• Title/Summary/Keyword: 액체질소 냉각

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A Preliminary Study of Low Temperature Condition by Heat Exchanger (열교환기를 이용한 저온 환경 구축에 대한 기초 연구)

  • Lee, Yang-Suk;Yang, Jae-Joon;Kim, Yoo;Ko, Young-Sung;Lim, Byeung-Jun
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2007.11a
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    • pp.23-26
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    • 2007
  • A preliminary, study of low temperature condition was performed to simulate high altitude condition. The mixed air temperature were investigated at various condition by experiments using cryogenic air by heat exchanger and normal temperature air. An experimental setup was constructed to simulate low temperature condition with liquid nitrogen. To control mass flow rate, orifice and pressure regulators were used. The experimental results show that the mixed air temperature increases linearly with mass flow rate of normal temperature air. Therefore it can be help to simulate a low temperature condition of high altitude.

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Liquid-free milling to prepare a cocrystal of ibuprofen and nicotinamide (액체 첨가가 없는 밀링법을 이용한 ibuprofen과 nicotinamide의 공결정 형성)

  • Ham, Jinok;Jang, Jisun;Kim, Il Won
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.26 no.6
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    • pp.232-237
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    • 2016
  • Cocrystallization of active pharmaceutical ingredients has been widely recognized as a versatile tool to regulate the physical properties of pharmaceutical compounds through designed crystal structures. Grinding or milling has been especially useful to screen the feasibility of cocrystal formation, and the addition of a small amount of liquid is routinely necessary. In the present study, the effect of temperature was studied for the milling cocrystallization of ibuprofen and nicotinamide to establish a liquid-free method. The milling-induced cocrystallization was more effective with liquid nitrogen cooling than at room temperature, which was confirmed by XRD and DSC analyses. This behavior was attributed to the limited molecular mobility below the glass transition temperatures of the cocrystal components, which made it effective to destruct the crystals of raw materials and consequently form the ibuprofen/nicotinamide cocrystal. Further studies would be necessary to establish the utility of the current conclusion to the field of pharmaceutical crystallization.

A Study on Pyrolysis of Cellulosic Organic Solid Wastes (셀룰로오스질 유기고형폐물의 열분해에 관한 연구)

  • Park Nae Joung
    • Journal of the Korean Chemical Society
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    • v.21 no.4
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    • pp.293-303
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    • 1977
  • Cellulosic organic solid wastes such as bark and sawdust, and filter papers as a pure cellulose were pyrolyzed at $300^{\circ}C$ under nitrogen current and mixed current of nitrogen and air. Amounts of condensates collected in air, water, and dry ice-acetone cooling traps, noncondensable gases, and carbonized residues were surveyed. The components of volatile liquids condensed in dry ice-acetone trap were separated by means of gas chromatograph and identified by retention times and syringe reactions. Pyrolysis under nitrogen current produced 13.4∼29.6${\%}$ of tar, 0.01∼0.12${\%}$ of aqueous liquids, 0.24∼1.43${\%}$ of volatile liquids, 9.84∼42.41${\%}$ of noncondensable gases, and 44.0∼65.81${\%}$ of carbonized residues. Pyrolysis under mixed current decreased tar and condensable liquids, but increased noncondensable gases.Volatile liquids collected under nitrogen current separated into the same 19 components by Porapak Q column regardless of the materials and only difference among materials was relative amounts of components. Volatile liquids collected under mixed current separated into six components and mainly lower molecular weight compounds such as methanol and formaldehyde were produced. According to the retention times and syringe reactions, methanol, formaldehyde, acetone, acetaldehyde, acetic acid, and three other compounds presumably containing hydroxyl group in the molecular structure were identified out of 19 compounds.

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Temperature Distribution of Liquid Nitrogen Jet at Sub- and Supercritical States (아임계 및 초임계에서 액체 질소 분류의 온도 분포)

  • Lee, Hyunchang;Kim, Haisol;Cho, Seongho;Sung, Hong-Gye;Yoon, Youngbin
    • Journal of the Korean Society of Propulsion Engineers
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    • v.22 no.1
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    • pp.1-6
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    • 2018
  • Temperatures of cryogenic nitrogen jet inside an injector and at three different downstream positions (0.9, 10.6, and 28.1d) were measured with thermocouples in sub- and supercritical states. The jet temperature decreased while cooling the supply line and injector. The jet experienced from flash boiling, boiling and then no boiling according to decreasing temperature. As an analogy to flash-boiling at the subcritical state, pseudo-flash boiling has been assumed considering the existence of pseudo-boiling at the supercritical state. By showing an area where the temperature did not increase downstream, the plausibility of pseudo-flash boiling is proposed.

