• Title/Summary/Keyword: 압축 물성

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In-situ Stress behavior of Cu thin films during thermal evaporation (열증착법에 의한 구리박막의 실시간 응력 거동연구)

  • Ryu, Sang;Lee, Gyeong-Cheon;O, Seung-Geun;Kim, Yeong-Man
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2007.04a
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    • pp.107-108
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    • 2007
  • 박막형태의 소재는 일반적으로 광 전자 및 소재가 공 관련 산업에서 특수한 기능이 요구되는 부품 제조에 광범위하게 응용되고 있다. 이러한 박막 소재는 물성 면에서 벌크물질일 때의 물성과 매우 다를 수 있는 것으로알려져 있다. 박막에 스트레인이 존재하면 전자의 이동도나 밴드갭 에너지를 변화시켜 줄 수 있으며, 계면의 전위는 소자를 열화 시키는 역할을 하기도 한다. 이러한 이유로 박막 성장 시 실시간으로 스트레인을 관찰하고 이 결과를 실제 제조공정에 피드백 하여, 소자의 신뢰성을 확보하는 노력이 행해지고 있다. 구리박막의 실시간 응력거동은 F.Spaepen에 의해 보고된 초기 압축응력, 인장응력, 2차적으로 나타나는 점진성의 압축응력의 독특한 3단계 응력거동으로 나타나는 것으로 알려져 있으며, 본 실험에서는 박막증착도중 단시간 증착을 중단한 이후 재 증착을 하여 응력거동을 관찰함으로써 독특한 3단계 응력거동의 메커니즘을 알고자 하였다.

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An Experimental Research on the Material Properties of Super Flowing Concrete (초유동 콘크리트의 재료특성에 관한 실험적 연구)

  • 김진근;한상훈;박연동;노재호
    • Magazine of the Korea Concrete Institute
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    • v.8 no.3
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    • pp.135-146
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    • 1996
  • In this study, the properties of super flowing concrete containing fly ash were experimentally investigated and compared with those of ordinary concrete. Tests were carried out on five types of super flowing concrete mixes containing fly ash and three types of ordinary concrete mixes without fly ash. Flow test, 0-funnel test, box test, L type test and slump test were carried out to obtain the properties for flowability and workability of fresh concrete. The mechanical properties of hardened concrete were also investigated in terms of compressive strength, splitting tensile strength, modulus of elasticity, creep and drying shrinkage. In fresh concrete, it was found that super flowing concrete had excellent workability and flowability compared with ordinary concrete, and had self-compactable performance. Super flowing concrete *also had good mechanical properties at both early and late ages with compressive strength reaching as high as 40 MPa at 28 days. The creep deformation of super flowing concrete investigated was relatively lower than that of ordinary concrete, but drying shrinkage was much higher.

The Effect of Mixing Ratio of Blast Furnace Slag and Fly Ash on Material Properties of 80MPa High Strength Concrete with Ternary Cement (고로슬래그와 플라이애시 대체율이 80MPa 3성분계 고강도콘크리트의 재료물성에 미치는 영향)

  • Lee, Bum-Sik;Jun, Myoung-Hoon;Lee, Do-Heun
    • Land and Housing Review
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    • v.3 no.3
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    • pp.287-297
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    • 2012
  • To develop 80MPa-high strength concrete with ternary cement used in OPC, blast-furnance slag, and fly ash, mixing ratio of blast-furnace slag and fly ash was evaluated in material characteristics before and after hardening of the high strength concrete. According to the evaluated results of material characteristics before and after hardening of the high strength concrete, the flowability and long-term compressive strength increase up to 30% mixing ratio of blast-furnace slag and fly ash. Also, it is superior to characteristics of length change and neutralization due to the use of mineral admixture when compared in test sample mixed with OPC. The evaluated results show that material characteristics of the high strength concrete was the most outstanding performance at blast-furnace slag of 25% and fly ash of 15%. The result of this study will be useful for the development of high strength concrete as a substitute of costly silica fume in the near future.

