• Title/Summary/Keyword: 연자성

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Synthesis of Water-Soluble Magnetite Nanoparticles from Formation of $Fe_3O_4$ Nanocrystals ($Fe_3O_4$ 나노 결정체의 형성을 통한 수용성의 자성 나노 입자의 합성)

  • Kim, Chanyoung;Kim, Sunghyun;Kwon, Hyungjun
    • Journal of Integrative Natural Science
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    • v.1 no.3
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    • pp.247-249
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    • 2008
  • 자성 결정체인 $Fe_3O_4$ 나노 입자를 합성하기위하여 강한 극성 용매인 2-pyrrolidone을 연전도 반응매개체로 하여 용액 내에 $FeCl_3{\cdot}6H_2O$을 용해시켜 2-pyrrolidone의 비등점까지 나노 결정체 고온 열분해 방법을 이용하여 제조되었다. 고온 열분해 후, $Fe_3O_4$ 나노 입자는 methanol/diethyl ether (1:3)에 의해서 침전되어졌다. 합성된 $Fe_3O_4$ 나노 입자는 고결정도, 고자기성을 가지고 있으며, 수용성의 자성 나노 결정체이다. 합성된 $Fe_3O_4$ 나노 입자의 크기와 결정도는 transmission electron microscope (TEM, Tecnai F20)를 이용하여 특성 분석하였으며, area electron diffraction (SAED) pattern과 HRTEM을 이용하여 나노입자의 격자 패턴 (lattice fringes)을 확인하였다.

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Magnetic Properties of FeZrBAg Soft Magnetic Thin Films with High Permeability and High Magnetization (고투자율, 고포화자화 FeZrBAg 연자성 박막의 자기적 특성)

  • 민복기;김현식;송재성
    • Journal of the Korean Magnetics Society
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    • v.9 no.6
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    • pp.285-290
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    • 1999
  • The magnetic properties of sputtered amorphous $Fe_{86.7}Zr_{3.3}B_4Ag_6$ thin films, which contains an additional insoluble element Ag, have been investigated as a function of uniaxal field annealing temperature. The amorphous $Fe_{86.7}Zr_{3.3}B_4Ag_6$ thin films produced by relatively low temperature annealing at 40$0^{\circ}C$ for 1 hour was found to have very high permeability of 7800 at 50 MHz, 0.2 mOe, high magnetization of 1.7 T, low coercivity of 1.0 Oe and very low core loss of 1.4 W/cc at 1 MHz, 0.1 T, respectively. It is notable that the permeability and core loss values for various kinds of the soft magnetic thin films reported up to now. The reason for the appearance for the good soft magnetic properties is presumably due to the homogeneous formation of very fine bcc $\alpha$-Fe clusters with the size in the amorphous $Fe_{86.7}Zr_{3.3}B_4Ag_6$ thin films matrix, which can be deduced from the XRD results.

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A Micro Fluxgate Magnetic Sensor with Closed Magnetic Path (폐자로를 형성한 마이크로 플럭스게이트 자기 센서)

  • 최원열;황준식;강명삼;최상언
    • Journal of the Microelectronics and Packaging Society
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    • v.9 no.3
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    • pp.19-23
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    • 2002
  • This paper presents a micro fluxgate magnetic sensor in printed circuit board (PCB). In order to observe the effect of the closed magnetic path, the magnetic cores of rectangular-ring and two bars were each fabricated. Each fluxgate sensor consists of five PCB stack layers including one layer magnetic core and four layers of excitation and pick-up coils. The center layer as a magnetic core is made of a Co-based amorphous magnetic ribbon with extremely high DC permeability of ~100,000. Four outer layers as an excitation and pick-up coils have a planar solenoid and are made of copper foil. In case of the fluxgate sensor having the rectangular-ring shaped core, excellent linear response over the range of -100 $\mu$T to + 100 $\mu$T is obtained with 540 V/Tsensitivity at excitation square wave of 3 $V_{p-p}$ and 360 KHz. The chip size of the fabricated sensing element is $7.3 \times 5.7\textrm{mm}^2$. The very low power consumption of ~8 mW was measured. This magnetic sensor is very useful for various applications such as: portable navigation systems, telematics, VR game and so on.n.

