• Title/Summary/Keyword: 손상제어시험

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Development and validation of analytical methods for pyrifluquinazon residues determination on agricultural commodities by HPLC-UVD (HPLC-UVD를 이용한 농산물 중 pyrifluquinazon 잔류시험법 개발 및 검증)

  • Do, Jung-Ah;Kwon, Ji-Eun;Kim, Mi-Ra;Lee, Eun-Mi;Kuk, Ju-Hee;Cho, Yoon-Jae;Chang, Moon-Ik;Kwon, Kisung;Oh, Jae-Ho
    • Analytical Science and Technology
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    • v.26 no.3
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    • pp.174-181
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    • 2013
  • Pyrifluquinazon is classified with a quinazoline insecticide that regulates food intake by controling the feeding behavior acting on the endocrine or nervous system of pests such as aphids and white fly. To keep safety on pyrifluquinazon residues in agricultural commodities a simple, accurate and rapid analytical method was developed and validated using high performance liquid chromatograph (HPLC-UVD). The pyrifluquinazon residues acidified with 1% formic acid in samples were extracted with acetonitrile and partitioned with hexane subsequently to dichloromethane then purified with silica solid phase extraction (SPE) cartridge. The purified samples were detected using HPLC-UVD. The method was validated using apple and pear spiked with pyrifluquinazon at 0.02, 0.05 and 0.1 mg/kg and hulled rice, pepper, soybean at 0.05 and 0.1 mg/kg. Average recoveries were 70.5~107.9% with relative standard deviation less than 10%. The result of recoveries and overall coefficient of variation of a laboratory results in Gwangju regional FDA and Daejeon regional FDA was followed with Codex guideline (CODEX CAC/GL 40). This method is appropriated at pyrifluquinazon residues determination and will be used as official method of analysis.

Development of Oriental Melon Harvesting Robot in Greenhouse Cultivation (시설재배 참외 수확 로봇 개발)

  • Ha, Yu Shin;Kim, Tae Wook
    • Journal of Bio-Environment Control
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    • v.23 no.2
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    • pp.123-130
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    • 2014
  • Oriental melon (Cucumis melo var. makuwa) should be cultivated on the soil and be harvested. It is difficult to find because it is covered with leaves, and furthermore, it is very hard to grip it due to its climbing stems. This study developed and tested oriental melon harvesting robots such as an end-effector, manipulator and identification device. The end effector is divided into a gripper for harvest and a cutter for stems. In addition, it was designed to control the gripping and cutting forces so that the gripper could move four fingers at the same time and the cutter could move back and forth. The manipulator was designed to realize a 4-axis manipulator structure to combine orthogonal coordinate-type and shuttle-type manipulators with L-R type model to rotate based on the central axis. With regard to the identification device, oriental melon was identified using the primary identification global view camera device and secondary identification local view camera device and selected in the prediction of the sugar content or maturity. As a result of the performance test using this device, the average harvest time was 18.2 sec/ea, average pick-up rate was 91.4%, average damage rate was 8.2% and average sorting rate was 72.6%.

