• Title/Summary/Keyword: 시간 분해 측정

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Preparation of Calcium Powder from Eggshell and Use of Organic Acids for Enhancement of Calcium Ionization (난각칼슘의 제조 조건 및 유기산이 칼슘의 이온화에 미치는 영향)

  • Shin, Hyung-Soon;Kim, Kong-Hwan
    • Applied Biological Chemistry
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    • v.40 no.6
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    • pp.531-535
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    • 1997
  • An efficient process for recovery of calcium from the eggshell was developed and some organic acids were used in an attempt to enhance the degree of calcium ionization. Eggshell membrane was readily separated from crushed eggshell based on the differences in specific gravities. The conditions which allowed most efficient membrane removal were found to be 30 rpm of speed, 30 min of residence time and 0.08 of volume fraction. It took 3 hours for the eggshell powder prepared at $1000^{\circ}C$ to reach L value of 90 with the Hausner ratio being 1.43. The calcium ion concentrations were 990, 3500, 3900 and 4200 ppm in pure water, acetic acid, citric acid and lactic acid$(0.05{\sim}3%)$ aqueous solution, respectively. The degrees of ionization of calcium-citrate-malate complex(CCM), calcium-citric acid complex(CC) and calcium malic acid complex(CM) increased by 4 to 5 times compared to eggshell calcium powder.

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인삼사포닌의 모에 미치는 효과에 관한 연구

  • Kim, Chang-Gyu;Sim, Sam-Ju;Lee, Ok-Seop
    • Journal of the Society of Cosmetic Scientists of Korea
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    • v.7 no.1
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    • pp.1-18
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    • 1979
  • 인삼(人蔘)사포닌으로 처리(處理)한 모발(毛髮)의 인장강도(引張强度)와 신장도(伸張度)를 collagen 가수분해물(加水分解物)로 처리한 모발(毛髮)과 비교(比較)하였다. 모발(毛髮)에 인삼(人蔘)사포닌 흡수량(吸收量)은 high speed liquid chromatography로 측정(測定)하였으며 liquid scintillation counter로 확인(確認)하였다. 모발(毛髮)에 collagen 가수분해물(加水分解物)의 흡수량(吸收量)은 모발(毛髮)을 collagen 가수분해물(加水分解物) 용액(溶液)속에 침적(沈積)시켰을 때 처음 30분(分) 동안은 많은 량(量)의 흡착(吸着)이 일어났으나 1시간(時間) 경과후(經過後)부터는 더 이상(以上)의 증가(增加)는 보이지 않았다. 이와는 반대(反對)로 인삼(人蔘)사포닌의 경우(境遇)는 침적시간(沈積時間)의 증가(增加)에 비례(比例)하여 흡수량(吸收量)의 증가(增加)를 나타내었다. 실험결과(實驗結果)는 인삼(人蔘)사포닌이 collagen 가수분해물(加水分解物) 보다 모발(毛髮)에 더욱 효과적(效果的)임을 보여 주었고, 그리고 인삼(人蔘)사포닌의 모발(毛髮)에 대(對)한 흡수(吸收)와 인장강도(引張强度)의 증가(增加)는 모발(毛髮)의 strain-stress곡선(曲線)과 인삼(人蔘)사포닌의 계면활성(界面活性)에 의(依)해 설명(說明)하였다.

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Study on Physicochemical Properties of Pesticides. (II) Water Solubility, Hydrolysis, Vapor Pressure, and Octanol/water Partition Coefficient of Flupyrazofos (농약의 물리화학적 특성 연구 (II) Flupyrazofos의 수용성, 가수분해, 증기압, 옥탄올/물 분배계수)

  • Kim, Jeong-Han;Kim, Yong-Hwa;Kim, Kyun
    • Applied Biological Chemistry
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    • v.40 no.1
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    • pp.76-79
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    • 1997
  • Several physicochemical properties such as water solubility, vapor pressure, hydrolysis and octanol/water partition coefficient(Kow) of flupyrazofos, the first organophosphorus insecticide developed in Korea, were measured based on EPA and OECD methods. Water solubility was low showing 0.80 ppm at $25^{\circ}C$ and in hydrolysis study, half-life at $25^{\circ}C$ was 266.5 hr(pH 4.0), 180.0 hr(pH 7.0) and 120.9 hr(pH 9.0) demonstrating instability in alkaline solution. At $40^{\circ}C$ hydrolysis rate was $2{\sim}4$ times higher than that at $25^{\circ}C$. The equation log P=0.673-(1565.4/T) was obtained from vapor pressure experiments at three different temperatures (25, 35, $45^{\circ}C$) and $2.81{\times}10^{-5}$ torr was obtained at $25^{\circ}C$. This value is similar to that of diazinon and 1,000 times lower than that of DDVP suggesting it would not give environmental contamination by volatilization. High log Kow(5.24) was observed and this might result in bioconcentration through food chain. However, its possibility is not likely to be high due to its relatively rapid hydrolysis.

