong Nam
    • Applied Chemistry for Engineering
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    • v.35 no.3
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    • pp.214-221
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    • 2024
  • Polyether ketone (PEEK) has been widely used in membranes because of its excellent thermal stability, chemical resistance, and significant mechanical strength. However, the melting temperature is very high, making it difficult to find suitable solvents. Therefore, in this study, PEEK and benzophenone (DPK) were used as diluents to prepare a membrane with excellent mechanical strength and chemical stability using the thermally induced phase separation (TIPS) method to compensate for the shortcomings of PEEK membrane preparation and achieving the highest performances. The optimal membrane manufacturing conditions were confirmed through the crystallization temperature and cloud point according to the polymer content through the phase diagram. Subsequently, the morphological changes of the membrane, influenced by the polymer and diluent content, were confirmed through scanning electron microscopy (SEM). Additionally, the membrane thickness tended to increase with higher polymer content. Tensile strength and DI-water permeability tests were conducted to confirm the mechanical strength and permeability of the membrane. Through the previous characteristic evaluation, it was confirmed that the membrane using PEEK had excellent mechanical strength and permeability.

Synthesis of Low-Priced Catalyst from Coal Fly Ash for Pyrolysis of Waste Low Density Polyethylene (석탄비산재(石炭飛散災)로부터 저밀도(低密度) 폴리에틸렌 폐기물(廢棄物) 열분해용(熱分解用) 저가(低價) 촉매(觸媒) 합성(合成))

  • Jeong, Byung-Hwan;Na, Jeong-Geol;Kim, Sang-Guk;Mo, Se-Young;Chung, Soo-Hyun
    • Resources Recycling
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    • v.16 no.2 s.76
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    • pp.48-55
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    • 2007
  • A low-priced catalyst for pyrolysis of LDPE has been synthesized. Fly ash, which is waste material generated from coal-fired power plants was used as silica and alumna sources for solid acid catalyst. Amorphous silica-alumina catalysts (FSAs) were pre-pared by dissolution of silica and alumina from fly ash, followed by co-precipitation of the dissoluted ions. A series of LDPE pyrolysis were carried out in a thermogravimetric analyzer to investigate the effects of synthesis conditions such as NaOH/fly ash weight ratio and activation time one catalytic performance of FSAs. The physical properties of FSAs were examined and related to their catalytic performances. FSA(1.2-8) synthesized with NaOH/fly ash weight ratio of 1.2 and the activation time of 8 hours showed the best catalytic performance. The catalytic performance of FSA(1.2-8) was comparable with that of commercial catalysts and it was concluded that the FSA could be a good candidate for catalytic use in the recycling of waste polyolefins.