• Title/Summary/Keyword: 스파터

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탄소나노튜브 에미터 기반 Flat Light Lamp 제작 시 금속전극 선폭과 간격 변화에 따른 전계방출 특성평가

  • Lee, Han-Seong;Im, Byeong-Jik;Ha, In-Ho;O, Se-Uk;Lee, Cheol-Seung;Lee, Gyeong-Il;Jo, Jin-U
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.02a
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    • pp.520-520
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    • 2013
  • Lateral 구조를 갖는 탄소나노튜브 에미터 캐소드의 금속전극 선폭과 간격은 탄소나노튜브 에미터 밀도와 게이트에 인가되는 전계의 크기에 밀접한 관계가 있어 전계방출특성에 큰 영향을 나타내므로 조속한 상업화를 위해서는 최적화 연구가 요구된다. 따라서 본 연구에서는 금속전극의 선폭과 간격을 110/30, 80/30, 40/30과 120/20, 90/20, 20/20 ${\mu}m$로 각각 변화시켜 4.6인치 탄소나노튜브 에미터 기반 flat light lamp 개발연구를 진행하였다. 이때 사용한 금속전극은 2 mm 두께를 갖는 4.6인치 소다라임 글라스 위에 패턴 된 PR에 Ag를 sputtering하여 증착 후 PR을 lift-off하여 형성하였다. 이와 같이 형성된 금속전극은 ~1 ${\mu}m$와 12 nm의 두께와 표면단차를 각각 가지고 있었다. 형성된 금속전극 위에 유전체와 탄소나노튜브 에미터를 각각의 페이스트를 사용하여 스크린 인쇄와 소성과정을 통해 형성하였다. 이때 레이저 빔을 전극사이의 빈 공간에 조사하여 탄소나노튜브 에미터를 금속전극 위에 정밀하게 정렬하였으며 잔존하는 유기물과 유기용매를 없애기 위해 대기압 공기분위기의 $410^{\circ}C$에서 10분간 소성과정을 거친 후 접착테이프를 사용하여 잔탄 속에 있는 탄소나노튜브 에미터를 물리적 힘으로 수직하게 노출시켜 캐소드를 준비하였다. 애노드는 전계에 의해 방출된 전자의 측정과 전계방출 이미지를 얻기 위해서 P22 형광체와 Al박막이 증착된 2 mm 두께의 소다라임 글라스를 사용하였다. 캐소드와 애노드 사이의 간격은 6~10 mm로 유지하였고, 진공챔버의 기본 압력을 $5{\times}10^{-6}$ Torr 이하로 유지하였다. 캐소드와 게이트 전극에 1, 4 kHz와 3% duty를 갖는 bipolar 형태의 DC 사각펄스파를, 애노드에 ~18 kV의 DC 고전압을 각각 인가하여 평가하였으며 추후, 이렇게 제작된 다양한 선폭과 간격을 갖는 탄소나노튜브 에미터 기반 flat light lamp의 전계방출특성과 효율에 대한 비교 연구를 진행할 계획이다.

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Ceramic barrier coated Pd hydrogen membrane on a porous nickel support (수소 분리용 팔라듐계 분리막의 세라믹 코팅 영향)

  • Lee, Chun-Boo;Lee, Sung-Wook;Park, Jin-Woo;Kim, Kwang-Ho;Hwang, Kyung-Ran;Park, Jong-Soo;Kim, Sung-Hyun
    • 한국신재생에너지학회:학술대회논문집
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    • 2010.11a
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    • pp.114.1-114.1
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    • 2010
  • A highly performed Pd-based hydrogen membrane has prepared successfully on a modified porous nickel support. The porous nickel support modified by impregnation method of $Al(NO_3)_3{\cdot}9H_2O$ (Aldrich Co.) over the nickel powder showed a strong resistance to hydrogen embrittlement and thermal stability. Plasma surface modification treatment was introduced as a pre-treatment process instead of conventional HCl wet activation. Ceramic barrier was coated on the external surface of the prepared nickel supports to prevent intermetallic diffusion and to enhance the affinity between the support and membrane. Palladium and copper were deposited at thicknesses of $4\mu}m$ and $0.5{\mu}m$, respectively, on a barrier-coated support by DC sputtering process. The permeation measurement was performed in pure hydrogen at $400^{\circ}C$. The single gas permeation of our membrane was two times higher than that of the previous membrane which do not have ceramic barrier.

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A Study on the Anisotropy Inhomogeneity of Permalloy Thin Films (퍼말로이 박막의 이방성불균일에 관한 연구)

  • 장평우;최태원;유성초;김희중
    • Journal of the Korean Magnetics Society
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    • v.7 no.4
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    • pp.186-190
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    • 1997
  • We measured an anisotropy inhomogeniety and dispersion of rf sputterd permalloy thin films by TBP(Transverse Biased Permeability) measurement method. Angular distribution function had a shape similar to the Lorentzian distribution, but magnitude distribution function deviates from the sysmetric Lorentzian distribution because of long tail to the region of a high Hk value. With increasing film thickness, the angular and magnitude anisotropy dispersion increased. The increase of angular dispersion was due to both the increase of grain size and local anisotropy in thicker films.