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The Effects of Heparin-Coated Circuit on the Total Amount of Heparin During Cardiopulmonary Bypass (심폐기 사용 중에 HCC가 총 Heparin사용량에 미치는 영향)

  • 이현우;이재웅;박철현;박국양
    • Journal of Chest Surgery
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    • v.33 no.12
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    • pp.954-958
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    • 2000
  • 배경: 헤파린표면처리 도관(Heparin-coated circuit: HCC)이 도관과 혈액사이의 반응(Blood-marterial reaction)을 줄여주어서 보체활성화(complement activation), 백혈구활성화(leukocyte activation)와 사이토킨 분비(cytokinerelease)등을 감소시켜 준다. 그러나 HCC가 수술 후에 출혈 양을 줄여주고 헌혈 필요량을 감소시켜 준다는 임상적 효과에 대해서는 인정된 부분이 많으나 아직까지 그 기전은 대부분은 미지의 상태로 남아있는 것이 사실이다. 본 연구는 HCC를 사용한 군(Group H)과 사용하지 않은 군(Group C)간에 심폐기 사용기간(Pumptime), 활성화 응고시간(activated clotting time: ACT)과 헤파린 사용량을 비교 분석해 봄으로서 두 군간에 존재할 수 있는 헤파린 사용량을 비교 분석해 본으로서 두 군간에 존재할 수 있는 헤파린 사용량 차이에 대하여 알아보려고 하게되었다. 대상 및 방법: 본원에서 1999년 5월 1일부터 동년 12월 31일 사이에 연령이 16세 이상인 환자에서 HCC를 사용했던 16명(Group H)과 사용하지 않았던 19명(Group C)을 대상으로 하였다. 모든 환자에서 수술 전 체중, 신장, 체표면적, 심폐기 사용시간(pumptime), 수술 중 최저체온, 대동맥 차단시간(Aortic cross clamping time. ACC time), ACT, 헤파린 및 프로타민 사용 양 등을 조사하였다. 결과: 연구대상 환자의 연령, 체중, 신장, 체표면적, 대동맥차단 시간, 체온 등은 HCC를 사용한 군(H 군)과 사용하지 않은 군(C군)간에 의미 있는 차이가 없었다(p<0.05). 헤파린 공급 전, 공급 후 20분, 40분, 60분과 프로타민 공급 후 20분에 측정한 ACT는 두 군간에 의미 있는 차이가 없었다. 두 군간의 처음에 공급한 헤파린 양과 총 프로타민 사용량은 차이가 없었으나(p>0.05), 추가 공급한 헤파린 양(11$\pm$30 versus 67$\pm$49mg, p<0.05)과 총 헤파린 사용량(176$\pm$44 versus 239$\pm$70mg, p<0.05)은 H군에서 의미 있게 적게 나왔다. 두 군간에서 심폐기 사용시간에는 차이가 없었으면서 H군에서 약 38%정도의 헤파린을 적게 사용하였다. 결론: 결론적으로 HCC의 사용으로 심폐기 사용 시간과 상관없이 추가하는 헤파린 양을 줄임으로서 총 헤파린 사용량을 줄여 줄 수 있었으며 이것이 HCC의 임상적 효과를 나타나게 하는 하나의 요소로 작용할 수 있다고 생각된다.

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Cultural Condition for the mycelial growth of Ganoderma lucidum on Cereals (곡물을 이용한 영지버섯의 균사체 배양조건)

