• Title/Summary/Keyword: 속시렛추출

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Comparison of Extraction Methods for the Analysis of Total Petroleum Hydrocarbons in Contaminated Soil (오염토양내 석유계 총탄화수소 분석을 위한 추출방법의 비교)

  • Eui-Young Hwang;Wan Namkoong;Jung-Young Choi
    • Journal of Korea Soil Environment Society
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    • v.5 no.2
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    • pp.45-53
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    • 2000
  • Two extraction methods for total petroleum hydrocarbon (TPH) from contaminated soil were evaluated. The soil used for this study was sandy loam. Diesel oil was selected as representative petroleum hydrocarbons and was spiked at 100, 10,000, 50,000mg TPH/kg dry soil. Percentage recovery of TPH by shaking method was higher compared to Soxhlet extraction. At extraction time of 2 hours and sample to solvent ratio of 1 : 5, the highest percentage recovery was obtained. In this condition, percentage recovery of TPH in soil contaminated with 100mg/kg and 50,000mg/kg as TPH was 95.9% and 95.5%, respectively The volume of solvent lost by volatilization in shaking method was relatively small compared to Soxhlet extraction.

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The usability evaluation of domestic urban sewage sludge as feedstock for biodiesel production( I ) - Comparison of the yields and composition of fatty acid methyl esters - (바이오디젤 생산을 위한 원료로서 국내 도시 하수슬러지의 활용성 평가( I ) - 지방산메틸에스테르(FAMEs)의 수율 및 조성 비교 -)

  • Kim, Nack-Joo;Jung, You-Won;Lee, Ik-Soo
    • Journal of Korean Society of Water and Wastewater
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    • v.26 no.1
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    • pp.115-121
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    • 2012
  • This study was performed to assess the possibility of application of sewage sludge which is the side-product from domestic sewage treatment plant to the materials for biodiesels by investigating the yields and composition of the lipids and fatty acid methyl esters(FAMEs) from soxhlet extraction and in-situ transesterification. As the results, yields of in-situ transesterification were higher than soxhlet extraction. In comparison by sewage sludge type, yields of sewage sludge mixed nightsoil or livestock were higher than a single sewage sludge. And maximum yield showed up to 14 wt%. Fatty acid composition of extracted lipids and synthesized FAMEs consists of palmitic acid(C16:0), palmitoleic acid(C16:1), stearic acid(C18:0), oleic acid(C18:1), and linoleic acid(C18:2).