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Effects of Substrate Temperature on the Properties Sputtered Fe Films Epitaxially Grown on Mgo(001) (기판온도가 MgO(001) 기판위에서 에피택시성장한 Fe스파터박막의 특성에 미치는 영향)

  • 김동우;장평우;김원태;유성초
    • Journal of the Korean Magnetics Society
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    • v.9 no.4
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    • pp.184-189
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    • 1999
  • 1000 $\AA$ thick Fe films were epitaxially grown on MgO(001) by an rf sputtering and effects of substrate temperature on the structural and magnetic properties were investigated. X-ray diffraction intensity increased with increasing substrate temperature and inter-planar spacing $d_{(002)}$ decrease with increasing the temperature up to 25$0^{\circ}C$. The increased intensity and decreased inter-planar spacing were thought to be attributed to the enhancement of lattice match between Fe films and MgO, thus yielding good epitaxial growth. By using torque magnetometer, VSM and pole figure, very nice epitaxial growth of sputtered Fe films on MgO could be confirmed and $K_1$ value of Fe films grown at 25$0^{\circ}C$ was $4.6{\times}10^5\;erg/cc$, which was very similar to that of bulk single Fe crystal.

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Cross-sectional Design and Stiffness Measurements of Composite Rotor Blade for Multipurpose Unmanned Helicopter (다목적 무인헬기 복합재 로터 블레이드의 단면 구조설계 및 강성 측정)

  • Kee, Young-Jung;Kim, Deog-Kwan;Shin, Jin-Wook
    • Journal of Aerospace System Engineering
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    • v.13 no.6
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    • pp.52-59
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    • 2019
  • The rotor blade is a key component that generates the lift, thrust, and control forces required for helicopter flight by the torque transmitted through the hub and the blade pitch angle control, and should be designed to factor vibration characteristics so that there is no risk of resonance with structural safety. In this study, the structural design of the main rotor blade for MPUH(Multi-Purpose Unmanned Helicopter) was conducted and the sectional stiffness measurement of the fabricated blade was performed. The evaluation of the vibration characteristics of the main rotor system was then conducted factoring the measured stiffness distribution. The interior of the rotor blade comprised of the skin, spar, and torsion box, and carbon and glass fiber composites were applied. The Ksec2D program was applied to predict the stiffness of blade, and the results were compared to the measured data. CAMRADII, a comprehensive rotorcraft analysis program, was applied to investigate the natural frequency trends and resonance risks due to the rotor rotation.

Studies on the Development of Food Resources from Waste Seeds -II. Chemical Composition of Apple Seed- (폐기종실(廢棄種實)의 식량자원화(食糧資源化)에 관(關)하여 -제(第) 2 보(報) : 사과씨의 화학적(化學的) 조성(組成)-)

  • Yoon, Hyung-Sik;Choi, Cheong;Oh, Man-Jin
    • Korean Journal of Food Science and Technology
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    • v.15 no.2
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    • pp.128-132
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    • 1983
  • The apple seed contained 25.96% of crude fat and 37.62% of crude protein. The lipid fractions obtained by cilicic column chromatography were mainly composed of about 93.52% neutral lipid, whereas compound lipid was only 6.48% level. Among the neutral lipid separated by thin layer chromatography, triglyceride was 92.17%, sterol ester, sterol, diglyceride and free fatty acid were 3.53, 2.25, 1.44 and 0.56, respectively. The predominent fatty acids of total and neutral lipids were linoleic acid (59.79-69.37%) and oleic acid (20.04-29.82%), but those of glycolipid and phojspholipid were linoleic acid (29.20-36.04%). The major fatty acids of triglyceride separated from neutral lipid were oleic acid (44.31%), linoleic acid (36.66%) and palmitic acid (12.48%). The salt soluble protein of apple seed was highly dispersible in 0.02M sodium phosphate buffer containing about 1.0M $MgSO_4$, and the extractability of seed protein was 37%, Glutamic acid was the major amino acid in salt soluble protein, followed by arginine and aspartic acid. The eletrophoretic analysis showed three bands in apple seed protein, and the collection rate of the main protein fraction purified by Sephadex G-100 and G-200 was 76.6%. Glutamic acid, aspartic acid and arginine were the major amino acids of the main apple seed protein. The molecular weight for the main protein of the apple seed was estimated to be 45,000.

