• Korean Journal of Materials Research
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• v.6 no.11
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• pp.1061-1066
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• 1996

RF magnetron reactive sputtering법으로 Fe75.5Zr8.3N16.2/SiO2(250$\AA$) 다층 박막을 FeZrN의 두께를 변화시키면서 제조하고, 제조된 박막을 진공 열처리하여 열처리 온도에 따른 포화자화, 보자력, 고주파에서의 투자율 그리고 열적 안정성을 조사하였다. Fe75.5Zr8.3N16.2/SiO2(250$\AA$) 다층박막은 FeZrN의 두께가 800$\AA$이상일 때 좋은 연자성을 나타내었다. Fe75.5Zr8.3N16.2/SiO2(250$\AA$)다층 박막을 45$0^{\circ}C$로 열처리 했을 때 포화자속밀도(1.08 T), 보자력 0.41 Oe, 1 MHz에서의 실효 투자율은 3000이상의 연자성을 나타내었다. 그 이유는 X-선 회절 분석 결과 열처리에 의해서 ZrN 미결정이 석출하여 $\alpha$-Fe 결정 성장이 억제되어 우수한 연자기적 성질이 나타난다고 판단된다. 이때 $\alpha$-Fe 입자 크기는 40-50$\AA$, ZrN의 입자 크기는 10-15$\AA$이다. 그리고 실효 투자율의 주파수 의존성에서 단층막에서는 5 MHz 이상에서 실효 투자율이 급격히 감소하는 경향을 보였으나, 다층막에서는 40MHz까지 실효 투자율이 1600이 되어 고주파에서의 연자성이 개선되었다.

• Proceedings of the Korean Magnestics Society Conference
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• 2013.05a
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• pp.27-27
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• 2013

• The Journal of the Korea institute of electronic communication sciences
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• v.9 no.8
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• pp.921-926
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• 2014

In this paper, the characteristics of inset fed microstrip antenna loaded with CSLR(complementary single loop resonator) are studied. Effective permeability parameters of the SLR unit cell is retrieved from simulated scattering parameters, and structure parameters of the SLR unit cell are selected so that effective permeability is negative value at the operating frequency. The optimized inset fed microstrip antenna loaded with SLR for a $3{\times}3$ array in the ground plane of a conventional patch antenna is designed and simulation results of return loss and radiation pattern are shown. At resonant frequency 2.82 GHz, the overall dimension of the proposed antenna is reduced by approximately 56.8% compared to the conventional inset fed antenna. Simulation results are obtained by 3D FEM solver(Ansoft's HFSS).

• Journal of the Korean Magnetics Society
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• v.15 no.3
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• pp.191-197
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• 2005

In the fabrication process of Fe-based amorphous alloy powder cores by pulverization of the melt-spun ribbons and cold compaction, the effects of powder preparation method on the magnetic & electric properties, powder shapes and microstructure of cores have been investigated. The powder cores made by using rotor mill showed low effective permeability as compared to the cores prepared by ball milling. However the frequency dependence and quality factor properties were superior in the case of rotor-milling. Further the powders prepared by rotor mill had homogeneous and round shapes through strong shearing in the sieve ring, while the ball milled powders were inhomogeneous and relatively small. The lower permeability of the powder cores fabricated with rotor mill was considered to be due to the high internal stress occurred by very intensive shearing. Moreover the powder cores produced by rotor-milling showed lower core loss and good frequency dependence of effective permeability possibly due to the higher electrical insulation between magnetic particles. The dc bias property of the powder cores made by rotor-milling was better than the one by ball-milling.

• Korean Journal of Materials Research
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• v.6 no.10
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• pp.1043.2-1048
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• 1996

자기기록의 고밀도화로 인해 보자력(Hc)이 큰 자기기록매체가 필요하게 되었다. 고보자력매체에 신호를 충분히 기록하기 위해서는 보다 강한 자장이 필요하다. 이 때문에 포화자화(Ms)가 큰 재료가 필요하며 고주파 영역에서 실효투자율($\mu$eff)이 높아야 한다. Fe계 합금박막은 이에 적합한 재료이다. 본 연구에서는 Fe의 결정자기이방성에 영향을 미치는 Si과 Fe의 격자 변형을 유도할 수 있는 B를 첨가하였다. Fe-B-Si 계 박막을 질소분위기 중에서 RF Matnetron Sputter로 제작하여 연자기적 특성에 관하여 고찰하였다. Fe91.49B4.01Si4.50at% 박막은 35$0^{\circ}C$에서 1시간 열처리를 행함으로써 약 900(10MHz) 정도의 투자율과 7.6Oe의 보자력을 나타냈으며 포화자화는 1300emu/㎤를 얻었다.

