• Title/Summary/Keyword: 압출공정

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Fabrication and Property Evaluation of Tubular Segmented-in-Series Solid Oxide Fuel Cell (SOFC) (세그먼트 관형 SOFC의 제작 및 특성 평가)

  • Yun, Ui-Jin;Lee, Jong-Won;Lee, Seung-Bok;Lim, Tak-Hyoung;Park, Seok-Joo;Song, Rak-Hyun;Shin, Dong-Ryul;Han, Kyoo-Seung
    • Korean Chemical Engineering Research
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    • v.50 no.3
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    • pp.562-566
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    • 2012
  • A novel design of tubular segmented-in-series(SIS) solid oxide fuel cell (SOFC) sub module was presented in this paper. The tubular ceramic support was fabricated by the extrusion technique. The NiO-YSZ anode and the yttria-stabilized zirconia (YSZ) electrolyte were deposited onto the ceramic support by dip coating method. After sintering at $1350^{\circ}C$ for 5 h, a dense and crack-free YSZ film was successfully fabricated. Also, the multi-layered cathode composed of LSM-YSZ composite, LSM and LSCF were coated onto the sintered ceramic support by dip coating method and sintered at $1150^{\circ}C$. The performance of the tubular SIS SOFC cell and sub module electrically connected by the Ag-glass interconnect was measured and analysed with different fuel flow and operating temperature.

고강도 및 파괴인성을 갖는 AI-Li-Cu 합금 개발

  • Kim, Song-Hui;Yun, Yeo-Beom;Hwang, Yeong-Hwa;Choe, Chang-U;Hong, Jun-Pyo;Lee, Eung-Jo
    • Korean Journal of Materials Research
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    • v.3 no.3
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    • pp.253-260
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    • 1993
  • High strength and fracture toughness of Al-Li-Cu alloy(2090 Al alloy) have been achieved by the improvement of melting and casting, extrusion and heat treatment techniques. To establish the sucessful process for semi-industrial scale ingot(20Kg) the following areas have been investigated: (1) Improvement of melting and casting techniques for ingot by introducing atmospheric modifications, vacuum and rotary degassing, and deslagging. (2) The effect of heat treatment on mechanical properties (3) Mechanical characterization by tensile test, fracture toughness test and fatigue crack propagation test. High mechanical properties were found to be intimately related with ingot soundness. Tensile strength of final products varied from 534MPa to 566MPa in peak aged condition while elongation/ductility ranged from 9.0% to 11.9%. From the fracture toughness test with using compact tensile specimen, plane strain fracture toughness($K_{Ic}$) appeared to be 39MPa${\surd}$m in peak aged condition and 23MPa${\surd}$ m in underaged condition. When load ratios of 0.1, 0.3 and 0.5 were given ${\Delta}K_{th}$ was 6.0MPa${\surd}$ m, 5.3MPa${\surd}$ m and 4.3MPa${\surd}$ m respectively.

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Vitamin Retention in Rice Bran during Extrusion Cooking (Extrusion Cooking처리가 미당(米糖)에 함유하는 비타민의 잔존율에 미치는 영향)

  • Kim, Bok-Nam;Cheigh, Hong-Sik;Lee, Kyu-Han
    • Korean Journal of Food Science and Technology
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    • v.18 no.3
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    • pp.187-191
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    • 1986
  • Vitamin retention in rice bran during the extrusion cooking adapted for the rice bran stabilization was studied. The rice bran of different moisture content (9.5% and 15.6%) were extruded with cooking extruder (screw dia: 100mm. strew rpm:900. L/D ratio: 10.0) under the given conditions of specific power consumption(42.1 67.9 W/Kg) and extrusion temperatures $(99-135^{\circ}C)$. The affected retention rates of thiamine, riboflavin and niacin in extruded rice bran were determined. The extruded rice bran with higher moisture level had a lower or similar vitamin retention rate at lower specific power consumption and extrusion temperatures, relatively. The vitamin retention in extruded rice brail with the same moisture level were gradually decreased by the increased specific politer consumption and extrusion temperatures. The vitamin retention of rice bran during the extrusion cooking for the rice bran stabilization were observed as 89.9-97.0% for thiamin, 83.4- 97.3% for riboflavin and 94.0 - 97.7% for niacin, respectively.

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Effect of Alkali Treatment Method and Concentration of Rice Straw on the Flexural Properties and Impact Strength of Rice Straw/Recycled Polyethylene Composites (볏짚/재활용폴리에틸렌 복합재료의 굴곡특성 및 충격강도에 미치는 볏짚의 알칼리처리 방법 및 농도의 영향)

  • Lee, Ki Young;Cho, Donghwan
    • Journal of Adhesion and Interface
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    • v.20 no.3
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    • pp.87-95
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    • 2019
  • In the present study, the effect of alkali treatment of rice straw on the flexural properties and impact strength of rice straw/recycled polyethylene composite was investigated. Alkali treatments were performed by means of two different methods at various sodium hydroxide (NaOH) concentrations. One is static soaking method and the other is dynamic shaking method. The composites were made by compression molding technique using rice straw/recycled polyethylene pellets produced by twin-screw extrusion process. The result strongly depends on the alkali treatment method and concentration. The shaking method done with a low concentration of 1 wt% NaOH exhibits the highest flexural and impact properties whereas the soaking method done with a high concentration of 10 wt% NaOH exhibits the highest properties, being supported qualitatively by the fiber-matrix interfacial bonding of the composites. The properties between the two highest property cases above-described are comparable each other. The study suggests that such a low concentration of 1 wt% NaOH may be used for alkali treatment of natural fibers to improve the flexural and impact properties of resulting composites, rather than using high concentrations of NaOH, 10 wt% or higher. Considering of environmental concerns of alkali treatment, the shaking method is preferable to use.