A $LN_2$-cooled, Broadband cw CO Laser (액체질소 냉각형광대역 cw CO 레이저)

  • Kim, Y.P.;Choi, J.W.;Won, J.W.
    • Proceedings of the KIEE Conference
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    • 1989.07a
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    • pp.667-671
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    • 1989
  • The CO laser is one of powerful light source for laser magnetic resonance spectroscopy in the mid-infrared region of the spectrum because of its wideband operational characteristics. In this work, a liquid nitrogen cooled cw CO laser is developed to allow broad-band operation from 5 to 8 ${\mu}m$. The design details will be presented.

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Development of bearing/sealing test facility for turbopump system (터보펌프 시스템용 베어링/실 시험설비 개발)

  • 우관제;김경호;우유철
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2003.10a
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    • pp.25-28
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    • 2003
  • The bearing/sealing test (BST) facility is intended for tests of bearing and seal for turbopump of liquid rocket engine (LRE) in various media (water, liquid nitrogen, liquid oxygen). The bearing test for serviceability is fulfilled with the estimation of the flow rate of cooling medium through the test bearing separator and with the simulation of axial and(or) radial loading. The purpose of seals test is the determination of magnitude of leakages through the seal and a time variation of this magnitude.

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PROTOTYPE DEVELOPMENT OF CCD IMAGING SYSTEM FOR ASTRONOMICAL APPLICATIONS (천문관측용 극미광 영상장비 시험 모델 개발)

  • Jin, Ho;Han, Won-Yong;Nam, Wuk-Won;Lee, Jae-Woo;Lee, Seo-Gu;Lee, Woo-Baik
    • Journal of Astronomy and Space Sciences
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    • v.14 no.2
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    • pp.259-268
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    • 1997
  • We present the development process of a prototype CCD imaging system which is being built at Korea Astronomy Observatory(KAO) for astronomical applications. The CCD imaging system requires very low noise and high stability characteristics and is widely used for astronomical purposes from infrared to ultraviolet wavelength regions. However its system design, particularly for the controller design technique, as heart of the system, is not secured in Korea so far. The prototype electronics developed in this study consists of a signal chip controller which was implemented in an EPLD(Erasable Programable Logic Device) and an analog driver, a video processor with a LN2 cooling cryostat. A PC system was employed to control the whole system and to store the image data considering compatibility of the system. We have successfully obtained the first image in the laboratory with the prototype of this imaging system, and an image of the M15 at Sobaeksan Astronomy Observatory.

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An Analysis of Heat Transfer and Pressure Drop Characteristics for Optimum Design of Cryogenic Heat Exchanger used for Liquid Nitrogen Cooling (액체질소 냉각용 극저온 열교환기의 최적설계를 위한 열전달 및 압력강하 특성 분석)

  • Ko, Ji Woon;Jeon, Doong Soon
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.30 no.1
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    • pp.24-32
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    • 2018
  • In this paper, analytical studies were conducted to obtain optimal design factors and analysis parameters of liquid nitrogen cooling exchanger applied in cryogenic refrigerator. The target value of heat transfer rate was more than 1 kW and pressure drop was less than 40 kPa. Design factors of cryogenic heat exchanger included width of channel and configuration of paths. Analytical factors of liquid nitrogen cooling exchanger included temperatures of coolant header surface and inlet liquid nitrogen. The width and number of channels in the design parameters were 0.0050~0.0150 m and 4~8, respectively. The configuration of channel path was 4 ways. Temperatures of coolant header surface and inlet liquid nitrogen in analytical parameters were 74 to 78K and 82 to 86K, respectively. As result, the design factor and analysis parameter satisfying the target values were obtained. The biggest heat transfer rate was 1.36 kW with pressure drop of 32.26 kPa.