• Textile Coloration and Finishing
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• v.3 no.3
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• pp.44-56
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• 1991

진공하에서 일어나는 glow 방전을 이용해서 행하는 plasma 반응은, 표면 특이적(Surface specific)인, 또는 비파괴적인 처리공정(Non-destructive process) 으로서 주목되고 있는 기술이다. 전반은 plasma chemistry로서, 섬유가공의 기초가 되는 plasma를 이용한 반응에 대하여 정리한다. 또 다음 후반에는 섬유가공에 관한 응용예에 대해서, 특히, 최근 실용화를 이룩하고 있는 일본에 있어서의 plasma 응용의 연구개발들, polyester 섬유염색물의 농색화가공, 양모직물의 방축가공 등의 기술동향 및 실용화를 위한 장치개발 등을 소개코자 한다.

• Journal of the Korean Society of Clothing and Textiles
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• v.33 no.7
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• pp.1121-1127
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• 2009

This study presents an eco-friendly and one-step finishing method for modifying fiber property that reduces fiber damage in wool/polyester blend fabrics. Lipase from aspergillus oryzae is used in this experiment. The enzymatic treatment condition is optimized by measuring the relative activity of lipase depending on pH level, temperature, concentration of lipase, and treatment time. The concentration of $CaCl_2$as an activator is determined by the characteristics including whiteness, water contact angle (WCA), and dyeing property. The modified properties of lipase treated fabrics are tested for pill resistance and surface morphology. The results are described as follows: the optimum condions for lipase treatment constitute a pH level of 8.0, treatment temperature of 40$^{\circ}$$_C$, concentration of lipase at 100% (o.w.f), and a treatment time of 90 minutes. $CaCl_2$helps in raising lipase activation, and the optimum concentration is 50mM. The whiteness, wet ability, and pill resistance of lipase treated fabrics improves as compared to the control. The dyeing property of lipase treated fabrics improved by 53.5% after using the one-bath dyeing method. This means that lipase treatment can save time and cost during the dyeing process since lipase treatment modifies wool and polyester fibers. The surface of lipase treated wool fibers do not exhibit any change, however voids and cracks manifest on the surface of lipase treated polyester fibers.

• Journal of the Korean Society of Clothing and Textiles
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• v.33 no.2
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• pp.213-221
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• 2009

This study provides the optimum papain treatment method and its effect on wool/polyester blend fabrics. The enzymatic treatment condition is optimized depending on its pH level, temperature, concentration of enzyme, treatment time and concentration of activators. The characteristics of samples treated with the papain are measured using weight loss, tensile strength, whiteness, WCA, dyeing property and surface micrographs. The results are described as follows: According to measuring weight loss, tensile strength and whiteness, a pH level of 7.5, $70^{\circ}C$, 10% papain(o.w.f.) and 60minutes of treatment time are optimized for papain treatment. L-cysteine and sodium sulfite are able to activate the papain. The optimum concentrations of them are 10mM and 50mM respectively. The WCA of fabrics is decreased since papain treatment makes wool/polyester blend fabrics more hydrophilic. Scouring with papain treatment improves whiteness and dyeing property of fabrics. The dyeing property of papain-treated fabrics is enhanced simply by a single step dyeing process using a basic dye. The surface of wool treated with papain in the presence of L-cysteine shows to be descaled. The surface of wool fibers in the presence of sodium sulfite, however, shows it is hydrolyzed evenly instead of being descaled. The surface of papain treated polyester fibers shows cracks and voids.

• The Research Journal of the Costume Culture
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• v.28 no.5
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• pp.669-676
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• 2020

The purpose of this research was to revive the bathochromic effects of wool fabrics by using natural dyestuffs with minimum heavy metallic mordants. The natural dyestuffs used in this research were the indigo plant, Phellodendron amurense, and Caesalpinia sappan. Sample no. 1 was pre-dyed five times with indigo. Sample no. 2 was pre-dyed five times with indigo and then once dyed with Phellodendron amurense. Following the same method as sample no. 2 with an additional Phellodendron, Sample no. 3 consisted of a pre-dye five times with indigo and twice with Phellodendron amurense. Sample no. 4 was pre-dyed six times with indigo and then once dyed with Caesalpinia sappan. Sample no. 5 followed the same method as no. 4 with an additional dye of Caesalpinia sappan. Sample no. 6 was pre-dyed five times with indigo and then once dyed with Phellodendron amurense and once dyed with Caesalpinia sappan. The results were as follows: first, all samples showed deeper colors. Second, according to the results of the surface K/S measurement, the surface K/S of wool fabrics was >20. Third, the results of lightfastness measurement showed superiority over grade 4 in samples no. 1, 2, 3, 5, and 6. However, sample no. 4 was grade 3. In the colorfastness to washing measurement, sample no. 2 showed greater superiority than grade 3-4, while samples no. 1 and 3 were grade 3. In addition, the colorfastness to dry cleaning for all samples was satisfactory or excellent by more than grade 3.