Synthesis of Alumina-Silica ceramic armor materials(I) (알루미나-실리카계 세라믹복합체 방탄재료 연구(I))

  • Kim Cheol-soo;Lee Hyung-Bock
    • Composites Research
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    • v.18 no.6
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    • pp.40-47
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    • 2005
  • In this study, we tried to invent ceramic armor material with brilliant ballistic properties by the silica of the high compression-expansion ratio and based on alumina that has the most economical and higher ballistic efficiency. After we choose three compositions, proper sintering temperature for each composition was decided. After physical/mechanical measurement, we measured ballistic properties about KE(Kinetic Energy, L/D=10.7, tungsten heavy alloy) and HEAT(High Explosive Anti-Tank, K215) projectiles. As a result, $46\%\;Al_2O_3\;-\;51\%\;SiO_2$ of three compositions had the highest ballistic efficiency md better properties than alumina.

Fundamental Properties of Mortar and Concrete Using High Calcium Fly Ash (고칼슘 플라이애시를 활용한 모르타르 및 콘크리트의 기초적 물성)

  • Lee, Min-Hi
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.4 no.3
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    • pp.284-291
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    • 2016
  • To evaluate the properties of inorganic composites using a great quantity of high-calcium fly ash generated in combined heat and power plants, high-calcium fly ash and F-class fly ash commonly used as concrete admixtures were substituted with binding materials to examine changes of fluidity and compressive strength depending on the substitution ratio for each curing temperature. According to the experimental result, CFA-mixed mortar showed a tendency to reduce its flow unlike FFA-mixed mortar as the substitution ratio was increased, but its flow loss showed smaller than FFA as time passed. As a result of examining compressive strength depending on mixing FA, FFA-mixed mortar had an optimum range within 50% when curing at ambient temperature, but it was found that the compressive strength is reduced when mixing CFA. When curing at high temperature, FFA did not relatively have a great effect on the substitution ratio, but CFA could expect a strength enhancement effect compared with 100% of OPC when using within 25% of binding materials.

Reinforced Polymer/Clay Nanocomposite Foams with Open Cell Prepared via High Internal Phase Emulsion Polymerization (고내상 에멀션 중합에 의해 제조된 열린 기공을 갖는 고장도 고분자/점토 나노복합 발포체)

  • Song, In-Hee;Kim, Byung-Chul;Lee, Seong-Jae
    • Polymer(Korea)
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    • v.32 no.2
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    • pp.183-188
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    • 2008
  • Reinforced open cell micro structured foams were prepared by the polymerization of high internal phase emulsions incorporating inorganic thickeners. Organoclays were used as oil phase thickener, and sodium montmorillonite was used as aqueous phase thickener. Rheological properties of emulsions increased as oil phase thickener concentration and agitation speed increased, due to the reduced drop size reflecting both competition between continuous and dispersed phase viscosities and increase of shear force. Drop size variation with thickener concentration could be explained by a dimensional analysis between capillary number and viscosity ratio. Upon the foams polymerized by the emulsions, compression properties, such as crush strength and Young's modulus were measured and compared. Among the microcellular foams, the foam incorporated with an organoclay having reactive group showed outstanding properties. It is speculated that the exfoliated silicate layers inside polystyrene matrix, resulting in nanocomposite foam, are the main reason why this foam has enhanced properties.

Study on the Change of Physical Properties in Polyurethane Foam by NCO index at the Aging Condition (NCO index에 따른 폴리우레탄 폼의 노화 물성변화 연구)

  • Kim, Kwangin;Kim, Sangbum
    • Journal of the Korean Institute of Gas
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    • v.16 no.6
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    • pp.115-122
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    • 2012
  • Polyurethane foams were synthesized with different contents and kinds of catalysts to know change of properties under various NCO index. UTM(universal testing machine), DSC(differential scanning calorimetry), SEM(scanning electron microscope) and FT-IR(Fourier transform spectroscopy) were used for studying the PUF's physical properties change. Compressive strength of PUF increased with increasing contents of catalyst. Glass transition temperature(Tg) and compressive strength of PUF using PC-8 and 33LV catalyst, increased with increasing NCO index at the aging. According to the results of Infrared spectral analysis, reduction of NCO peak was found in gelling catalyst, because unreacted NCO reacted with polyurethane. Although Tg and compressive strength of PUF using TMR-2, unchanged with increasing NCO index at the aging, because trimerization of isocyanate.

