• Composites Research
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• v.18 no.4
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• pp.21-26
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• 2005

Nondestructive damage sensing and load transfer mechanisms of carbon nanotube (CNT) and nanofiber (CNF)/epoxy composites have been investigated by using electro-micromechanical technique. The electrospun PVDF nanofibers were also prepared as a piezoelectric sensor. The electro-micromechanical techniques were applied to evaluate sensing response of carbon nanocomposites by measuring electrical resistance under an uniform cyclic loading. Composites with higher volume content of CNT showed significantly higher tensile properties than neat and low volume$\%$ CNT composites. CNT composites showed humidity sensing within limited temperature range. CNT composites with smaller aspect ratio showed higher apparent modulus due to high volume content in case of shorter aspect ratio. Thermal treated electrospun PVDF nanofiber showed higher mechanical properties than the untreated case due to crystallinity increase, whereas load sensing decreased in heat treated case. Electrospun PVDF nanofiber web also showed sensing effect on humidity and temperature as well as stress transferring. Nanocomposites and electrospun PVDF nanofiber web can be applicable for sensing application.

• Proceedings of the Korean Vacuum Society Conference
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• 2011.08a
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• pp.284-284
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• 2011

Ion sensitive field effect transistor (ISFET)는 용액 중의 각종 이온 농도를 측정하는 반도체 이온 센서이다. ISFET는 작은 소자 크기, 견고한 구조, 즉각적인 반응속도, 기존의 CMOS공정과 호환이 가능하다는 장점이 있다. ISFET의 기본 구조는 기존의 metal oxide semiconductor field effect transistor (MOSFET)에서 고안되었으며, ISFET는 기존의 MOSFET의 게이트 전극 부분이 기준전극과 전해질로 대체되어진 구조를 가지고 있다. ISFET소자의 pH 감지 메커니즘은 감지막의 표면에서 pH용액의 수소이온이 막의 표면에 속박되어 표면전위의 변화를 유발하는 것에 기인한다. 그 결과, 수소이온의 농도에 따라 ISFET의 문턱전압의 변화를 일으키게 되고 드레인 전류의 양 또한 달라지게 된다. 한편, ISFET의 좋은 pH감지특성과 높은 출력특성을 얻기 위하여 high-k물질들이 감지막으로써 지속적으로 연구되어져 왔다. 그 중 Al2O3와 HfO2는 높은 유전상수와 좋은 pH 감지능력으로 인하여 많은 연구가 이루어져온 물질이다. 하지만 HfO2는 높은 유전상수를 갖음에도 불구하고 화학용액에 대한 non-ideal 효과에 취약하다는 보고가 있다. 반면에 Al2O3의 유전상수는 HfO2보다 작지만 화학용액으로 인한 손상에 대하여 강한 immunity가 있는 재료이다. 본 연구에서는, 이러한 각각의 high-k 물질들의 단점을 보안하기 위하여 SiO2/HfO2/Al2O3(OHA) 적층막을 이용한 ISFET pH 센서를 제작하였으며 SOI 기판에서 구현되었다. SOI기판에서 OHA 적층막을 이용한 ISFET 제작이 이루어짐에 따라서 소자의 signal to noise 비율을 증대 시킬것으로 기대된다. 실제로 SOI-ISFET와 같이 제작된 SOI-MOSFET는 1.8${\times}$1010의 높은 on/off 전류 비율을을 보였으며 65 mV/dec의 subthreshold swing 값을 갖음으로써, 우수한 전기적 특성을 보이는 ISFET가 제작이 되었음을 확인 하였다. OHA 감지 적층막의 각 층은 양호한 계면상태, 높은 출력특성, 화학용액에 대한non-ideal 효과에 강한 immunity을 위하여 적층되었다. 결론적으로 SOI과 OHA 적층감지막을 이용하여 우수한 pH 감지 특성을 보이는 pH 센서가 제작되었다.