• Journal of the Korean Society of Clothing and Textiles
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• v.32 no.9
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• pp.1461-1466
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• 2008

This study provides effects of mixed activators on enzymatic activation and determines optimum mixture ratio for enzymatic treatment. Wool 80% and polyester 20% blend fabric and papain from carica papaya are used in this experiment. L-cysteine and sodium sulfite are used as activators for papain treatment process. The treatment condition is pH 7.5, $70^{\circ}$, papain concentration 10%(o.w.f), 60 minutes. L-cysteine and sodium sulfite are added in enzyme solution with various concentrations($0{\sim}50mM$). The optimum treatment condition is determined by measuring weight loss, tensile strength, whiteness, water contact angle(WCA), dyeability and surface micrographs. The results are as follow; The optimum mixture ratio of activators is L-cysteine 2mM and sodium sulfite 10mM. Mixed activators assists in improving the activation of papain. WCA of papain treated fabrics is decreased since papain treatment with activator mixture makes wool polyester blend fabrics more hydrophilic. Dyeing property of papain-treated fabrics more improves by the treatment with mixed activators than with single activator. It means that this method can save time and lower cost. After papain treatment in the presence of mixed activator, the surface of fabrics is modified. The surface of wool fiber shows to be descaled and hydrolyzed, and that of polyester fiber shows to be cracked.

• Journal of the Korean Society of Clothing and Textiles
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• v.36 no.2
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• pp.127-137
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• 2012

This study focuses on the optimal washing conditions for dry cleaning recommended fabrics to minimize dimensional changes using wet cleaning. We suggest water-based alternatives to a perchloroethylene based cleaning process. Wool and rayon fabrics were laundered under various washing conditions and then air-dried for 24hrs. All specimens were extended after spinning and shrunk after drying. This is probably because the fibers were swollen and extended by wetting. The wool fabrics were shown to be acutely influenced by washing temperature and mechanical force. The optimal washing conditions for wool fabric to minimize the dimensional change implied a normal washing temperature and minimized mechanical force. For rayon specimens, dimensional change by a hand wash showed a remarkable decrease compared with a machine wash. Rayon fabric seemed to be influenced by the quantity of water contained in the fabric after spinning and washing time. Therefore, the desirable washing conditions for rayon fabric are to reduce the time required for washing and to increase the spin speed.

• The Research Journal of the Costume Culture
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• v.13 no.2 s.55
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• pp.248-254
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• 2005

In this study, wool fabric specimens were pre-mordanted using Sn, Al, Cu, Cr, and Fe, and subsequently dyed using cochineal, maintaining the pH of the dye bath constant using pH buffer solutions of 4, 5, 6, 7, and 8. In the case of wool fabric specimen, regardless of the type of mordanting agents, peak dye-uptake amount was obtained at the acidic region, pH 4, and above pH 6, the dye-uptake amount decreased remarkably. Differing from the cotton fabric case, the dyed wool fabric specimen exhibited red shade even in the case of non-mordanting, at the region of pH values of 4 and 5. It is presumed that in the acidic dye bath the effect of cationic amine group present in the structure of wool fiber molecules took place. The amount of color difference, among the mordanting agents, due to the increase of pH value, was highest for the Fe mordanting case. It seems, therefore, that the Fe mordanting is affected most by the pH value.

• Textile Coloration and Finishing
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• v.13 no.3
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• pp.155-164
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• 2001

Textile wet-processing industry usually five rise to environmental pollution problems caused by using chemical substance. The objective of this study is to apply enzymes for wool and reduce the environmental problems. Three commercial protein degradation enzymes and a cellulose degradation enzyme as a reference were treated to prevent the shrinkage of wool fabric on laundering. Shrink resistant effects used change with the kinds of enzyme, the amount of enzyme, assistant chemicals, and the pre-treatment condition of wool fabric. When pre-treated with corona before enzyme treatment under ultrasonic condition, the weight loss was increased and strength was decreased and elongation was increased. Both corona pre-treatment and the addition of $Na_2SO_4$ also decreased shrinkage of wool fabrics on laundering. The existence of assistant chemicals increased alkali solubility of wool fabrics.

• Textile Coloration and Finishing
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• v.3 no.2
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• pp.1-9
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• 1991

In order to improve the shrink resistance of wool, the fabric was treated with D.C.C.A.(Di-chloro Isocyanuric Acid) and Hercosett. The results obtained as follows, 1. The optimum condition for the shrink resistance of wool fabric was Hercosett concentration of about 2.0~2.5%(o.w.f), pH of 7, the curing temperature of about $140^{\circ}C$, and curing time of 3 minutes. 2. The physical properties with the experimental conditions, such as the tensile strength, bending strengh, crease recovery, tearing strengh were confirmed by measurements.

• Fashion & Textile Research Journal
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• v.6 no.2
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• pp.239-244
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• 2004

On the whole the various medium colors were developed by repeat dyeing with different colorants after dyeing with one colorant in case of natural dyeing. In this study, in order to obtain various colors on wool fabrics with Gardenia and Sappan wood colorants, pre-mordanting and combination dyeing were carried out. Gardenia and Sappan wood used as natural colorants for combination dyeing showed good miscibility in dye bath, Metal compounds containing alum, copper and iron were used for pre-mordants. The various medium colors such as yellow-red were obtained according to various metal compounds for pre-mordants and various mixing portion of these natural colorants. The surface reflactance spectra and color characteristics of wool fabrics by mordanting and combination dyeing were investigated.