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A New LC Resonator Fabricated by MEMS Technique and its Application to Magnetic Sensor Device (MEMS 공정에 의한 LC-공진기형 자기센서의 제작과 응용)

  • Kim, Bong-Soo;Kim, Yong-Seok;Hwang, Myung-Joo;Lee, Hee-Bok
    • Journal of the Korean Magnetics Society
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    • v.17 no.3
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    • pp.141-146
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    • 2007
  • A new class of LC-resonator for micro magnetic sensor device was invented and fabricated by means of MEMS technique. The micro LC-resonator consists of a solenoidal micro-inductor with a bundle of soft magnetic microwire cores and a capacitor connected in parallel to the micro-inductor. The core magnetic material is a tiny glass coated $Co_{83.2}B_{3.3}Si_{5.9}Mn_{7.6}$ microwire fabricated by a glasscoated melt spinning technique. The core materials were annealed at various temperatures $150^{\circ}C,\;200^{\circ}C\;,250^{\circ}C\;,$ and $300^{\circ}C$ for 1 hour in a vacuum to improve soft magnetic properties. The solenoidal micro-inductors fabricated by MEMS technique were $500{\sim}1,000{\mu}m$ in length with $10{\sim}20$ turns. The changes of inductance as a function of external magnetic field in micro-inductors with properly annealed microwire cores were varied as much as 370%. Since the permeability of ultra soft magnetic microwire is changing rapidly as a function of external magnetic field. The inductance ratio as well as magnetoimpedance ratio (MIR) in a LC-resonator was varied drastically as a function of external magnetic field. The MIR curves can be tuned very precisely to obtain maximum sensitivity. A prototype magnetic sensor device consisting of the developed microinductors with a multivibrator circuit was test successfully.

Study of the Effects of Fe94Si5Cr1-Rubber Absorbers with Sheet-Thickness (Fe94Si5Cr1을 이용한 Sheet 두께에 따른 전파흡수특성 연구)

  • Kim, Moon-Suk;Min, Eui-Hong;Koh, Jae-Gui
    • Journal of the Korean Magnetics Society
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    • v.19 no.2
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    • pp.62-66
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    • 2009
  • The soft magnetic FeSiCr were processed the ball-mill for 30 hours and the shape of FeSiCr particles was changed from sphere to flake type, which was observed using scanning electron microscope. The complex permittivity and permeability spectra and reflection loss of FeSiCr-rubber composite was measured using Network Analyzer in order to investigate the relationship between the microwave absorption and the material constants. The matching frequency shifted toward lower frequency range with microwave absorber thickness, and microwave absorber with FeSiCr-rubber composite showed a maxium reflection loss of -8.3 dB at 1.86 GHz for a 1.3 mm thickness.

Reduction of Leakage Magnetic Fields in Low Frequency WPT System Using Soft Magnetic Materials (연자성체를 이용한 저주파 무선전력전송 시스템의 누설 자기장 저감)

  • Lee, In-Gon;Kim, Nam;Cho, In-Kui;Hong, Ic-Pyo
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.28 no.1
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    • pp.76-79
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    • 2017
  • This paper presents the electromagnetic shielding structure for low frequency wireless power transfer system with magnetic induction method using soft magnetic materials. Soft magnetic materials have advantages such as high permeability and low magnetic loss, but have undesirable effect of power loss by eddy current. To overcome this, we proposed the patterned soft magnetic material to suppress the eddy current path. For validity of this paper, we simulated the coil transfer efficiency and the radiated electromagnetic field, and fabricated the proposed structure using 79-permalloy. The measured results shows good agreements with the simulated results and reduction of the radiated electromagnetic field compared to commercial ferrite plate.

Magnetic Bias Effects in Field-annealed CoFeSiB Amorphous Ribbons (공기 중에서 자기장 열처리된 CoFeSiB 비정질 리본에서의 자기 바이어스 효과)

  • Cha, Yong-Jun;Jeong, Jong-Ryul;Kim, Cheol-Gi;Kim, Dong-Young;Yoon, Seok-Soo
    • Journal of the Korean Magnetics Society
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    • v.19 no.6
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    • pp.191-196
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    • 2009
  • Magnetic bias phenomena of field-annealed CoFeSiB amorphous ribbons showing asymmetric giant magnetoimpedance was investigated by MOKE method. The specimens removed the crystalline layer at one surface side by chemical etching were prepared and measured magnetization curves by MOKE to investigate the effect of the crystalline layer on magnetization of inner soft amorphous phase. We observed the shift of hysteresis loop, and concluded that the crystalline layer exerts bias field effect on inner soft amorphous phase and the direction of bias filed is opposite to the magnetization direction of surface crystalline layer.

