• Applied Chemistry for Engineering
• /
• v.30 no.5
• /
• pp.615-619
• /
• 2019

Statistical design of experiments was performed to optimize MOF-235 synthesis process. Concentrations of terephthalic acid (TPA), iron (III) chloride hexahydrate, N,N-dimethylformamide (DMF) and ethanol were important factors to develop the crystal structure of MOF-235. MOF-235 was synthesized with various concentrations of the listed chemicals above and the crystallinity was measured by XRD. The effect of the composition on the synthesis of MOF-235 was evaluated using a statistical analysis. For the variance analysis using F-test, the concentration of ethanol showed the greatest effect on the crystallinity and TPA the least influential. A regression model for predicting the crystallinity of MOF-235 was derived and the prediction results for two synthetic variables were presented using contour plots. Finally, the crystallinity was predicted by a mixture method with $FeCl_3$, ethanol and DMF.

• Journal of the Korea Concrete Institute
• /
• v.21 no.6
• /
• pp.745-752
• /
• 2009

This paper presents the optimized mixing design of lightweight aerated concrete using hydrogen peroxide. Design of experiments in order to the optimized mixing design was applied and commercial program (MINITAB) was used. Statistical analysis was used to Box-Behnken (B-B) method in response surface analysis. The influencing factors of experimental are unit cement content, water ratio and hydrogen peroxide ratio. According to the analysis of variance, at the hardened state, water ratio and hydrogen peroxide ratio affects on dried density, compressive strength and bending strength of lightweight aerated concrete, but unit cement content affects on only dried density. In the results of response surface analysis, to obtain goal performance, the optimized mixing design for lightweight aerated concrete using hydrogen peroxide were unit cement content of 800 kg/$m^3$, water ratio of 44.33% and hydrogen peroxide ratio of 10%.

• Proceedings of the Korean Institute of Surface Engineering Conference
• /
• 2013.05a
• /
• pp.130-131
• /
• 2013

최근 연구에서는 상용 통계분석 프로그램인 Minitab을 사용하여 실험 요소 설계 및 최적 공정조건을 구하는데 많이 이용하고 있다. 본 연구에서는 도금 제품의 Peeling 최적화를 위해 도금 전처리 공정인 에칭 및 화학 니켈 공정 시간을 인자로 설정하였다. 또한 2인자 2수준(2 factor 2 Level)의 직교 배열표를 구성하고 도금 제품의 밀착성을 만족하는 범위 내에서 설계변수에 의한 반응표면법(Response surface analysis)을 사용하여 최적 조건을 설정하였다. 실험 결과, 에칭 및 화학니켈 공정 시간의 주효과도에서 에칭 공정시간이 낮을수록, 화학니켈 공정시간이 높을수록 Peeling 값이 향상된다는 결과를 얻었다. 그리고 최적 조건을 도출하기 위한 방법으로 반응표면 설계법 중의 중심합성법을 사용하여 에칭(10min 15sec)및, 화학니켈(10min 15sec)의 최적 공정 시간을 도출하였다.

• The Korean Journal of Applied Statistics
• /
• v.1 no.1
• /
• pp.21-28
• /
• 1987

In agricultural research field experiments are usually conducted with the sam etreatments in the same experimental design over several locations for several years in order to draw widely adaptable results. For generalization of the results from the individual locations and the properties of the treatment responses may be evaluated by carrying out the combined analysis over agricultural climate zones or country level. A method of combined analysis of variance was presented and examined by applying to a set of data obtained from a series of rice variety adaptability trials conducted by Kyung Buk Provincial Office of Rural Developmention 1986.

• Applied Chemistry for Engineering
• /
• v.33 no.4
• /
• pp.402-407
• /
• 2022

Statistical design of experiments was used to optimize the MOF-5 synthesis process. A mixture design was employed to optimize precursor concentration. The optimal composition of three chemical materials, terephthalic acid, zinc acetate dihydrate, and N,N-dimethylformamide for MOF-5 synthesis was determined by extreme vertices design methods as follows; 1 mol : 2.7 mol : 40 mol. A multilevel factorial design was selected to screen the significance of synthesis reaction conditions such as temperature, time, and stirring speed. Statistical analysis results suggested excluding stirring speed from further investigation. Using a central composition design, the synthesis time and temperature were optimized. The quadratic model equation was derived from 13 synthesis experiments. The model predicted that MOF-5 synthesized at 119 ℃ for 10.4 h had the highest crystallinity.