• Journal of the Korean Magnetics Society
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• v.6 no.4
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• pp.211-217
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• 1996

The effects of Al addition to Fe-B-Nb-Cu alloy for improving the high-frequency magnetic properties and the magnetic properties of ultrathin $Fe_{78}Al_{4}Nb_{5}B_{12}Cu_{1}$ nanocrystalline alloy ribbons with the thickness less than $10\;\mu\textrm{m}$ were investigated. It was found that the effective permeability at frequencies over- 100 kHz was very high and the core loss was very low for the composition $Fe_{78}Al_{4}Nb_{5}B_{12}Cu_{1}$ alloy. Moreover, the reduction of the ribbon thickness below $10\;\mu\textrm{m}$ was very effective in improving their permeability and the core loss characteristics up to the MHz frequency range. The values of effective permeability at 1 MHz and core loss at 0.2 T, 1 MHz were 5,000 and 1.4 kW/kg, respectively. It was considered that these results were due to far refined $\alpha-Fe$ phase structure with grain size less than 10 nm and domain structure modification.

• Journal of the Korean Magnetics Society
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• v.6 no.5
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• pp.317-322
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• 1996

Thin films of Fe-Zr-N were fabricated by rf magnetron reactive sputtering method. The saturation magnetization and coercivity as functions of annealing temperature and partial pressure of nitrogen gas, effective permeability at high frequencies, and thermal stability were investigated. Magnetic softness was exhibited in the composition range of $Fe_{72-78}Zr_{7-10}N_{15-18}$ which was boundary between polycrystalline and amorphous structure. These films exhibited magnetic softness with saturation magentic flux density of 1.55 T and effective permeability of about 3000 at 1 MHz. These films also exhibited thermal stability by sustaining effective permeability of 2500 or above as the temperature was raised to $550^{\circ}C$. It is asswned that good magnetic softness is obtained because grain growth of $\alpha-Fe$ is prohibited due to the precipitation of ZrN nanocrystals. The grain sizes of $\alpha-Fe$ films were $40~50\AA$ and the grain sizes of ZrN nanocrystals were $10~15\AA$.

• Journal of the Korean Magnetics Society
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• v.14 no.1
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• pp.7-12
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• 2004

The annealing-temperature dependence of magnetic properties in compressed powder cores being composed of ball-milled F $e_{73.5}$C $u_1$N $b_3$S $i_{15.5}$ $B_{7}$ alloy powders (size 250∼850${\mu}{\textrm}{m}$) and 5 wt% of ceramic insulators has been investigated. When annealed at 5$50^{\circ}C$ for 1 h and so transformed to $\alpha$-Fe phase nanocrystalline structure with the grain size of 11 nm (electrical resistivity : 110 $\mu$Ω$.$cm), the highest effective permeability of 125 and quality factor of 53 were obtained, and the permeability persisted up to about 500 KHz. Further the core loss measured at the frequency of 50 KHz and the induction amplitude of 0.1 T was very low (230 mW/㎤). However the dc bias characteristics was not satisfactory as compared to that of conventional powder core materials(MPP, Sendust etc.). The inferior dc bias property of F $e_{73.5}$C $u_1$N $b_3$S $i_{15.5}$ $B_{7}$ alloy powder cores was attributed to the fact that the size of powder was too large for obtaining the same permeability with that of conventional materials.

• Journal of the Korean Magnetics Society
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• v.10 no.5
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• pp.191-195
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• 2000

With the object of developing a non-gap choke core, effects of annealing in oxygen atmosphere on magnetic properties for Fe$_{78}$Si$_{9}$B$_{13}$ amorphous alloy were investigated. After annealing for 2 hrs at 440 $^{\circ}C$, optimum magnetic properties for choke core were obtained, where the effective permeability was 180 and was almost constant up to several MHz, and the decrease in permeability upon large DC bias current of 12 A or DC bias magnetic field of 8,000 A/m was very little. Moreover the AC magnetic loss was very low as compared to the conventional choke cores. Upon the optimum annealing, the magnetic hysteresis loop was inclined accompanying the increase of coercive force and the appearance of fine crystallites of $\alpha$-Fe phase. The good choke core properties was considered to be due to the suppression of domain boundary motion and domain refinement by the crystallites.

• Journal of the Korean Magnetics Society
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• v.8 no.5
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• pp.255-260
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• 1998

Fabrication condition and magnetic properties of ultrathin Co-based amorphous alloy have been investigated. When the ejection gas pressure was lower than 0.05 kgf/$\textrm{cm}^2$ at the roll speed of 55 m/s, ultrathin ribbons with the thickness less than 10 ${\mu}{\textrm}{m}$ were successfully obtained. The ribbon thickness decreased linearly with the decrease in ejection pressure. Moreover the significant decrease in ribbon width was accompanied with the decrease of thickness in the range of ejection pressure to form an ultrathin ribbon. This behavior was attributed to the decrease of effective ejection pressure in the both end-sides of rectangular nozzle due to the larger friction between molten metal and nozzle wall. The effective permeability at low frequency (1 kHz) decreased largely with the decrease in ribbon thickness, while the coercive force increased with the thickness decrease. It was considered that these behaviors were due to the enhancement of surface effect leading to the suppression of wall motion. However effective permeability at high frequency (1 MHz) increased with the decrease in ribbon thickness, and this was ascribed to the easier magnetization rotation owing to the reduction of eddy current.