정형외과 모의수술을 위한 원격 시뮬레이터의 개발에 관한 연구

  • 최수미;김명희
    • Proceedings of the Korea Society for Simulation Conference
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    • 1996.05a
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    • pp.6-6
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    • 1996
  • 컴퓨터 통신망의 활용이 각 분야에서 걸쳐서 점차 확대되고 있으며 의료 분야에서도 원격진료(tele-medicine), 원격교육(tele-education), 원격수술(tele-surgery) 등에 대한 시스템 개발이 관심을 끌고 있다. 본 연구에서는 초고속 정보통신망 환경에서 정형외과 모의수술을 하기 위한 시뮬레이터의 프로토타입을 구현하였다. 원격 모의수술 시뮬레이터를 구축하기 위해서는 CT, MRI와 같은 의학영상 처리, 다지점간의 회의를 제어할 수 있는 통신 제어, 환자의 진료를 위한 멀티미디어 데이터의 저장 및 검색을 위한 데이터베이스 구축 등 다양한 기술들의 총체적인 결합이 요구되어진다. 구축 시뮬레이터는 세가지 주요 서브 시스템으로 구성된다. 첫째, 원격 시뮬레이션을 위한 전반적인 관리, 운영, 제어를 담당하는 수술회의 시스템, 둘째, 모의수술을 가능케 하기 위한 2차원 영상의 전처리 3차원 영상 재구성 및 조작을 통한 모의수술 시스템, 셋재, 멀티미디어 환자 자료의 검색 및 관리를 하기 위한 데이터베이스 운영시스템으로 구성된다. 제안된 원격 모의수술 시뮬레이터는 서버-클라이언트 구조를 기반으로 하고, 여러명의 의사가 공동작업(CSCW: Computer Supported Cooperative Work)에 의해 모의수술을 할 수 있도록 공용 윈도우를 기반으로 한 그래픽 사용자 인터페이스를 제공한다. 멀티미디어 의료 데이터의 전송은 TCP/IP 프로토콜을 사용하고, 사용자 인터페이스는 X-window를 이용하여 구축하였다. 본 시뮬레이터는 SUN Server 1000을 서버로 하고, 두대의 SDT Workstation을 클라이언트로 하여 Ethernet 환경에서 구현 및 검증하였다. 또한 ATM Network에서 본 시뮬레이터를 시험함으로써 국책 사업으로 구축되는 초고속 정보통신망 환경에서의 사용 가능성을 입증하였다. 판단된다.원과 섭식장소, 수중생물의 경우는 특히 수온, 수량 영양원등이다.(중략). 본 연구의 접근방법으로는 ASRS의 개념적인 Reference Model을 수립하고 이 Reference Model에 대한 Formal Model로 DEVS(Discrete Event System Specification)을 이용하여 시스템을 Modeling하였다. 이의 Computer Simulation을 위하여 DEVS형식론 환경에서의 Simulation Language인 DEVSim ++ⓒ를 이용하여 시스템을 구현하였다.. 실형 결과로는 먼저 선형 상미분방정식의 예로 mass-damper-spring system, 비선형 상미분방정식의 예로는 van der Pol 방정식, 연립 상미분방정식의 예로는 mixing tank problem 등을 보였으며, 그의 공학에서 일어나는 여러 가지 문제들도 다루었다.화물에 대한 방어력이 증가되어 나타난 결과로 여겨지며, 또한 혈청중의 ALT, ALP 및 LDH활성을 유의성있게 감소시키므로서 감잎 phenolic compounds가 에탄올에 의한 간세포 손상에 대한 해독 및 보호작용이 있는 것으로 사료된다.반적으로 홍삼 제조시 내공의 발생은 제조공정에서 나타나는 경우가 많으며, 내백의 경우는 홍삼으로 가공되면서 발생하는 경우가 있고, 인삼이 성장될 때 부분적인 영양상태의 불충분이나 기후 등에 따른 영향을 받을 수 있기 때문에 앞으로 이에 대한 많은 연구가 이루어져야할 것으로 판단된다.태에도 불구하고 [-wh]의미의 겹의문사는 병렬적 관계의 합성어가 아니라 내부구조를 지니지 않은 단순한 단어(minimal $X^{0}$ elements)로 가정한다. 즉, [+wh] 의미의 겹의문사는 동일한 구성요 소를 지닌 병렬적 합성어([$[W1]_{XO-}$ $[W1]_{

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PWR 원전환경에서 오스테나이트 스테인리스강의 피로균열성장특성에 미치는 질소의 영향

  • Min, Gi-Deuk;Kim, Dae-Hwan;Lee, Bong-Sang;Kim, Seon-Jin
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2011.10a
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    • pp.39.1-39.1
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    • 2011
  • 가압경수로의 압력경계기기는 약 $300^{\circ}C$, 150기압의 고온고압수환경에서 가동되고 있다. 특히 가압기 밀림관은 고온수와, 저온수가 교차하는 부분으로 열성층 형성으로 열적, 기계적 피로 및 수화학환경이 더해진 부식피로 등에 의하여 손상을 받는다. PWR 원전에서 수화학환경은 대표적으로 용존산소(DO) 5ppb, pH 6~8, 용존수소(DH) <30 cc/kg, 온도 $316^{\circ}C$의 환경을 유지하게 된다. 가압기 밀림관에는 오스테나이트계 스테인리스강이 사용되는데, 오스테나이트계 스테인리스강은 고온 수화학환경에 민감한 것으로 알려져 있다. 따라서 오스테나이트계 스테인리강을 공기중에서의 기계적특성 및 피로특성을 향상시키기 위하여 질소를 첨가한 스테인리스강을 제조하여 PWR 원전환경에서의 피로균열성장특성을 평가하였다. 실험에 사용된 재료는 PWR 원전 가압기 밀림관 소재인 Type 347 스테인리스강에 0.0005 wt%가 첨가된 상용재와 0.11 wt% 질소가 첨가된 재료이다. 사용된 시편형상은 두께 5 mm, 폭 25.4 mm의 CT 시편이다. 수화학환경은 150기압, 온도 $316^{\circ}C$, 용존산소(DO) 5ppb, 용존수소(DH) 30 cc/Kg, pH는 약 7로 유지 하였으며, 응력비 0.1, 하중 반복속도 10Hz의 기계적 조건에서 하중제어로 시험을 진행하였다. 균열길이는 직류전위차법(Direct Current Potential Drop: DCPD)을 이용하여 측정하였다. 질소함량이 증가할수록 동일 사이클에서 균열길이가 늦게 성장하였고, 피로균열성장속도도 약간 늦어지는 것으로 나타났다. 각 스테인리스강의 피로파면 관찰결과 상용재는 약 1 ${\mu}m$의 산화물들이 생성되는 반면 질소첨가 스테인리스강은 약 0.1 ${\mu}m$정도 산화물이 생성되었다. 산화막의 두께도 질소가 첨가됨으로써 상용재에 비해 얇게 생성되었다. 따라서 질소가 첨가됨으로써 부식환경에서 내산화성이 향상되었으며, 이는 피로균열성장특성에 영향을 미치는 것으로 판단된다.