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Studies on the Development of Food Resources from Waste Seeds -I. Chemical Composition of Grape Seed- (폐엽종실(廢棄種實)의 식량자원화(貪糧資源化)에 관(關)하여 -제(第) 1 보(報) : 포도씨의 화학적(化學的) 조성(組成)-)

  • Yoon, Hyung-Sik;Kwon, Joong-Ho;Hwang, Joo-Ho;Choi, Jae-Chun;Shin, Dae-Hyn
    • Korean Journal of Food Science and Technology
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    • v.14 no.3
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    • pp.250-256
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    • 1982
  • A series of studies were conducted to find out the possibility of utilizing grape seed as resources of food fats and proteins, and the results of the studies are as follows: The grape seed contained 25.1%, of crude fat and 12.0% of crude protein. The lipid, fractions obtained by silicic acid column chromatography were mainly composed of about 95.5% neutral lipid, whereas compound lipid was only 4.5% level. Among the neutral lipid by thin layer chromatography, triglyceride was 91.89%, sterol ester, sterol, diglyceride and free fatty acid were 3.24%, 2.87%, 1.20% and 0.80%, respectively The predominant fatty acids of total and neutral lipids were linoleic acid $(69.72{\sim}71.72%)$ and oleic acid $18.09{\sim}19.46%)$, but those of glycolipid and phospolipid were linoleic acid $(31.49{\sim}38.18%)$, oleic acid $(20.20{\sim}35.27%)$ and palmitic acid $(26.80{\sim}39.98%)$. The major fatty acids of triglyceride separated from neutral lipid were oleic acid (43.08%), linoleic acid (38.42%) and palmitic acid (11.60%). The salt soluble protein of grape seed was highly dispersible in 0.02M sodium phosphate buffer containing about 1.0M $MgSO_4$, and the extractability of seed protein was 31%. Glutamic acid was the major amino acid in salt soluble protein, followed by arginine and aspartic acid. The electrophoretic analysis showed 3 bands in grape seed protein, and the collection rate of the main protein fraction purified by Sephadex G-100 and G-200 was 82%. Glutamic acid, aspartic acid and arginine were the major amino acids of the main grape seed protein. The molecular weight for the main protein of the grape seed was estimated to be 81,000.

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Design of Mach-Scale Blade for LCH Main Rotor Wind Tunnel Test (소형민수헬기 주로터 풍동시험을 위한 마하 스케일 블레이드 설계)

  • Kee, YoungJung;Park, JoongYong
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.46 no.2
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    • pp.159-166
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    • 2018
  • In this study, the internal structural design, dynamic characteristics and load analyses of the small scaled rotor blade required for LCH(Light Civil Helicopter) main rotor wind tunnel test were carried out. The test is performed to evaluate the aerodynamic performance and noise characteristics of the LCH main rotor system. Therefore, the Mach-scale technique was appled to design the small scaled blade to simulate the equivalent aerodynamic characteristics as the full scale rotor system. It is necessary to increase the rotor speed to maintain the same blade tip speed as the full scale blade. In addition, the blade weight, section stiffness, and natural frequency were scaled according to the Mach-type scaling factor(${\lambda}$). For the design of skin, spar, torsion box, which are the main components of the blade, carbon and glass fiber composite materials were adopted, and composite materials are prepreg types that can be supplied domestically. The KSec2D program was used to evaluate the section stiffness of the blade. Also, structural loads and dynamic characteristics of the Mach scale blade were investigated through the comprehensive rotorcraft analysis program CAMRADII.

Low-speed Impact Localization on a Stiffened Composite Structure Using Reference Data Method (기준신호 데이터를 이용한 보강된 복합재 구조물에서의 저속 충격위치 탐색)

  • Kim, Yoon-Young;Kim, Jin-Hyuk;Park, Yurim;Shrestha, Pratik;Kwon, Hee-Jung;Kim, Chun-Gon
    • Composites Research
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    • v.29 no.1
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    • pp.1-6
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    • 2016
  • Low-speed impact was localized on a stiffened composite structure, using 4 FBG sensors with 100 kHz-sampling rate interrogator and devised localization algorithm. The composite specimen consists of a main spar and several stringers, and the overall size of the specimen's surface is about $0.8{\times}1.2m$. Pre-stored reference data for 247 grid locations and 36 stiffener locations are gathered and used as comparison target for a random impact signal. The proposed algorithm uses the normalized cross-correlation method to compare the similarities of the two signals; the correlation results for each sensor's signal are multiplied by others, enabling mutual compensation. 20 verification points were successfully localized with a maximum error of 43.4 mm and an average error of 17.0 mm. For the same experimental setup, the performance of the proposed method is evaluated by reducing the number of sensors. It is revealed that the mutual compensation between the sensors is most effective in the case of a two sensor combination. For the sensor combination of FBG #1 and #2, the maximum localization error was 42.5 mm, with average error of 17.4 mm.