• Analytical Science and Technology
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• v.28 no.6
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• pp.446-452
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• 2015

In order to evaluate and improve the ability of Korean testing laboratories to measure Polybrominated diphenyl ethers in acrylonitrile-butadiene-styrene (ABS), a proficiency test was organised by Korea Research Institute of Standards and Science (KRISS) based on ISO/IEC 17043. The proficiency test material used was 10 g of a granular ABS fortified with a mixture of congeners of PBDE (BDE-154, 183, 206, 209). Homogeneity and stability were investigated to assess the adequacy of the test material. The certified value established by KRISS based on the national reference was used for assigned value of each PBDE. The test materials were distributed to the 16 participating laboratories. The participating laboratories were requested to analyse the samples employing the methods used in their routine analysis. Each laboratory was given it’s own code to secure the anonymity. Participants results were evaluated with z-scores according to ISO/IEC 17043. The standard deviation for proficiency assessment was set by standard deviation of the participants results except for outlier. The results, the laboratory's performance and improvement of accuracy were discussed.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.21 no.6
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• pp.18-27
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• 2020

This study compared and analyzed the results of proficiency testing between testers based on the international standard ISO/IEC 17043 proficiency testing requirements using ISO/IEC 25023 software quality characteristics evaluation. Application of the test was submitted to the KASTO as a software test in the electric test field defined by KOLAS. Among ISO/IEC 25023, the evaluation items for proficiency testing between testers were selected as functional completeness and time behavior. The comparison test between testers was carried out on May 28, 2019 at the accredited LG Electronics SW Laboratory in Seoul and attended by KOLAS assessors. The test evaluation method was measured once per tester with functional completeness, and measurement was repeated 10 times per tester according to time behavior. As a result, in the case of functional completeness, all 12 test steps were passed, and the satisfaction was evaluated. Time behavior was repeated 10 times, and the mean was 9.45 ± 0.01 seconds for testers 1 and 3 and 9.52 ± 0.0 seconds for tester 2, but there was no statistically significant difference. In conclusion, the proficiency of the testers was equal, and the reliability of the test results of the test institute was confirmed.

• Analytical Science and Technology
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• v.22 no.5
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• pp.369-375
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• 2009

We evaluated the homogeneity and accuracy of low level airborne fibrous standard, and accomplished the proper proficiency test. We had found that the correlation of concentration of standard solution and asbestos density was 0.9863~0.9968, and concluded that the proper guideline of the analysis result was ${\mid}Z{\mid}{\leq}2$ interval of Z-score.

• The Korean Journal of Pesticide Science
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• v.16 no.4
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• pp.350-356
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• 2012

Performance of proficiency testing and the validation of analytical method was included a scheme of quality assurance in analytical chemistry laboratory to monitor a laboratory's performance abilities and produce consistently reliable data. This study was assessed the applicability of proficiency testing scheme proposed for analytical laboratories of pesticide product in domestic. The validation of analytical methods, stability and homogeneity for formulated pesticide products (emulsifiable concentrate) of emamectin benzoate and lufenuron was confirmed for the proficiency testing. The z-score of 33 participation laboratories for emamectin benzoate were that the numbers of outlier were 2 laboratories (6.0%), z-score outside the range from -3 to 3 designated "unaccptable" were 2 laboratories and z-score in the ranges -2 to -3 and 2 to 3 designated "questionable" were 3 laboratories (9.0%). Three laboratories (9.0%) showed the z-score designated "questionable" for lufenuron. The additional proficiency testing for various product types will be needed to establish the scheme of quality control.

• Analytical Science and Technology
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• v.14 no.3
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• pp.230-237
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• 2001

In general, the pH measurement follows calibration of glass electrode system using pH standard solution. When pH is measured at constant temperature, uncertainty factors are mainly related to the accuracy of pH standard solution and the accuracy and precision of glass electrode. Participants in this proficiency test were the volunteers trying to know the distribution of the measured pH values for the same sample and the sources of error through 1998 and 1999. The samples for proficiency test are phosphate salt standard solutions specially prepared in KRISS, of which pH values were 6.860, 7.415(at $25^{\circ}C$), and the stability test was performed for the same periods of proficiency test. The results of the proficiency test were plotted according to Youden plot, which shows whether the error is random or systematic. The results of Youden plot showed that the source of error was from the systematic effect of laboratories in each year. This shows that the source of error is the standard solutions used in laboratories.

• Transactions of the KSME C: Technology and Education
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• v.5 no.2
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• pp.105-113
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• 2017

KOLAS (KOrea Laboratory Accreditation Scheme) belongs to APLAC (Asia Pacific Laboratory Accreditation Cooperation). KOLAS manages the accreditation scheme for measurement traceability to SI units. As per June 2016, there are 22 KOLAS laboratories for liquid flow metering. Among them, 12 laboratories participated in the proficiency test (PM2015-08) for water flow metering, organized by KASTO (Korea Association of Standards and Testing Organizations). This proficiency test was performed with three kinds of flow ranges ($3.6m^3/h{\sim}12m^3/h$, $40m^3/h{\sim}80m^3/h$, $40m^3/h{\sim}200m^3/h$) considering the CMC (calibration and measurement capability) of the participating laboratories. The purpose of the proficiency test was to find out measurement equivalence of the CMC's between each participating laboratory and the reference testing laboratory (KRISS). The measurement equivalence was tested by the number of equivalence ($E_n$). If ${\mid}E_n{\mid}$ < 1, the measurement equivalence was established. All the participating laboratories passed this proficiency test.

• The Korean Journal of Pesticide Science
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• v.15 no.4
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• pp.529-544
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• 2011

Many international organizations, such as the International Organization for Standardization (ISO) and Collaborative International Pesticide Analytical Council (CIPAC), have published a guide to quality control requirements, proficiency testing and method validation for pesticide formulation. In general, proficiency testing is to determine the performance of individual laboratories from the comparison of test results and to monitor a laboratory's performance abilities. One of quality assurance (QA) scheme would be include the validation of analytical method that implies a performance characteristics, specificity, selectivity, linearity and so on. According to many international organizations, the quantification methods of active substance in formulated pesticide products are required to be reproducible, accurate and precise. This study was conducted to compare the international guidelines for the quality control, proficiency testing and method validation of analytical laboratories and to propose a general guidance for the establishment of quality control system in the analytical chemistry laboratories of pesticide formulation in domestic.

• Proceedings of the Korean Nuclear Society Conference
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• 2003.05a
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• pp.362.2-362.2
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• 2003

• Proceedings of the Korean Environmental Sciences Society Conference
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• 1999.04a
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• pp.296-297
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• 1999

• Proceedings of the Korea Air Pollution Research Association Conference
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• 1998.10a
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• pp.248-249
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• 1998