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Fire Resistance Performance of High Strength Concrete Columns with Fireproof Gypsum Board (방화석고보드를 부착한 고강도 콘크리트 기둥의 내화성능)

  • Youm, Kwang-Soo;Jeon, Hyun-Gyu
    • Journal of the Korea Concrete Institute
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    • v.22 no.2
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    • pp.229-235
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    • 2010
  • In this study, fire resistance performance of high strength concrete specimen with fireproof gypsum board was investigated for possible use in upgrading fire-resistant performance of the existing building and repair of fire damaged structures. Fire test of eight identical high strength concrete columns were carried out for 180 minutes in accordance with ISO-834. The temperature distributions in longitudinal reinforcement and concrete temperature at various depths were recorded. The fireproof performance of gypsum board and explosive spalling of concrete were observed. The specimens with 15 mm thick twoply fireproof gypsum board spalled after gypsum board crumbled regardless of fastening methods. However, when the thickness of fireproof gypsum board was more than 30 mm, it was possible to prevent the explosive spalling and control the rebar temperature. Although the effect of cover thickness could not be compared because the explosive spalling occurred, there seemed to be no difference in insulation efficiency.

Investigation into the Thermal Stability of Fluoropolymer Coating for Heat-Resistant Application (내열성 불소수지 코팅막의 열 안정성에 관한 연구)

  • Cho, Hey-Jin;Ryu, Ju-Hwan;Byun, Doo-Jin;Choi, Kil-Yeong
    • Polymer(Korea)
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    • v.29 no.1
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    • pp.96-101
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    • 2005
  • Fluoropolymer of PTFE and PFA etc. is a heat resistance polymeric material that it is known as that maximum continuous use temperature reaches for 260 $^{\circ}C$. It was observed that these polymers had the enough thermal stability so enough that it was kept by thermal aging of 280 $^{\circ}C$/7 weeks too in this study. However, such thermal stability means that bulk material property is kept such as mechanical strength, melting point and initial pyrolysis temperature etc. If these polymers are evaluate by coating property such as surface contact angle, surface morphology, surface scratch, thing that heat resistance is not enough was confirmed in this study. Thermal aging of flouropolymer coating was achieved by gear aging oven that the exchange rate of air was controlled, and the analysis results were indicating serious damage of surface morphology and adhesive strength on metal substrate.

Durability Improvement of Functional Polymer Film by Heat Treatment and Micro/nano Hierarchical Structure for Display Applications (열처리와 복합구조화를 통한 디스플레이용 기능성 고분자 필름의 내구성 향상 연구)

  • Yeo, N.E.;Cho, W.K.;Kim, D.I.;Jeong, M.Y.
    • Journal of the Microelectronics and Packaging Society
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    • v.25 no.4
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    • pp.47-52
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    • 2018
  • In this study, the effects of the heat treatment and multi-scale hierarchical structures on the durability of the nano-patterned functional PMMA(Poly(methyl-methacrylate)) film was evaluated. The heat treatments that consisted of high-pressure/high-temperature flat pressing and rapid cooling process were employed to improve mechanical property of the PMMA films. Multi-scale hierarchical structures were fabricated by thermal nanoimprint to protect nano-scale structures from the scratch. Examination on surface structures and functionalities such as wetting angle and transmittance revealed that the preopposed heat treatment and multi-scale hierarchical structures are effective to minimize surface damages.

