• Title/Summary/Keyword: 비등 수

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Changes in Properties of Silk Monofilament Caused by Drawing and Hydrolysis (견 Monofilament의 연신과 가수분해에 의한 특성변화)

  • 김동건;최진협
    • Journal of Sericultural and Entomological Science
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    • v.38 no.2
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    • pp.160-167
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    • 1996
  • The middle silk gland, that is a liquid silk thread gland consisting of silk protein, was taken out and a silk monofilament was made by drawing rapidly to approximately 3 times. In order to deteriorate the inter molecular hydrogen bonding force and to stretch in, the drawn silk filament was swoolen in boiling water. The results obtained are as follows ; The silk gland sample that just dried silk gland was occupied in crystalline region of silk-I type and random amorphous region. According to the examination of X-ray diffraction and thermal analysis, silk-II type crystal begins to appear partially in monofilament sample and spread to almost complet silk-II type crystal in 65.2% drawn sample. And, orientation of silk fibroin mlecule increased suddenly in early stage with a rise of drawing ratiofrom birefringence and density, and it was found that orientation of fibroin molecule was completed. As drawing ratio increases relation with time of hydrolysis, birefringence appeared almost fixed a tendency. Crystallization collapse by hydrolysis was not found in X-ray diffraction and thermal analysis. But, amorphous region began to flow by treated hydrolysis, that orientation of crystallization part was disturbed was supposed.

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A Floristic Study on the Economic Planys of Jisimdo, Naedo and Yundoldo around Koje Island (거제도 인근도서(지심도, 내도, 윤돌도)의 자원식물상 연구)

  • Woo Bok-ju;Park Seong-Jun;Hwang Gyu-Jin;Kim Kum-Suk;Lee Jeung-Wook;Park Seon-Joo
    • Korean Journal of Plant Resources
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    • v.18 no.3
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    • pp.479-489
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    • 2005
  • The floras of Jisimdo, Naedo and Yundoldo around Koje Island were investigated 3 times from January 2004 to November 2004. The vascular plants recorded were 165 taxa, 1 forms, 15 varieties, 149 species, 140 genera, 72 families, The rare and endangered plants were recorded as 1 taxa (Quercus gilva Blume), Korean endemic plants were recorded as 2 taxa (1 variety, 1 species, 2 genera, 2 families). The naturalized plants were 10 taxa, 10 species, 10 genera, 6 families, $3.52\%\;and\;6.1\%$ among the total naturalized plants and Urbanization Index in Korea. Anglers and visiter's number is expected to increase fast because nature of Jisimdo, Naedo and Yundoldo, in which kind and number of naturalized plants are forecasted to be increased more.

A Hippocampus Segmentation in Brain MR Images using Level-Set Method (레벨 셋 방법을 이용한 뇌 MR 영상에서 해마영역 분할)

  • Lee, Young-Seung;Choi, Heung-Kook
    • Journal of Korea Multimedia Society
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    • v.15 no.9
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    • pp.1075-1085
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    • 2012
  • In clinical research using medical images, the image segmentation is one of the most important processes. Especially, the hippocampal atrophy is helpful for the clinical Alzheimer diagnosis as a specific marker of the progress of Alzheimer. In order to measure hippocampus volume exactly, segmentation of the hippocampus is essential. However, the hippocampus has some features like relatively low contrast, low signal-to-noise ratio, discreted boundary in MRI images, and these features make it difficult to segment hippocampus. To solve this problem, firstly, We selected region of interest from an experiment image, subtracted a original image from the negative image of the original image, enhanced contrast, and applied anisotropic diffusion filtering and gaussian filtering as preprocessing. Finally, We performed an image segmentation using two level set methods. Through a variety of approaches for the validation of proposed hippocampus segmentation method, We confirmed that our proposed method improved the rate and accuracy of the segmentation. Consequently, the proposed method is suitable for segmentation of the area which has similar features with the hippocampus. We believe that our method has great potential if successfully combined with other research findings.