  • Jung, In-Chang;Kim, Seon-Hee;Kwon, Yong-Il;Lee, Jae-Sung
    • The Korean Journal of Mycology
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    • v.24 no.1 s.76
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    • pp.81-88
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    • 1996
  • Cereals were used as solid-substrate for the cultivation of Ganoderma lucidum. The hydration time with cold water appeared to be 10, 11 and 12 hours for Malt, Danyeob and Black soybeans respectively, and the water content was enough for mycelial growth in this condition. The hydration times required for sorghum, job's tears, barley, brown rice and wheat were 2.5, 4, 5, 10 and 12 hours respectively, but the final water content was much less than optimum water content (65%). Hot water reduced the hydration time of soybeans, and the water content reached to 65% within $120{\sim}150$mins. This condition showed the optimum for the mycelial growth. For the other cereals, it took about $17{\sim}120$ mins to reach the optimum water content (65%). From this result, hot water was better than cold water for the hydration of cereals. We attempted to develop a practically applicable process by combining the soaking and sterilization. This process was successful with soybean and about 1.1 times of water based on the weight of soybean appeared to be suitable. In all varieties of cereal, the water content of 65% appeared to be the best for the growth of the fungi and production of glucosamine related to the amount of mycelium. The mycelial growth rate in accordance with kinds of solid-state materials was in the order of barley > wheat > job's tears > sorghum > brown rice > soybean. The glucosamine content for determing the mycelial growth in solid material was in the order of wheat> barley > brown rice > job's tears > sorghum > soybean.

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Clinical Antagonistic Effect of Atipamezole in Cats Anesthetized with Tiletamine-Zolazepam and Medetomidine (고양이에서 tiletamine-zolazepam과 medetomidine 마취에 대한 atipamezole의 임상적 길항 효과)

  • Kim, Hyung-Ung;Park, Chang-Sik;Jun, Moo-Hyung;Jeong, Seong-Mok;Kim, Myung-Cheol
    • Journal of Veterinary Clinics
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    • v.24 no.2
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    • pp.104-108
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    • 2007
  • The purpose of the study is to evaluate the clinical antagonistic effect of atipamezole(0.25 mg/kg, IM) in cats anesthetized with tiletamine-zolazepam ($Zoletil^{(R)}$, 10 mg/kg, IM) and medetomidine (0.05 mg/kg, IM). Twelve healthy 1 year old Korean mixed breed cats were used for this study. They were 4 males and 8 females. These cats were randomly assigned to two groups. One was control group ($Zoletil^{(R)}$ + medetomidine, ZM), and the other was treatment group ($Zoletil^{(R)}$ + medetomidine and antagonism by atipamezole, ZMA). All cats were examined 15 minutes before, 5, 25, 65 and 105 minutes after administration of tiletamine-zolazepam and medetomidine. Atipamezole was injected intramuscularly 20 minutes after ZM administation. Recovery time, heart rate, respiratory rate, total plasma protein and blood glucose were significantly different between ZM group and ZMA group (P<0.05). However, rectal temperature was not significantly different between ZM group and ZMA group. Two groups were able to induce sternal recumbency within 2 minutes and lateral recumbency within 4 minutes after the anesthetics injection. Mean sternal position time ($mean{\pm}SD$) was $174.0{\pm}44.6\;and\;116.2{\pm}27.3$ minutes, and mean standing position time was $210.8{\pm}45.6\;and\;154.2{\pm}21.1$ minutes in ZM and ZMA group, respectively. In these two groups, adverse effects during recovery time from anesthesia were not seen. As a result, the ZMA group had a faster recovery than the ZM group. Thus it was concluded that atipamezole could exert a useful reversal effect in cats anesthetized with medetomidine-tiletamine/zolazepam combination.

Performance Measurement of the Wireless Charging Devices Using Eletromagnetic Induction Techniques (전자기유도방식을 이용한 무선 충전 기기의 구현 및 성능 측정)

  • Ryu, Daun;Kim, Young Hyun;Koo, Kyung Heon
    • Journal of Advanced Navigation Technology
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    • v.19 no.3
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    • pp.237-243
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    • 2015
  • This paper presented the design of wireless power transfer (WPT) system using electromagnetic induction techniques and analysed WPT efficiency. Also, we presented the optimum coil condition by measuring the efficiency variation according to some receiving coil parameter changes. Voltage change is measured by receiving coil position for the designed transmitting and receiving circuit. Voltage change according to inductance variation at the same position and charging time are compared at the same environment by using a developed application program to realize an optimum WPT system. Developed wireless power transfer system using electromagnetic induction techniques uses 125 kHz. It takes 16 minutes by using wired charger, and 23 minutes by using wireless charger for charging from 50% to 60% charging status.