Processing and Characterization of Polyamide 610/Carbon Fiber/Carbon Nanotube Composites through In-Situ Interfacial Polymerization (계면중합법을 이용한 폴리아마이드 610/탄소섬유/탄소나노튜브 복합재 제조 및 물성 평가)

  • Cho, Beom-Gon;Hwang, Sang-Ha;Park, Young-Bin
    • Composites Research
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    • v.33 no.6
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    • pp.415-420
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    • 2020
  • The interfacial properties in carbon fiber composites, which control the overall mechanical properties of the composites, are very important. Effective interface enhancement work is conducted on the modification of the carbon fiber surface with carbon nanotubes (CNTs). Nonetheless, most surface modifications methods do have their own drawbacks such as high temperatures with a range of 600~1000℃, which should be implemented for CNT growth on carbon fibers that can cause carbon fiber damages affecting deterioration of composites properties. This study includes the use of in-situ interfacial polymerization of polyamide 610/CNT to fabricate the carbon fiber composites. The process is very fast and continuous and can disperse CNTs with random orientation in the interface resulting in enhanced interfacial properties. Scanning electron microscopy was conducted to investigate the CNT dispersion and composites morphology, and the thermal stability of the composites was analyzed via thermogravimetric analysis. In addition, fiber pull-out tests were used to assess interfacial strength between fiber and matrix.

Characterization of Stress Corrosion Cracking at the Welded Region of High Strength Steel using Acoustic Emission Method (음향방출법에 의한 고 장력강 용접부의 부식손상 특성 평가)

  • Na, Eui-Gyun;Kim, Hoon
    • Journal of the Korean Society for Nondestructive Testing
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    • v.23 no.3
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    • pp.212-219
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    • 2003
  • This study is to evaluate the characteristics of SCC at the welded region of high strength steel using acoustic emission(AE) method. Specimens were loaded by a slow strain rate method in synthetic seawater and the damage process was monitored simultaneously by AE method. Corrosive environment was controlled using the potentiostat, in which -0.8V and -1.1V were applied to the specimens. In the case of one-pass weldment subjected to -0.8V, much more AE counts were detected compared with the PWHT specimen. It was verified through the cumulative counts that coalescence of micro cracks and cracks for the one pass weldment with -0.8V were mostly detected. In case of the one pass weldment subjected to -1.1V, time to failure became shorter and AE counts were produced considerably as compared with that of the two pass weldment. It was shown that AE counts and range of AE amplitude have close relations with the number and size as well as width of the cracks which were formed during the SCC.

Effects of ionizing and ultraviolet radiation on microbial mutation and DNA damage (전리방사선 및 자외선의 미생물 돌연변이와 DNA 손상에 대한 영향)

  • Nam, Ji-Hyun;Shin, Ji-Hye;Lee, Jung-Yun;Lee, Dong-Hun
    • Korean Journal of Microbiology
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    • v.53 no.1
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    • pp.20-28
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    • 2017
  • Physical sterilization methods using ultraviolet radiation and ionizing radiation such as gamma ray and electron beam are applied in various industry fields due to disinfection effects and economic efficiency but may also cause microbial mutation. In this research, Salmonella enterica and Escherichia coli strains were treated with ionizing and ultraviolet radiation and their survival rate, mutation rate, and DNA damage were studied to evaluate the genetic safety. The survival rate of the strains decreased drastically as the irradiation dose of ultraviolet ray, gamma ray, and electron beam increased, and over 90% of the strain was exterminated at a dosage of $0.40{\sim}25.06mJ/cm^3$, 0.11~0.22 kGy, 0.14~0.53 kGy respectively. In SOS / umu-test, genotoxicity causing DNA damage was identified in all samples. In Ames test, back-mutation rate increased to $3.82{\times}10^{-4}$ and $9.84{\times}10^{-6}$ respectively when exposed to ultraviolet ray and gamma ray. At exposure to ultraviolet ray, gamma ray, and electron beam with dosage of over 99.99% extinction rate of S. enterica TA100, back-mutation rate increased 347 times, 220 times, 0.6 times respectively to the spontaneous back-mutation rate. Rifampicin resistance mutation rate of E. coli CSH100 exposed to ultraviolet ray, gamma ray, and electron beam was $2.46{\times}10^{-6}$, $1.66{\times}10^{-6}$, $4.12{\times}10^{-7}$ respectively. Therefore, gamma radiation is effective in microorganism control from the perspective of disinfection and electron beam has the advantage of sterilizing with little DNA damage and bacterial mutation.