Structural Segmentation for 3-D Brain Image by Intensity Coherence Enhancement and Classification (명암도 응집성 강화 및 분류를 통한 3차원 뇌 영상 구조적 분할)

  • Kim, Min-Jeong;Lee, Joung-Min;Kim, Myoung-Hee
    • The KIPS Transactions:PartA
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    • v.13A no.5 s.102
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    • pp.465-472
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    • 2006
  • Recently, many suggestions have been made in image segmentation methods for extracting human organs or disease affected area from huge amounts of medical image datasets. However, images from some areas, such as brain, which have multiple structures with ambiruous structural borders, have limitations in their structural segmentation. To address this problem, clustering technique which classifies voxels into finite number of clusters is often employed. This, however, has its drawback, the influence from noise, which is caused from voxel by voxel operations. Therefore, applying image enhancing method to minimize the influence from noise and to make clearer image borders would allow more robust structural segmentation. This research proposes an efficient structural segmentation method by filtering based clustering to extract detail structures such as white matter, gray matter and cerebrospinal fluid from brain MR. First, coherence enhancing diffusion filtering is adopted to make clearer borders between structures and to reduce the noises in them. To the enhanced images from this process, fuzzy c-means clustering method was applied, conducting structural segmentation by assigning corresponding cluster index to the structure containing each voxel. The suggested structural segmentation method, in comparison with existing ones with clustering using Gaussian or general anisotropic diffusion filtering, showed enhanced accuracy which was determined by how much it agreed with the manual segmentation results. Moreover, by suggesting fine segmentation method on the border area with reproducible results and minimized manual task, it provides efficient diagnostic support for morphological abnormalities in brain.

Pyrolysis Characteristics of Sawdust and Rice Husk (톱밥과 왕겨의 열분해 특성 연구)

  • Park, Dong Kyoo;Seo, Myung Won;Goo, Jeong Hoi;Kim, Sang Done;Lee, See Hoon;Lee, Jae Goo;Song, Byung-Ho
    • Applied Chemistry for Engineering
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    • v.18 no.5
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    • pp.415-423
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    • 2007
  • Pyrolysis characteristics of sawdust and rice husk as biomass resources in a thermogravimetric analysis were determined. Experiments were carried out with a linear heating rate under inert atmosphere of $N_2$ gas. Pyrolysis of the biomass can be classified as a lower temperature reaction zone where the major component of holocellulose is thermally decomposed and a high temperature reaction zone where lignin is thermally decomposed. The obtained data was analyzed by the two-step consecutive reaction model. Activation energies of sawdust and rice husk are found to be respectively 82.5 kJ/mol and 85.1kJ/mol in the low temperature zone according to the first order reaction model and 19.7 kJ/mol, 22.0 kJ/mol in the high temperature zone according to the three-way transport model. The reaction rate constant with variation of heating rate can be well predicted by the kinetic compensation relation of Gaur-Reed.

Chemical and Functional Characteristics of Mechanically Deboned Chicken Meat and its Utilization in Processed Meat -II. Utilization of Mechanically Deboned Chicken Meat- (기계발골가금육(機械拔骨家禁肉)의 특성(特性) 및 이용(利用)에 관(關)한 연구(硏究) -제(第) 2 보(報) : 기계발골가금육(機械拔骨家禁肉)의 이용(利用)-)

  • Kim, Jong-Won;Ahn, Byung-Yoon;Lee, Yu-Bang
    • Korean Journal of Food Science and Technology
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    • v.13 no.3
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    • pp.176-180
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    • 1981
  • Chicken patties and frankfurters were manufactured by varying the relative proportion of MDM to HDM as raw materials, and their palatability, shelf-life and textural properties were evaluated. The obtained results were as follows: 1. Chicken patty containing MDM slowed gradual increase in TBA value during frozen storage, but its storage up to g weeks presented no problems in flavor stability. 2. Color score and total palatability of chicken patty were best for the product containing 30% MDM. It was also concluded that MDM can be included in the patties up to 50% of total meat with good results, but more than 70% was not recommended. 3. The formulation of MDM up to 50% in frankfurter gave a quite satisfactory acceptability and textural properties compararable to frankfurter made of 100% HDM, but the inclusion of more than 70% MDM was not recommended. 4. The TBA value of frankfurter containg MDM did not increase to any great extent until 4 weeks of storage at $4^{\circ}C$, indicating no unique problems in flavor instability compared to regular frankfurter. 5. It was concluded that processed meat products such as patties and frankfurters containing MDM up to $30{\sim}35%$ of total meat ingredients gave satisfactory results in color, texture and palatability, comparable to regular products.

