• Applied Microscopy
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• v.29 no.3
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• pp.265-274
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• 1999

The microstructure of Cu thin films in various deposition conditions was characterized. Cr films (50 nm thick) and Cu films (500 or 1000 nm thick) were deposited on polyimide films by DC magnetron sputtering. The Ar pressure during Cu deposition was controlled to 5, 50 and 100 mtorr. The microstructure was characterized using conventional and high resolution SEM and TEM. As sputtering pressure increases, open boundaries are observed more frequently. The Cu film deposited at 5 mtorr has a dense and uniform structure, while low-density regions or open boundaries between columns exist in the film deposited at higher pressure. As the film grows thicker, open boundaries are wider and the density of open boundaries are higher. The comparison between SEM and TEM show that the small features shown in high resolution SEM are grains. High resolution SEM is very effective to characterize the microstructure of the thin films. One column in the films deposited at 50 and 100 mtorr consists of several grains, which are smaller than those deposited at 5 mtorr.

• Composites Research
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• v.33 no.3
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• pp.147-152
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• 2020

In this study, void behavior of composite laminate by local internal pressure gradient due to structural geometry and surface film application condition was experimentally evaluated through fabrication of spar/skin integrated structure specimens. Viscosity comparison and thermal analysis for both carbon fiber prepreg and surface film were conducted and cure characteristic and rate difference were analyzed. 2 types of spar/skin integrated structural specimens were prepared based on different application condition of surface film. Subsequently, those specimens were evaluated through visual surface inspection, non-destructive and destructive inspection. In a specimen #1 with full application of surface film, low pressurized area of composite laminate created by pressure gradient of structural geometry had voids. It exhibited that voids could not be evacuated and were locked in cured laminate by the influence of pre-cured surface film with relatively faster cure rate. In a specimen #2 without surface film, it revealed that all internal voids disappeared in the cured laminate. Therefore, it is verified that surface film acts as barrier film preventing void movement and evacuation during autoclave cure.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.16 no.2
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• pp.82-87
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• 2006

Glassy specimen was obtained by melting and quenching a borosilicate glass frit miked with $10{\sim}80wt%$ EAF dust. The glass transition temperature, $T_g$ of glassy specimen was measured around $550^{\circ}C$ from the DTA curve and the eat treatment condition to crystallize a glassy specimen was selected as $700^{\circ}C$/1 hr. The spinel crystal peaks were found in XRD analysis for the glass containing dust > 70 wt%. For the glass-ceramics, however, the spinel peaks in a specimen containing dust > 40 wt%, and the spinel and willemite peaks in dust > 80 wt%. The crystals of several tens of nanometer with aspect ratio of $0.7{\sim}1.0$ were observed at a glassy specimen containing dust > 40 wt% by SEM which was not found by XRD analysis. For the glass-ceramics, the crystals were found in a specimen containing dust of even 10 wt% by SEM. The feature and distribution of crystals observed through the specimen for a glass-ceramics were diverse and not uniform. The crystals found in the glass-ceramics containing 70 wt% dust were hexahedral with an aspect ratio of around unity.

• Composites Research
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• v.31 no.1
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• pp.1-7
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• 2018

In the case of a conventional composite patch repair using a heat blanket, the adhesive is pressurized using only a vacuum bag. In this study, however, a pressurization system has been developed to apply additional air pressure on the vacuum bag. In order to verify the performance of the developed system, the composite laminates were repaired with scarf patches and then tested under tensile load to be compared with the strength of the defect-free laminate. Tensile tests were also conducted on specimens with the same configuration but bonded in an autoclave. As a result of the test, the tensile strengths of the specimens repaired using the heat blanket with vacuum only without external pressure, the specimens repaired with additional pressure by the developed system, and the specimens repaired with the same external pressure in an autoclave, showed the strength recovery ratios of 74.9, 81.0, and 78.2%, respectively. The results of the tensile test after moisture saturation and the dried fatigue test also showed that the strength recovery ratios of the specimens repaired under the external pressure of 1 atm using the developed system are slightly higher than that of specimens bonded in autoclave.

• Proceedings of the Korea Contents Association Conference
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• 2011.05a
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• pp.535-536
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• 2011

주사전자현미경은 시편의 표면형상을 수 nm의 정밀도로 관찰할 수 있는 측정 장비로, 과학 기술 및 산업 분야에서 널리 사용되고 있다. 이러한 주사현미경은 30여종 이상의 변수조합에 의해 운영되며, 정상적인 영상을 관찰하기 위해서는 변수를 최적화하는 보정작업을 필요로 한다. 본 논문에서는 이러한 보정작업을 용이하게 하기 위한 메타 휴리스틱 기법을 소개한다.