• Journal of the Korean Society for Nondestructive Testing
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• v.29 no.4
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• pp.308-315
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• 2009

Because the attenuation of AE signal in composite materials is relatively higher than that of metallic materials, it is required to develop a damage assessment technique less affected by the attenuation property of composite materials in order to use AE sensing as a damage detection method. In the signal processing procedure, it is profitable to use the leading wave that arrives first because the leading wave is less influenced by the boundary conditions. Using wavelet transform, we investigated the frequency characteristics of impact induced AE signals focused on the leading wave in advance and chose the key factors to discriminate the damaged condition quantitatively. In this research, we established a damage assessment technique using the sharing percentage of the wavelet detail components of AE signal, and conducted a low-velocity impact test on composite laminates to confirm the feasibility of the proposed signal processing method.

• Composites Research
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• v.26 no.3
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• pp.201-206
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• 2013

The electrical resistance measurement was investigated as a damage monitoring method. In this study, 0.5 wt% Carbon nanotube reinforced polypropylene (CNT/PP) composites were evaluated under compressive fatigue loading. The shape of specimens was $20^{\circ}$ curved round type. Compression strength and electrical resistance were measured at different sections of specimen during compression. The microcracks of CNT/PP composites were detected based on the changing ratio of electrical resistance. Micro-damage during compressive fatigue test could be detected by electrical resistance measurements. The reason is that the contact points of CNTs in composites decreased under fatigue loading. During compressive fatigue test, larger change of electrical resistance was detected at the microcrack sections. It was proved that microcracks could be detected by electrical resistance measurement under compression test, whereas the real delamination parts were consistent with the predicted results by electrical resistance measurement.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.37 no.8
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• pp.780-788
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• 2009

AE technique was applied to the static structural test of the composite wing structure to evaluate the structural integrity and damage. During the test, strain and displacements measurement technique were used to figure out for static structural strength. AE parameter analysis and source location technique were used to evaluate the internal damage and find out damage source location. Design limit load test, the 1st and 2nd design ultimate load tests and fracture test were performed. Main AE source was detected by an sensor attached on skin near by front lug. Especially, at the 1st design ultimate test, strain and displacements results didn't show internal damage but AE signal presented a phenomenon that the internal damage was formed. At the fracture test, AE activities were very lively, and strain and displacements results showed a tendency that the load path was changed by severe damage. The internal damage initiation load and location were accurately evaluated during the static structural test using AE technique. It is certified from this paper that AE technique is useful technique for evaluation of internal damage at static structural strength test.

• Proceedings of the Korean Society for Agricultural Machinery Conference
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• 2017.04a
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• pp.128-128
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• 2017

현재 식물공장에서 사용되고 있는 이식장치는 핀을 이용하여 육묘트레이 위에서 플러그묘를 뽑아 육묘트레이 또는 포트로 옮겨 심는 방식을 채택하고 있다. 이러한 이식 방식은 셀과 셀 사이에 있는 다른 묘의 잎을 파지함으로써 묘를 2개 이상 취출하는 현상이라든지 핀에 의한 잎 손상 등이 우려되고 있어 이에 대한 개선책이 필요하다. 본 연구는 플러그묘의 이식작업 시 잎 손상을 줄이면서 기계 적응성을 향상시킬 수 있는 이식시스템을 개발하기 위해 진공흡인을 이용한 이식 메커니즘에 대해 검토하였다. 플러그묘 이식시스템은 육묘트레이 셀을 X-Y로 옮기는 묘 이송부, 육묘트레이의 셀 하단으로부터 진공을 발생시켜 묘를 떨어뜨리는 진공 흡인부, 낙하되는 묘를 감지하는 센서와 블로워 및 공압 실린더로 구성된 진공 발생부, 혈공된 포트를 진공 발생부의 유도관으로 옮기는 포트 이송부 등으로 설계 제작하였다. 이식 메커니즘은 육묘트레이 하단부로부터 플러그묘를 1개씩 진공흡인하는 방식을 채택하였고, 이를 위해 상하 모두 개방된 72공 육묘트레이($L538{\times}W280{\times}H45mm$)를 윗부분(Ø35mm) 보다 아랫부분(Ø37mm)의 셀이 넓은 형상으로 PP재질의 육묘트레이를 사출금형 제작하였다. 묘 이송부에 장착된 플러그묘는 X축 방향(12개 셀)으로 이식작업이 이루어지고, Y축(6개 셀)으로 이동된 후 다시 동일한 방향으로 연속 작업이 가능하도록 제어프로그램을 구성하였다. 이식 원리는 진공 흡인부에 플러그묘가 이송되면 진공 발생부의 흡착패드가 위로 전진하여 진공을 발생시켜 묘를 흡인하고, 유도관 내에 부착된 광화이버센서에 의해 묘를 감지하여 블로워와 공압실린더를 제어함으로써 이식 공정이 끝나게 된다. 로메인상추의 플러그묘를 대상으로 진공흡인 시험을 실시한 결과 묘 손상없이 이식작업이 가능한 것으로 확인되었다.