Protease Activities in Tenderizing Effect of Vegetables used as Cooking Material (조리용 채소의 단백분해효소 활성 및 연육효과)

  • Suh, Hyung-Joo;Chung, Soo-Hyun;Choi, Yang-Mun;Cho, Won-Dai
    • Korean Journal of Food Science and Technology
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    • v.30 no.4
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    • pp.883-887
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    • 1998
  • Protease activities were measured in vegetables used as cooking material or a side dish. Proteases of green pepper (Kwari and Chungyang), perilla leaves, soybean sprout and mungbean sprout were showed high activities. Especially, protease in soybean sprout was the highest activity among them. After dialysis, remaining activities in mungbean sprout, green pepper (Kwari and Chungyang) and perilla leaves were 12, 23, 45% and 37%. In the results of thawing after freezing the proteases, remaining activities in sprout of mungbean and soybean were 100% and 65%. Protease in soybean sprout was showed higher activity and stability than others. Proteolytic effects of soybean sprout on myofibrillar and sarcoplasmic protein were showed higher than stroma protein. In SDS-PAGE, myosin heavy chain, actin and tropomyosin were hydrolyzed with increasing time. Protease activity was rapidly increased with increasing meat concentration in a early proteolysis reaction, but was slightly increased in later.

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Survey on ultrafast time resolved X-ray diffraction measurements of crystal structure (X선의 초고속 결정구조 측정법)

  • Koo, Y.D.;Kim, Y.C.;Oh, C.S.
    • Journal of Energy Engineering
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    • v.23 no.3
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    • pp.13-16
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    • 2014
  • We have surveyed on significant progress in recent developments of accelerator-based pulsed X-ray sources has offered the opportunity for time-resolved studies on fast structure dynamics on the nanometer scale. The required and currently available techniques for time resolved X-ray diffraction measurements using the third-generation synchrotron radiation sources are summarized. Ultrafast X-ray experimental techniques are discussed for femtosecond studies at future synchrotron radiation sources.

가공전 열처리가 Fresh-cut Muskmelon의 품질변화에 미치는 영향

  • 박연주;문광덕
    • Proceedings of the Korean Society of Postharvest Science and Technology of Agricultural Products Conference
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    • 2003.10a
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    • pp.166-166
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    • 2003
  • Muskmelon(Cucumis melo L.)은 독특한 향기와 높은 당도로 각광받고 있는 과일로 주로 지중해, 아시아, 북유럽과 미주지역에서 광범위하게 재배되고 있으며 우리나라에서는 주로 시설 내에서 재배되고 있다. 점차 그 수요가 증가하고 있는 fresh-cut제품은 유통, 저장 기간 동안 제품의 신선함 유지가 요구된다. 본 연구에서는 가공 전 열처리가 fresh-cut muskmelon의 품질에 미치는 영향과 최적 열처리 조건을 조사하였다. Half-cut melon을 대상으로 blanching 온도 설정을 위한 예비 실험을 한 결과 5$0^{\circ}C$ 열처리한 구가 향, 연화 저해 정도, 그리고 전체적인 기호도에 대한 관능평가 가장 우수하였다. 이를 바탕으로 5$0^{\circ}C$의 water bath상에서 whole melon을 10, 20, 30, 40분 blanching하여 5$^{\circ}C$에서 24시간 저장한 후 cork borer를 이용하여 cylinder 형의 fresh-cut melon을 가공하였다. 가공한 melon은 5$^{\circ}C$에서 6일 저장하면서 L-value, chroma-value, soluble solid, pH, 경도, 호흡 변화 등을 통해 품질변화를 측정하였다. 저장 6일후 L-value의 변화는 대조구에서 가장 크게 나타났으며, chroma-value는 저장 시간이 경과함에 따라 감소하였으며 10분 열처리 한 구에서 변화정도가 가장 낮게 나타났다. 수용성 고형분 함량은 저장기간의 경과에 따른 큰 변화는 없었으나 40분 열처리한 구에서 수용성 고형분 함량이 가장 낮았으며 20, 30분 열처리한 구에서 높게 나타났다. 저장 중 fresh-cut melon의 pH는 증가하는 경향을 보였으며 10분 열처리한 구에서 가장 낮게 나타났다. 호흡변화는 저장 기간이 경과함에 따라 $O_2$는 감소하고 $CO_2$는 증가했으며 특히 20분 열처리한 구에서 $CO_2$가 크게 증가한 것으로 나타났다. 증가 정도가 가장 크게 나타났다. 열처리한 fresh-cut melon의 hardness는 저장 3일 후 대조구와 40분 열처리 구에서 가장 낮아 연화현상을 확인했으며 20분 열처리구에서 초기 hardness가 유지되는 것으로 확인했다. 따라서 fresh-cut melon을 위한 가공 전 열처리를 위해서는 5$0^{\circ}C$에서 10분 열처리가 품질 변화를 유지하는데 적당하다고 판단된다.

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