Evaluation on Mechanical and Mixing Properties of Ultra-high Strength Concrete with fck=150MPa (150MPa 초고강도 콘크리트의 배합 및 재료역학특성 평가 연구)

  • Kang, Hoon;Ahn, Jong-Mun;Shin, Sung-Woo
    • Journal of the Korea Institute of Building Construction
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    • v.10 no.3
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    • pp.113-120
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    • 2010
  • Ultra-High Strength Concrete (UHSC) demands a clear presentation of its mechanical properties, as distinct from normal strength concrete, and an evaluation of the serviceability of high-rise buildings that use ultra-high strength concrete. Ultra-high strength concrete fck=150MPa was manufactured with pre-mix cement, and an experimental study was conducted to evaluate the mixing properties and compressive strength, with the major variables being unit cement contents, water-binder ratio, and type of pre-mix cement. The test result showed that 150MPa concrete requires about 6~7 minutes of mixing time until each of the materials (ordinary Portland cement, silica fume, blast-furnace slag powder and anhydrite) are sufficiently revitalized. The slump flow of fresh concrete was shown to be about 700~800mm with the proper viscosity. The average value of concrete compressive strength was shown to be about 70% in 7 days, 85% in 14 days, and 95% in 28 days, for 56 days of concrete material age.

Rheological Studies of the Fish Protein upon the Thermal Processing (열처리 공정에 따른 생선단백질의 물성 연구)

  • Kang, Byung-Sun;Kim, Byung-Yong;Lee, Jae-Kwun
    • Korean Journal of Food Science and Technology
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    • v.26 no.2
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    • pp.103-109
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    • 1994
  • Changes in the rheological properties and the linear viscoelasticity of fish protein gel upon the thermal processing were studied by using mathematical models with stress-relaxation data. The linear viscoelasticity of surimi gel was observed in the range of the true strain $0.105{\sim}0.693$ and cross-head speed $50{\sim}250\;mm/min$ applied in this study. The results of the generalized Maxwell analysis showed that the magnitudes of elastic elements $(E,\;E_e)$ were increased, but the viscous element $({\eta}) $was decreased, as the cross-head speeds and strain levels were increased. Compared to the protein gel heated directly at $90^{\circ}C$ without preheating, the protein gel pretreated at $4^{\circ}C$ and $40^{\circ}C$ showed the higher elastic modulus, but showed different trends in the viscous component, depending on the rheological model applied. Thus, the approaching methods and curve fitting of two mathematical models of stress-relaxation to describe the viscoelastic properties of fish protein gel were discussed.

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Morphology and Properties of Microcellular foams by High Infernal Phase Emulsion Polymerization: Effect of Emulsion Compositions (HIPE 중합에 의한 미세기공 발포체의 모폴로지 및 물성: 유화계 조성의 영향)

  • 정한균;지수진;이성재
    • Polymer(Korea)
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    • v.26 no.6
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    • pp.759-766
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    • 2002
  • Regular, spherical and isotropic open-microcellular foams having low density were prepared by the high internal phase emulsion (HIPE) polymerization mainly composed of styrene monomer and water The effects of Polymerization conditions. such as the content of water, divinylbenzene as a crosslinking agent and dodecane as a chain transfer agent, were investigated based on the tell size and foam properties. The microstructural morphology was observed using scanning electron microscopy (SEM) and the compression modulus of the foam was evaluated using compression test. The dropwise feeding of the aqueous phase into the oil phase was more effective than the batch feeding in producing the uniform and stable foam. Agitation speed and surfactant strongly influenced on the cell size and the window size between water droplets. Introduction of chain transfer agent increased the cell size, whereas it decreased the window size. Compression modulus increased with the crosslinking agent, but decreased with the chain transfer agent.