• Composites Research
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• v.16 no.2
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• pp.62-67
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• 2003

Interfacial properties and damage sensing for the carbon fiber/epoxy-amine terminated (AT)-polyetherimide (PEI) composite were performed using microdroplet test and electrical resistance measurements. As AT-PEI content increased, the fracture toughness of epoxy-AT-PEI matrix increased, and interfacial shear strength (IFSS) increased due to the improved fracture toughness by energy absorption mechanisms of AT-PEI phase. The microdroplet in the carbon fiber/neat epoxy composite showed brittle microfailure mode. At 15 phr AT-PEI content ductile microfailure mode appeared because of improved fracture toughness. After curing, the change in electrical resistance $\Delta\textrm{R}$) with increasing AT-PEI content increased gradually because of thermal shrinkage. Under cyclic stress, in the neat epoxy case the reaching time until same stress was faster and their slope was higher than those of 15 phr AT-PEI. The result obtained from electrical resistance measurements under curing process and reversible stress/strain was correspondence well with matrix toughness properties.

• Geotechnical Engineering
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• v.13 no.4
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• pp.121-134
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• 1997

Vibrations induced by traffic loading and construction activities are extremely important due to their potential to cause damage to adjacent structures and toy complaints to the neighbors. Vibration induced damage to the built environment may be caused by the direct transmission of vibrations as well as by the, vibration induced differential settlement. In order to effectively control the vibration related problems, the accurate in-situ vibration monitoring is essential. In this paper, a calibration technique of a geophone which is widely used in practice was described. Once the frequency characteristics of individual geophones were calibrated, the 3fomponent geophone was developed for the in-depth vibration measurement, and the dot ailed calibration and application techniques of the 3fomponent geophone were described. Vibrations caused by blasting, train loading, and pile driving were measured and the applicability of the 3fomponent geophone was assessed.

• The Journal of the Acoustical Society of Korea
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• v.28 no.4
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• pp.308-317
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• 2009

In the present work, a sensor system composed of an oscillator sensor and a Lamb wave sensor is proposed for the purpose of structural health monitoring. The oscillator sensing system detecting the shift of a structural resonant frequency in proportion to the amount of defects in the structure is a pretty sensitive and simple device, but its detectable range is limited to its local zone. The Lamb wave sensor system, however, is applicable to global detection of the defects. This study is aimed at investigating the feasible combination of the two systems to exploits their merits simultaneously. The scheme to use PZT patches as the oscillator sensor as well as the Lamb wave sensor was proposed to identify the position, length and number of cracks by means of TOF and amplitude of signals, and its validity was confirmed through experiments.

• Journal of the Korean Society for Nondestructive Testing
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• v.30 no.5
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• pp.411-422
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• 2010

Self-sensing on micro-failure, dispersion degree and relating properties, of carbon nanotube(CNT)/epoxy composites, were investigated using wettability, electro-micromechanical technique with acoustic emission(AE). Specimens were prepared from neat epoxy as well as composites with untreated and acid-treated CNT. Degree of dispersion was evaluated comparatively by measuring volumetric electrical resistivity and its standard deviation. Apparent modulus containing the stress transfer was higher for acid-treated CNT composite than for the untreated case. Applied cyclic loading responded well for a single carbon fiber/CNT-epoxy composite by the change in contact resistivity. The interfacial shear strength between a single carbon fiber and CNT-epoxy, determined in a fiber pullout test, was lower than that between a single carbon fiber and neat epoxy. Regarding on micro-damage sensing using electrical resistivity measurement with AE, the stepwise increment in electrical resistivity was observed for a single carbon fiber/CNT -epoxy composite. On the other hand, electrical resistivity increased infinitely right after the first carbon fiber breaks for a single carbon fiber/neat epoxy composite. The occurrence of AE events of added CNT composites was much higher than the neat epoxy case, due to micro failure at the interfaces by added CNTs.