• Title/Summary/Keyword: 에폭시 함침

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Interfacial Damage Sensing and Evaluation of Carbon and SiC Fibers/Epoxy Composites with Fiber-Embedded Angle using Electro-Micromechanical Technique (Electro-Micromechanical시험법을 이용한 섬유 함침 각에 따른 탄소와 SiC 섬유강화 에폭시 복합재료의 계면 손상 감지능 및 평가)

  • Joung-Man Park;Sang-Il Lee;Jin-Woo Kong;Tae-Wook Kim
    • Composites Research
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    • v.16 no.2
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    • pp.68-73
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    • 2003
  • Interfacial properties and electrical sensing fer fiber fracture in carbon and SiC fibers/epoxy composites were investigated by the electrical resistance measurement and fragmentation test. As fiber-embedded angle increased, the interfacial shear strength (IFSS) of two-type fiber composites decreased, and the elapsed time takes long until the infinity in electrical resistivity. The initial slope of electrical resistivity increased rapidly to the infinity at higher angle, whereas electrical resistivity increased gradually at small angle. Furthermore, both fiber composites with small embedded angle showed a fully-developed stress whitening pattern, whereas both composites with higher embedded angle exhibited a less developed stress whitening pattern. As embedded angle decreased, the gap between the fragments increased and the debonded length was wider for both fiber composites. Electro-micromechanical technique could be a feasible nondestructive evaluation to measure interfacial sensing properties depending on the fiber-embedded angle in conductive fiber reinforced composites.

Pot Life of Structural Adhesives for FRP Composite Used in Strengthening RC Members (구조보강용 FRP 함침·접착수지의 사용가능시간 분석)

  • Choi, Ki-Sun;You, Young-Chan;Kim, Keung-Hwan
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.12 no.3
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    • pp.191-198
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    • 2008
  • Pot life of two-component adhesives such as epoxy resin used in saturating FRP composite is defined as a certain time periods which can guarantee the bond performance and workability of epoxy resin. Therefore, adhesion procedure in strengthening RC members should be completed before chemical hardening is going on at job site. It has been known that there are two types of test method to evaluate the pot life of structural adhesive based on apparent viscosity or temperature change. This study is to verify the test methods how to assess pot life of structural adhesive for FRP composites by means of changing in apparent viscosity and means of exothermic reaction temperature proposed in existing test standards. Results of each test method were compared and analyzed, and reasonable test and evaluation method were suggested.

Hardening properties in MMA monomer using UP and EPS in addition hardener (경화제의 첨가에 따른 UP와 EPS 혼입 MMA 수지의 경화특성)

  • Lee, Jung-Hui;Song, Hun;Chu, Yong-Sik;Lee, Jong-Kyu
    • Proceedings of the Korea Concrete Institute Conference
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    • 2008.11a
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    • pp.445-448
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    • 2008
  • The unsaturated polyester(UP) and epoxy resin have a superior material properties and a chemical resistance using sewerage pipes rehabilitation. However, UP and epoxy have not a low temperatures harding, the requirement $8{\sim}11$ hours long times harding and heating system used by reinforcement liner. This study is to evaluate the effects of low temperature harding properties methyl methacrylate(MMA) monomer using expanded polystyrene(EPS) and UP in addition of initiator and promoters. From the test result, viscosity tends to increase with increasing EPS and UP contents. However, harding time change of the MMA resins which it follows in addition of the initiator and promoter.

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Evaluation of Nondestructive Damage Sensitivity on Single-Basalt Fiber/Epoxy Composites using Micromechanical Test and Acoustic Emission with PZT and PVDF Sensors (PZT 및 PVDF 센서에 따른 음향방출과 Micromechanical 시험법을 이용한 단일 Basalt 섬유 강화 에폭시 복합재료의 비파괴 손상감지능 평가)