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Studies on Fluid Inclusion and Pyrite Geochemistry in the Moisan Au-Ag Deposit, Haenam District, Korea (해남 모이산 금-은 광상의 유체포유물 및 황화물 지구화학 연구)

  • Park, Sol;Seo, Jung Hun;Kim, Chang Seong;Yang, Yoon-Seok;Oh, Jihye;Kim, Jonguk
    • Economic and Environmental Geology
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    • v.53 no.3
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    • pp.221-234
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    • 2020
  • We occur together with telluride minerals. Fluid inclusions in the euhedral quartz crystals are mainly aqueous liquid-rich inclusions, which have salinities about 0.18-2.24 wt% NaCl equivalent. Some quartz vein contains aqueous vapor-rich inclusions as well. Homogenization temperatures of the assemblages of the liquid-rich inclusions are about 141-384 ℃, and the temperatures are lower at the shallower vein samples. In the high Au-Ag grade depth intervals, relatively deeper fluids have relatively higher salinities and homogenization temperatures, while shallower fluids show somewhat wider ranges. These might indicate that the deep Au-Ag bearing hydrothermal fluids at the Moisan area experienced phase separation as well as mixing with meteoric water by decreasing pressure. Au-Ag precipitation in the Moisan deposit is not associated with pyrite, but pyrite include Au-Ag bearing phase as an inclusion, which might possibly be tellurides or electrum. Au/Ag ratios in the Au-Ag bearing phase do not change with different depth.

High Tc Superconductor Fiber $YBa_2Cu_3O_{7-{\sigma}}$ Synthesized by the Sol-gel Process (Sol-gel 법에 의한 고온 초전도체 $YBa_2Cu_3O_{7-{\sigma}}$ 선재 합성에 관한 연구)

  • Jin Ho Choy;Jong Seok Yoo;Bae Whan Kim;Seung Tae Hong
    • Journal of the Korean Chemical Society
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    • v.33 no.3
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    • pp.326-331
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    • 1989
  • Superconducting fiber of high Tc $YBa_2Cu_3O_{7-{\sigma}}$ was successfully prepared by the sol-gel method. The stoichiometric mixture of Y, Ba and Cu nitrates was dissolved in water, to which citric acid solution was added. Then ammonium hydroxide was added to the mixture in order to increase the pH to a value between 5.8 and 6.2. The mixture was heated carefully to form a homogeneous colloid sol at 358 K. The solution was viscous enough to draw a long gel fiber, which was then heated at 1223K for 8 hrs. under oxygen partial pressure of $Po_2$ = 1 atm., cooled slowly and annealed at 723K for 13 hrs.. The reacted superconducting sample maintained a fiber form with some shrinkage of its volume. The superconducting transition temperatures (Tc, onset and Tc, offset) of $YBa_2Cu_3O_{7-{\sigma}}$ have been determined to be approximately 95K and 82K, respectively. The superconducting phase was also confirmed by Meissner effect at liquid nitrogen boiling temperature.

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Kinetic Studies of CO2 Gasification by Non-isothermal Method on Fly Ash Char (비등온법에 의한 비산재 촤의 CO2 가스화 특성)