The Effect of Annealing on Soft Magnetic Properties of Ee-Hf-N Thin Films Prepared by Reactive Sputtering (반응성 스퍼터링에 의해 제조된 Fe-Hf-N 박막의 연자기 특성에 미치는 열처리 영향)

  • 김경일;김병호;김병국;제해준
    • Journal of the Korean Magnetics Society
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    • v.10 no.4
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    • pp.165-170
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    • 2000
  • The purpose of this study is to investigate the effect of annealing conditions on physical and magnetic properties of Fe-Hf-N thin films. When the thin films were annealed in $N_2$ gas, a surface oxide layer, comprised of Fe$_2$O$_3$ and Fe$_3$O$_4$, was formed at the surface of the thin films and a Fe-Hf-O-N layer was also formed under this surface oxide layer. It was found that the thicknesses of the surface oxide layer and the Fe-Hf-O-N layer increased, as the annealing temperature increased. It was also found that if the thickness of the surface oxide layer was excluded in the property calculation, the soft magnetic properties of the annealed thin films were not much different from those of the as-deposited thin films. Therefore, it was suggested that the Fe-Hf-O-N layer formed under the surface oxide layer did not lose significantly the soft magnetic properties of the Fe-Hf-N films and the Fe-Hf-N films annealed in $N_2$gas showed the soft magnetic properties of the Fe-Hf-N and Fe-Hf-O-N multi-layers.

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Effects of Annealing on Electromagnetic Wave Absorption Characteristics in FeSiCr Flakes/Polymer Composite Sheets (FeSiCr 박편/폴리머 복합 시트의 전자파 흡수 특성에 미치는 합금 어닐링 효과)

  • Kim, Ju-Beom;Noh, Tae-Hwan
    • Journal of the Korean Magnetics Society
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    • v.23 no.3
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    • pp.83-88
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    • 2013
  • The soft magnetic Fe-Si-Cr flakes with the thickness of about 1 ${\mu}m$ were annealed at 500 and $700^{\circ}C$ for 1 h, and the composite sheets for electromagnetic wave noise absorber available for quasi-microwave band were fabricated by using these annealed flakes and polymer. Further the power loss characteristics of the composite sheets was investigated to clarify the annealing effect on electromagnetic wave absorption properties. The power loss decreased in the frequency range of several GHz when the annealed flakes were used as compared to the sheet using the as-milled FeSiCr alloy flakes. Moreover the sheets using annealed flakes exhibited lower value of real and imaginary part of complex permeability. These inferior electromagnetic wave absorption properties of the composite sheets using annealed alloy flakes were considered to be obtained by the enhanced eddy current effect upon annealing-induced recovery of microstructure and resulted low complex permeability.

MAGNETIC PROPERTIES OF $Fe_{73.5}Cu_1Nb_3Si_{15.5}B_7/Co_{88.3}Fe_{5.07}B_{3.44}Si_{3.19}$ TWO-PHASES RIBBON

  • Kim, W. B.;S. M. Hong;Kim, C. O.;Kim, C. G.
    • Proceedings of the Korean Magnestics Society Conference
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    • 2002.12a
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    • pp.198-199
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    • 2002
  • 연자성 재료는 투자율이 높고, 큰 포화자속 밀도를 갖는 재료로서 외부자계에 용이하게 자화되며, 그 용도를 살펴보면 전기에너지 변환, 자기기록. 변압기, 변성기, 각종 코아, 모터, 자기센서, 전ㆍ자계차폐재등 많은 전자기기에 이용되고 있다. 따라서 연자성재료는 기본적으로 결정자기이방성과 자왜가 작아야 한다. 한편 전기, 전자기의 경량화 및 고효율화를 위하여서는 포화자속밀도의 극대화, 고주파영역에서의 우수한 연자기 특성 및 저에너지 손실을 갖는 재료개발이 요구된다. (중략)

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