Mechanical Characteristics and Microstructures of Hypereutectic Al-17Si-5Fe Extruded Alloys Prepared by Rapid Solidification Process (급속응고법으로 제조한 과공정 Al-17Si-5Fe 합금 압출재의 미세조직 및 기계적 특성)

  • KIM, Tae-Jun;LEE, Se-dong;BECK, Ah-Ruem;KIM, Duck-Hyun;LIM, Su-Gun
    • Journal of Korea Foundry Society
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    • v.39 no.2
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    • pp.26-31
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    • 2019
  • In this study, the mechanical characteristics and microstructure of hypereutectic Al-17Si-5Fe extruded alloys prepared by a rapid solidification process (RSP) were investigated. The hypereutectic Al alloy was fabricated by means of RSP and permanent casting. For RSP, the Al alloy melted at $920^{\circ}C$, cooling the specimens at a rate of $10^6^{\circ}C/s$ when the RSP was used, thus allowing the refining of primary Si particles more than when using permanent casting, at a rate of about 91%. We tested an extrusion RSP billet and a permanent-cast billet. Before the hot-extrusion process, heating to $450^{\circ}C$ took place for one hour. The samples were then hotextruded with a condition of extrusion ratio of 27 and a ram speed of 0.5 mm/s. Microstructural analyses of the extruded RSP method and the permanent casting method were carried out with OM and SEM-EDS mapping. The mechanical properties in both cases were evaluated by Vickers micro-hardness, wear resistance and tensile tests. It was found that when hypereutectic Al-17Si-5Fe alloys were fabricated by a rapid solidification method, it becomes possible to refine Si and intermetallic compounds. During the preparation of the hypereutectic Al-17Si-5Fe alloy by the rapid solidification method, the pressure of the melting crucible was low, and at faster drum speeds, smaller grain alloy flakes could be produced. Hot extrusion of the hypereutectic Al-17Si-5Fe alloy during the rapid solidification method required higher pressure levels than hot extrusion of the permanent mold-casted alloy. However, it was possible to produce an extruded material with a better surface than that of the hot extruded material processed by permanent mold casting.

A Study on Clogging during Installation of Compaction Pile (다짐말뚝 시공 시 공극 막힘 현상 분석 연구)

  • Choi, Jeong Ho;Park, Seong Jin;Choo, Yun Wook;Kim, Il Gon;Kim, Byeong Kyu
    • Journal of the Korean Geotechnical Society
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    • v.38 no.4
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    • pp.33-45
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    • 2022
  • A series of model tests were performed in this study to demonstrate the clogging mechanism created during the installation of a compaction pile to improve soft ground. The application of an air-jet to extrude sand or aggregates from a casing during the installation of a compaction pile imposes a remarkably high-pressure difference between the composite soil layers of clay and sand (or aggregates), resulting in severe clogging. Therefore, a one-dimensional testing system was developed to simulate composite soil layers consisting of clay and sand (or aggregates) and to apply a high-pressure differential at both boundaries, thus replicating the extrusion process used in compaction pile installation. Herein, the performance of two construction materials for compaction piles of crushed stone and grading-controlled aggregates was compared. A series of one-dimensional model tests were performed under multiple pressure settings, with clogging depth and permeability measured in each case. Results indicate that, blinding clogging mechanisms and blocking defined by previous studies were observed for crushed stone, and a new mechanism of "infiltration" was revealed and defined. Whereas, the controlled aggregates performed excellently against clogging because only blinding was observed.

A study on γ-Al2O3 Catalyst for N2O Decomposition (N2O 분해를 위한 γ-Al2O3 촉매에 관한 연구)

  • Eun-Han Lee;Tae-Woo Kim;Segi Byun;Doo-Won Seo;Hyo-Jung Hwang;Jueun Baek;Eui-Soon Jeong;Hansung Kim;Shin-Kun Ryi
    • Clean Technology
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    • v.29 no.2
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    • pp.126-134
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    • 2023
  • Direct catalytic decomposition is a promising method for controlling the emission of nitrous oxide (N2O) from the semiconductor and display industries. In this study, a γ-Al2O3 catalyst was developed to reduce N2O emissions by a catalytic decomposition reaction. The γ-Al2O3 catalyst was prepared by an extrusion method using boehmite powder, and a N2O decomposition test was performed using a catalyst reactor that was approximately 25.4 mm (1 in) in diameter packed with approximately 5 mm of catalysts. The N2O decomposition tests were carried out with approximately 1% N2O at 550 to 750 ℃, an ambient pressure, and a GHSV=1800-2000 h-1. To confirm the N2O decomposition properties and the effect of O2 and steam on the N2O decomposition, nitrogen, air, and air and steam were used as atmospheric gases. The catalytic decomposition tests showed that the 1% N2O had almost completely disappeared at 700 ℃ in an N2 atmosphere. However, air and steam decreased the conversion rate drastically. The long term stability test carried out under an N2 atmosphere at 700 ℃ for 350 h showed that the N2O conversion rate remained very stable, confirming no catalytic activity changes. From the results of the N2O decomposition tests and long-term stability test, it is expected that the prepared γ-Al2O3 catalyst can be used to reduce N2O emissions from several industries including the semiconductor, display, and nitric acid manufacturing industry.