• Journal of the Korean Society of Clothing and Textiles
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• v.25 no.2
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• pp.268-274
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• 2001

Dyeing properties of the colorants extracted from pomegranate hull on silk fabric were investigated. Pomegranate colorants were characterized by FT-IR analysis. Effects of dyeing condition and mordanting on dye uptake, color change and colorfastness were explored. Pomegranate colorants showed high affinity to silk fiber and its isotherm adsorption curve was Langmuir type. Therefore, ionic bond was involved in the adsorption of pomegranate colorants on to silk fiber. Mordants except Fe did not significantly increase dye adsorption. Pomegranate colorants produced mainly yellow color on silk fabric, but the silk mordanted with Fe showed yellow red color. Fastness to washing, perspiration, and rubbing was not improved by mordanting treatment, but light colorfastness was increased by Fe mordant.

• Journal of the Korean Society of Clothing and Textiles
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• v.25 no.3
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• pp.577-585
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• 2001

Dyeing properties of the colorants extracted from pomegranate hull on cotton fabric were investigated. Effects of dyeing conditions and mordanting on dye uptake, color change and colorfastness were explored. Cationic agent treatment was done for cotton to improve low dyeability in natural dyeing. In addition antimicrobial activity of the cotton fabrics dyed with pomegranate colorants was examined by the shake flask method. Pomegranate colorants showed low affinity to cotton fiber and its adsorption isotherm was Freundlich type. Therefore, hydrogen bonding was involved in the adsorption of pomegranate colorants onto cotton fiber. Mordants did not significantly increase dye adsorption. Pomegranate colorants produced mainly yellow color on cotton fabric. In order to improve dye uptake, cotton was cationized by treating with Cationon UK(quarterly ammonium salt) and chitosan. The cationized cotton with Cationon UK showed higher dye uptake and shorter dyeing time, compared with the untreated cotton. Chitosan treated cotton also showed high dye uptake, but chitosan was less effective compared with Cationon UK. Fastness to washing, perspiration, and rubbing was not improved by mordanting and cationizing treatment, but light fastness was increased by all mordants and cationic agent. As dye concentration increased, bacterial reduction rate was increased and mordants did not significantly increase bacterial reduction rate.

• 한국지구과학회:학술대회논문집
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• 2006.02a
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• pp.245-250
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• 2006

부여군 지선리에 있는 한국녹옥광산에서는 보석학 가치가 매우 우수한 귀사문석옥 광상이 형성되어 있다. 모암인 사문암은 페리도타이트와 같은 초염기성암이 저급변성작용 또는 열수변질작용을 받아 만들어진 것으로, 그 후 시대미상의 석류석맥의 관입함에 따라 양 접촉부에 귀사문석 광체가 형성되어 있다. 귀사문석옥은 안티고라이트 사문석이며, 그 광물조직이 모암인 사문암과는 크게 차이를 나타낸다. 짙은 녹색을 띠게 하는 발 색소는 주로 Fe이며, $755^{\circ}C$에서 탈수작용이 일어나며, $830^{\circ}C$에서 감람석으로 결정구조가 변한다. 이러한 실험적 사실은 모암인 사문암은 초염기성암이 열수변질작용을 받아 변한 것임을 의미한다.

• Journal of Conservation Science
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• v.28 no.2
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• pp.119-129
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• 2012

Excavated textiles provide very important research data on the costume culture of the Joseon dynasty. In particular, dyed textiles are indispensable for textile conservation research and for restoration of remains as well as for general costume culture research. Unfortunately, a prolonged burial environment causes the colors to change and gradually fade after excavation. Therefore, it is very difficult to identify the original color. In this study, natural dyed samples of red, yellow, purple and blue were prepared and analyzed using HPLC-PDA. Dyes of colorants extracted from excavated textile remains were analyzed by HPLC. In addition, mordants were analyzed using (SEM-EDX) in order to estimate the original color. The 16~17th Century's three samples were analyzed, sample 1, and 2 from Eunjin Song's Song Mun-Chang excavated at the Songchon-dong in Daejeon, and sample 3 from Yeosan Song's Song, Hee-Jong excavated at the Mokdal-dong in Daejeon. From the HPLC results, alizarin, purpurin, and indigo were detected on sample 1, alizarin and purpurin on sample 2, ellagic acid and indigo on sample 3. Therefore they were dyed with madder and indigo (sample 1), madder (sample2), pomagranted and indigo (sample 3). Al mordant was identified on three samples.