  • Kim, Dae-Sik;Park, Joung-Man;Jung, Jin-Kyu;Kong, Jin-Woo;Yoon, Dong-Jin
    • Composites Research
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    • v.17 no.4
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    • pp.61-67
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    • 2004
  • Nondestructive damage sensitivity on single-basalt fiber/epoxy composites was evaluated by micromechanical technique and acoustic emission (AE). Piezoelectric lead-zirconate-titanate (PZT), polyvinylidene fluoride (PVDF) and poly(vinylidene fluoride-trifluoroethylene) (P(VDF-TrFE)) copolymer were used as AE sensor, respectively. In single-fiber composite, the damage sensing with different sensor types were compared to each other. Piezoelectric PVDF polymer sensor was embedded in and attached on the composite, whereas PZT sensor was only attached on the surface of specimen. In case of embedded polymer sensors, responding sensitivity was higher than that of the attached case. It can be due to full constraint inside specimen to transfer elastic wave coming from micro-deformation. For both the attached and the embedded cases, the sensitivity of P(VDF-TrFE) sensor was almost same as that of conventional PVDF sensor.

Design of High Speed Composite Air Spindle System (초고속 복합재료 공기정압 주축의 설계)

  • 장승환;이대길;한흥삼
    • Composites Research
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    • v.14 no.1
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    • pp.47-56
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    • 2001
  • In order to enhance high speed stability the composite air spindle system composed of a high modulus carbon fiber composite shaft, powder contained epoxy composite squirrel cage rotor and aluminum tool holder was designed and manufactured. For the optimal design of the composite air spindle system, the stacking sequence and thickness of the composite shaft were selected by considering the fundamental natural frequency and deformation of the system. The analysis gave results that the composite air spindle system had 36% higher natural frequency relative to a conventional air spindle system. The dynamic characteristics of the composite spindle system were compared with those of a conventional steel air spindle system. From the calculated and test results, it was concluded that the composite shaft and the power contained composite rotor were able to enhance the dynamic characteristics of the spindle system effectively due to the low inertia and high speific stiffness of the composite materials.

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Hardening properties of MMA Monomer Using EPS in addition of Initiator and Promoter (개시제 및 촉진제의 첨가에 따른 EPS 혼입 MMA 수지의 경화특성)

  • Lee, Jung-Hui;Song, Hun;Chu, Yong-Sik;Lee, Jong-Kyu
    • Proceedings of the Korea Concrete Institute Conference
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    • 2008.04a
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    • pp.929-932
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    • 2008
  • The unsaturated polyester(UP) and epoxy resin have a superior material properties and a chemical resistance using sewerage pipes rehabilitation. However, UP and epoxy have not a low temperatures harding, the requirement $8{\sim}11$ hours long times harding and heating system used by reinforcement liner. This study is to evaluate the effects of low temperature harding properties methyl methacrylate(MMA) monomer using expanded polystyrene(EPS) in addition of initiator and promoters. From the test result, viscosity tends to increase with increasing EPS contents. However, harding time change of the MMA resins which it follows in addition of the initiator and promoter.

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Interfacial Properties and Stress-Cure Sensing of Single-Shape Memory Alloy (SMA) Fiber/Epoxy Composites using Electro-Micromechanical Techniques (미세역학적 시험법을 이용한 단-섬유 형태 형상기억합금/에폭시 복합재료의 계면특성 및 응력-경화 감지능)

  • Jang, Jung-Hoon;Kim, Pyung-Gee;Wang, Zuo-Jia;Lee, Sang-Il;Park, Joung-Man
    • Journal of Adhesion and Interface
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    • v.9 no.3
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    • pp.20-26
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    • 2008
  • It is well know that the structure of shape memory alloy (SMA) can change from martensite austenite by either temperature or stress. Due to their inherent shape recovery properties, SMA fiber can be used such as for stress or cure-monitoring sensor or actuator, during applied stress or temperature. Incomplete superelasticity was observed as the stress hysteresis at stress-strain curve under cyclic loading test and temperature change. Superelasticity behavior was observed for the single-SMA fiber/epoxy composites under cyclic mechanical loading at stress-strain curve. SMA fiber or epoxy embedded SMA fiber composite exhibited the decreased interfacial properties due to the cyclic loading and thus reduced shape memory performance. Rigid epoxy and the changed interfacial adhesion between SMA fiber and epoxy by the surface treatment on SMA fiber exhibited similar incomplete superelastic trend. Epoxy embedded single SMA fiber exhibited the incomplete recovery during cure process by remaining residual heat and thus occurring residual stress in single SMA fiber/epoxy composite.