• Transactions of the Korean Society of Mechanical Engineers
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• v.15 no.5
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• pp.1479-1485
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• 1991

본 연구에서는 고차판이론(higher order shear deformable plate theory)을 사용하여 DCB시편을 보형상이 아닌 실제의 얇은 판으로 해석하여 새로운 에너지해방률 식을 제시하고자 한다.한편, 이의 타당성을 입증하기 위하여 Gr/Ep 및 APC-2 복합 재료로 ASTM D30.02 round robin의 제안 방법에 의해 층간파괴인성치를 구하고, 또 이 강용이 제안한 Ae법에 의한 금속의 파괴인성치 결정법을 참고로 하여 미세파괴 초창기 의 층간파괴인성치를 결정하여 이론결과와 비교 검토한다.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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• 1995.06a
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• pp.25-30
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• 1995

본 연구에서는 건식 구름접촉시 발생하는 tribological한 현상들을 plate on ball tester를 이용하여 실험적으로 고찰하였다. 실험의 주된 관심은 각 열처리 방법으로 제작한 시편에 대하여 건식 구름접촉시 cycle수에 따른 plate의 표면 거칠기, 트랙의 형상, 졍도 및 구름저항의 변화이며 이런 자료를 토대로 열처리공정의 차이에서 오는 정도수명 및 피로수명에 대한 상대평가를 통해 마찰, 마멸의 저감에 적합한 열처리방법을 제시하고자 한다.

• Proceedings of the KAIS Fall Conference
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• 2005.05a
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• pp.93-95
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• 2005

와이어 컷 방전가공은 자동운전을 가능하게 한 NC가공 장치를 대표할 만한 가공법이다. 기존 기계가공으로 가공하기 어려운 형상의 제품을 쉽게 제작할 수 있다 그러나 기계가공으로 제작된 금형에 비해 수명이 현저히 저하된다. 이러한 요인은 와이어 컷 방전가공으로 제작된 금형 표면에 가공 변질층이 발생함으로 인한 것으로 사료된다. 이에 본 논문에서는 기계가공과 와이어 컷 방전가공으로 제작된 시편의 가공면 표면 특성을 비교하여 그 요인을 분석하고자 하였다.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2002.05a
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• pp.94-99
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• 2002

KS and ISO have proposed several evaluation methods of conventional machine tools. Even though the accuracy of the tools can be evaluated with these methods, there are still no proper evaluation methods of high speed machining. Because it is hard to evaluate characteristics of high speed machining such as decrease of cutting temperature, cutting force, and reduced machining time. Therefore, new evaluation method for high speed machine should be developed. In this paper, several shapes of model have been proposed to evaluate cutting accuracy of high speed machine.

• Proceedings of the Materials Research Society of Korea Conference
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• 2003.03a
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• pp.210-210
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• 2003

휘스커상의 뮬라이트의 생성온도와 속도는 출발물질로 사용되는 알루미나와 실리카의 화학적 순도, 입자크기 그리고 결정형태에 의존하며, 알루미나와 실리카의 조성비에 따라 생성되는 뮬라이트의 형태가 변한다. 각 원료에 대한 반응성을 관찰하기 위하여 출발원료인 Al(OH)$_3$, 비정질 SiO$_2$, AlF$_3$를 혼합 각각 단일조성과 2상 및 3상의 원료를 혼합 분쇄하여 분무건조한 조립분말을 5$0^{\circ}C$ 구간으로 나누어 상온에서 130$0^{\circ}C$까지 튜브 로에서 열처리하였다. Al(OH)$_3$와 AlF$_3$를 단독으로 열처리하였을 경우에는 안정한 상태로 열처리가 진행되었으나, 혼합하였을 경우에는 40$0^{\circ}C$ 이상의 온도에서 서서히 반응하였다. 각 온도구간에서 열처리한 시편은 미세구조 관찰과 상분석을 통하여 플루오르 토파즈와 휘스커상의 뮬라이트의 생성을 관찰하였으며, 생성된 휘스커 뮬라이트는 조립의 형상을 원형대로 보존하였으며, 조립의 강도를 측정하기 위하여, 초음파 분산기와, 초음파 Homgeniger를 이용하여 처리한 결과 대부분 원래의 형상을 유지하였다.