  • Kang, Suk-Hwan;Ryu, Jae-Hong;Lee, Jin-Wook;Yun, Yongseung;Kim, Gyoo Tae;Kim, Yongjeon
    • Korean Chemical Engineering Research
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    • v.51 no.4
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    • pp.493-499
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    • 2013
  • For the purpose of utilizing fly ash from gasification of low rank coal, we performed the series of experiments such as pyrolysis and char-$CO_2$ gasification on fly ash by using the thermogravimetric analyzer (TGA) at non-isothermal heating conditions (10, 20 and $30^{\circ}C/min$). Pyrolysis rate has been analyzed by Kissinger method as a first order, the reliability of the model was lower because of the low content of volatile matter contained in the fly ash. The experimental results for the fly ash char-$CO_2$ gasification were analyzed by the shrinking core model, homogeneous model and random pore model and then were compared with them for the coal char-$CO_2$ gasification. The fly ash char (LG coal) with low-carbon has been successfully simulated by the homogeneous model as an activation energy of 200.8 kJ/mol. In particular, the fly ash char of KPU coal with high-carbon has been successfully described by the random pore model with the activation energy of 198.3 kJ/mol and was similar to the behavior for the $CO_2$ gasification of the coal char. As a result, the activation energy for the $CO_2$ gasification of two fly ash chars don't show a large difference, but we can confirm that the models for their $CO_2$ gasification depend on the amount of fixed carbon.

고온 GaN 버퍼층 성장방법을 이용한 비극성 a-plane GaN 성장 및 특성평가

  • Park, Seong-Hyeon;Kim, Nam-Hyeok;Lee, Geon-Hun;Yu, Deok-Jae;Mun, Dae-Yeong;Kim, Jong-Hak;Yun, Ui-Jun
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.02a
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    • pp.125-125
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    • 2010
  • 극성 [0001] 방향으로 성장된 질화물 기반의 LED (light emitting diode) 는 분극현상에 의해 발생하는 강한 내부 전기장의 영향을 받게 된다. 이러한 내부 전기장은 양자우물 내의 전자와 정공의 공간적 분리를 야기하고 quantum confined Stark effect (QCSE)에 의한 발광 파장의 적색 편이가 발생하며 양자효율의 저하를 가져오게 된다. 이러한 문제를 해결하기 위해 InGaN/GaN이나 AlGaN/GaN 양자 우물구조를 GaN의 m-plane (1$\bar{1}$00) 이나 a-plane (11$\bar{2}$0) 등 비극성면 위에 성장하려는 시도를 하고 있다. 그러나 비극성 면의 비등방성 (anisotropy) 으로 인하여 결정성이 높은 비극성 GaN을 성장하는 데에는 많은 어려움이 있다. GaN 층의 표면을 평탄화하고 결정성을 향상시키기 위해서 저온 GaN 또는 AlN 버퍼층을 성장하는 2단계 방법이나 고온 버퍼층을 이용하여 성장하는 연구들이 많이 진행되고 있다. 본 연구에서는 고온 GaN 버퍼층을 이용하여 기존의 2단계 성장과정을 단순화한 비극성 a-plane GaN을 r-plane 사파이어 기판위에 유기금속 화학증착법 (MOCVD)으로 성장하였다. 사파이어 기판위에 AlN 층을 형성하기 위한 nitridation 과정 후 1030 도에서 두께 45 ~ 800 nm의 고온 GaN 버퍼층을 성장하고 총 박막 두께가 2.7 ~ 3 um 가 되도록 a-plane GaN을 성장하여 표면 양상의 변화와 결정성을 확인하였다. 또한 a-plane GaN 박막 성장 시에 성장 압력을 100 ~ 300 torr 로 조절하며 박막 성장의 변화 양상을 관찰하였다. 고온 GaN 버퍼층 성장 두께가 감소함에 따라 결정성은 증가하였으나 표면의 삼각형 형태의 pit 밀도가 증가함을 확인하였다. 또한 성장 압력이 감소함에 따라 표면 pit은 감소하였으나 결정성도 감소하는 것을 확인하였다. 성장 압력과 버퍼층 성장 두께를 조절하여 표면에 삼각형 형태의 pit이 존재하지 않는 RMS roughness 0.99 nm, 관통전위밀도 $1.78\;{\times}\;10^{10}/cm^2$, XRD 반가폭이 [0001], [1$\bar{1}$00] 방향으로 각 798, 1909 arcsec 인 a-plane GaN을 성장하였다. 이 연구를 통해 고온 GaN 버퍼 성장방법을 이용하여 간소화된 공정으로 LED 소자 제작에 사용할 수 있는 결정성 높은 a-plane GaN을 성장할 수 있는 가능성을 확인하였다.

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