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Importance of Impregnation and Polishing for Backscattered Electron Image Analysis for Cementitious Self-Healing Specimen (시멘트계 자기치유 시편에 대한 반사전자현미경 이미지 분석을 위한 함침과 연마의 중요성)

  • Kim, Dong-Hyun;Kang, Kook-Hee;Bae, Seung-Muk;Lim, Young-Jin;Lee, Seung-Heun
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.5 no.4
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    • pp.435-441
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    • 2017
  • Studies on self-healing have currently been diversified and the methods to evaluate the studies have become more diversified as well. Among them, the back-scattered electron (BSE) image acquired through the scanning electron microscope (SEM) is attempted as the means to evaluate the self-healing effect on cracks. In order evaluate by the BSE image, sophisticated pre-processing of specimen is critical and this injected inside the particle, pore and artificial crack of the hardener to stabilize the structure of the newly generated self-healing product and it enables to endure the stress on polishing without deformation. The impregnated specimen smoothen the surface to obtain the BSE image of high resolution that polishing is made for diamond suspension for wet polishing after dry polishing. As a result of evaluating the self-healing product on the impregnated and polished self-healing specimen, the generated product is formed from the surface of the artificial crack and the self-healing substances are confirmed as $Ca(OH)_2$ and C-S-H.

Experimental and Numerical Studies on the Flow Characteristics in Resin Transfer Molding Process (수지이동 성형공정의 유동특성에 관한 실험 및 수치모사 연구)

  • 이미혜
    • The Korean Journal of Rheology
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    • v.7 no.2
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    • pp.139-149
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    • 1995
  • 실제 복합재료 제조공정에 널리 이용되는 등방성 탄소섬유직조와 에폭시수지에 대 해서 수지의 유동을 일방향으로 근사하여 비정상상태 투과계수와 모세관압을 측정하는 실험 을 수행하였고 적층된 섬유직조의 기공율, 금형 주입압력 그리고 섬유직조의 적층수에 따른 수지유동특성을 분석하였다. 또한 금형 충전과정에 대한 유동가시화 실험을 수행하여 유동 선단과 충전시간을 측정하였다. 전체 조업압력에 미치는 모세관압의 영향을 규명하기 위해 일정 유입압력에 따른 금형충전과정에 대하여 유한요소/관할부피 방법을 이용한 수치모사를 수행하였다. 함침공정의 수지유동에서 비정상상태 투과계수는 섬유직조의 기공율에 따라 급 격히 증가하였고 에폭시수의 표면장력에 기인한 모세관압은 기공율 감소에 따라 급격히 증 가하였다. 동일한 기공율에서 섬유직조의 적층수가 증가함에 따라 투과계수와 모세관압은 모두 증가하는 경향을 보였다. 또한실험에서 측정한 모세관압을 고려하여 유동선단과 금형 충전시간을 수치모사방법으로 예측ㄷ한 결과는 유동가시화 실험에의한 결과와 잘 일치함을 보였다. 이결과로부터 낮은 압력에서 조업하는 RTM공정에서 모세관압효과는 유동선단과 금형 충전시간을 예측하는데 기여함을 알수 있다.

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Wettability Evaluation of Resin on the Glass Fabric (유리섬유직물에 대한 수지의 젖음성 평가)

  • Han, Seung-Wook;Choi, Nak-Sam;Lee, Min-Soo;Ahn, Hung-Kun
    • Composites Research
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    • v.24 no.2
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    • pp.30-37
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    • 2011
  • Analysis of wettability between epoxy resin and glass fabric was studied. The mixing ratios of epoxy resin and anhydride hardener were varied as 1:0.5, l:l and l:1.2. Catalyst content was fixed as 0.1wt% of the mixed resin. A curing analysis by differential scanning calorimeter(DSC) showed a possible impregnation of the mixed resin at the room temperature. An effective contact angle of the mixed epoxy resin drop onto the glass fabric being preset on a flat glass plate was measured as a function of time. The wet area of the epoxy resin drop was also measured. Behaviors of the contact angle, the droplet height, the neat wet area and the coefficient of wettability were used to evaluate the wettability of the epoxy resin onto the glass fabric. It was concluded that the equivalent ratio of 1: 1.2 was the most suitable for the wettability.