• Proceedings of the Materials Research Society of Korea Conference
• /
• 1999.05a
• /
• pp.57-57
• /
• 1999

핵연료 펠렛제조공정의 단순화를 위하여 분말을 플라즈마로 용융시킨 후 이를 펠렛몰더에 직접 침적시키는 방법으로 핵연료를 제조하고자 하였다. 침적물의 밀도에 미치는 영향을 관찰하기 위하여 쉬스가스 조성, 플라즈마 동력, 챔버내부압력 및 분말 공급량, 입자크기, 분사관 위치, 분사거리 및 쉬스가스조성 등을 변수로 하였다$^{1)}$ . 실험으로 얻어진 결과는 ANOVA(Analysis of Variance)의 통계적 방법으로 각각의 인자가 밀도에 미치는 영향의 크기뿐만 아니라, 두 가지 이상의 인자가 조합되어 나타나는 영향에 대해서도 분석하였다.

• Journal of Korean Society of Environmental Engineers
• /
• v.30 no.8
• /
• pp.781-788
• /
• 2008

This study shows how to find out optimum co-substrate conditions and continuous operating parameters for maximum acidification of three different organic wastes - livestock wastewater, sewage sludge and food waste. Design of experiments and statistical analysis were revealed as appropriate optimization schemes in this study. Analyses of data obtained from batch tests demonstrated the optimum substrate mixing ratio, which was determined by maximum total volatile fatty acids(TVFA) increase and soluble chemical oxygen demand(SCOD) increase simultaneously. Suggested optimum mixing ratio of livestock wastewater, sewage sludge and food waste was 0.4 : 1.0 : 1.1 based on COD, respectively. Response surface methodology(RSM) contributed to find out optimum operating parameter - hydraulic retention time(HRT) and substrate concentration - for the semi-continuous acidogenic fermentation of mixed organic wastes. The optimum condition for maximum TVFA increase was 2 days of HRT and 29,237 mg COD/L. Empirical equations obtained through regression analysis could predict that TVFA increase would be 73%. To confirm the validity of the statistical experimental strategies, a confirmation experiment was conducted under the obtained optimum conditions, and relative error between theoretical and experimental results was within 4%. This result reflects that using statistical and RSM technique can be effectively used for the optimization of real waste treatment processes.

• Journal of Korean Society of Coastal and Ocean Engineers
• /
• v.23 no.2
• /
• pp.163-170
• /
• 2011

An optimal layout condition of the offshore wind turbines is studied by using the response surface analysis which is a kind of the design of experiments. Based on the assumption that total 36 turbines would be installed in the offshore wind farm, the number and distance of the rows and columns are used as the design variables and the efficiency decrease of power generation due to the wake decay by the interactions of turbines and the installation cost of the internal electric grid are considered as the objective functions of the response surface analysis for the layout design of turbines. Useful design information can be derived by analyzing the relationship between the design variables and target functions. It is found that the row number and the distance between rows should be minimized, and the optimal distance between columns should be estimated and adopted to the layout design within the specified design range in order to ensure the economics for the offshore wind farm.

• Journal of the Korea Academia-Industrial cooperation Society
• /
• v.15 no.4
• /
• pp.1819-1824
• /
• 2014

The vacuum-glazing panel is a panel that keeps two glasses completely sealed in a vacuum condition. It is the high function insulation material of having the wall level minimizing the heat loss by the conduction and convection heat transmission coefficient. The edge sealing is a very important process of vacuum glass on the strength, thickness and air tightness. In this study, by using the hydrogen mixture gas torch, two sheets of glass was sealing in the furnace. The thickness and strength of the glass according to the process parameters is measurement and analysis, and predicting the edge sealing strength of glass by using taguchi method of experiment. We verified the validity of the experiment by checking the error rate through additional experiment.

• Transactions of the Korean Society of Mechanical Engineers
• /
• v.17 no.10
• /
• pp.2509-2517
• /
• 1993

Lapping is a very complicated and random process resulting from the variation of abrasive grains in its sizes and shapes and from the numerous factors having an effect on the process quality. Thus it needs to be analyzed by experimental method rather than by theoretical method to obtain the relative effects of factors quantitatively. In this study, cylindrical lapping experiment designed by Taguchi's L8 orthogonal array was performed and analyzed by Yates' ANOVA table. As a result, effective factors and interaction effects were identified and discussed. Also the optimal factor combination to obtain the largest improvement of surface roughness was selected and confirmatory experiments were peformed.