• Journal of the Society of Cosmetic Scientists of Korea
• /
• v.30 no.3 s.47
• /
• pp.399-404
• /
• 2004

Novel GHK-conjugated chitosan was prepared by the solid-phase method using $N^{\alpha}-Fmoc$ amino acids/BOP coupling reagent. For this purpose, the chitosan microbeads which had a mean diameter of 70 um were prepared by the W/O emulsion-phase separation method. The GHK was successfully coupled to the chitosan microbeads by stepwise solid-phase method. The result of amino aid analysis was in good agreement with the theoretical values; $Gly_{1.02}\;of\;His_{1.13}\;Lys_{0.96).$. The cell proliferation effect of the GHK-bound chitosan microbeads was measured by MTT assay. We concluded that GHK-bound chitosan microbeads gave higher cell Proliferation effect than chitosan microbeads.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.41 no.4
• /
• pp.321-327
• /
• 2017

In this study, to investigate the shape of the back bead as a weld quality parameter and to select the optimal condition of the root-pass TIG welding of a horizontal butt-joint, an experimental design and the response surface method (RSM) have been employed. Three parameters are used as input variables, which include the base current, peak current, and welding speed. The back bead width is selected as an output variable representing the weld quality, the target value of the width is 5.4 mm. Conducting the experiments according to the Box-Behnken experimental design, a $2^{nd}$ regression model for the back bead width was made, and the validation of the model was confirmed by using the F-test. The desirability function was designed through the nominal-the-best formula for the appropriate back bead width. Finally, the following optimal condition for welding was selected using the RSM: base current of 0.9204, peak current of 0.8676, and welding speed of 0.3776 in coded values. For verification, a test welding process under the optimal condition was executed and the result showed the back bead width of 5.38 mm that matched the target value well.

• Polymer(Korea)
• /
• v.33 no.1
• /
• pp.33-38
• /
• 2009

Monodisperse polystyrene and its copolymer beads containing amine function were prepared for the electroless silver plating using reduction of silver alkylcarbamate complex in organic solvent. Soap-free emulsion polymerization was adopted for the polymerization of styrene, divinylbenzene (DVB), and 2-(N,N-dimethylamino) ethyl methacrylate (DAEMA) in the presence of poly (vinyl alcohol) in a water/methanol solvent. The resulting poly (styrene/DVB/DAEMA), containing 30/0$\sim$1.5/0$\sim$3 wt% in monomer composition, were found to be a sphere-type particle with diameter of 1 ${\mu}m$. Silver Ag-coated polystyrene beads were prepared by in sito reduction of a silver 2-ethylhexylcarbamate (Ag-EHCB) complex solution with hydrazine without pretreatment of polystyrene beads. Robust Ag/polystyrene beads were analyzed by SEM, UV -visible spectrometer and XRD.

• Transactions of the Korean Society of Machine Tool Engineers
• /
• v.16 no.3
• /
• pp.81-87
• /
• 2007

It is important to investigate the relationship between weld process parameters and weld bead geometry for adaptive arc robot welding. However, it is difficult to predict an exact back-bead owing to gap in process of butt welding. In this paper, the quantitative prediction system to specify the relationship external weld conditions and weld bead geometry was developed to get suitable back-bead in butt welding which is widely applied on industrial field. Multiple regression analysis and artificial neural network were used as the research methods. And, the results of two prediction methods were compared and analyzed.

• Proceedings of the Korean Magnestics Society Conference
• /
• 2012.11a
• /
• pp.146-148
• /
• 2012

미크론 자성비드 검출용 바이오센서에 활용하는 GMR-SV 박막을 이온빔 스퍼터링 증착법으로 glass/Ta(5.8 nm)/NiFe(5 nm)/Cu(t nm)/NiFe(3 nm)/FeMn(12 nm)/Ta(5.8 nm)의 구조를 갖도록 증착하였다. 비자성체 Cu의 두께가 3.0 nm에서 2.2 nm까지 얇아질수록 교환결합력은 증가하였으며 자기저항비는 다소 낮았다. 비자성체의 두께가 얇으면 반강자성체의 층간 교환작용이 강자성체의 고정층 뿐만 아니라 자유층의 스핀배열에도 영향을 주고 있음을 확인할 수 있었다. 또한 리소그래피 공정 과정을 거쳐 GMR-SV 소자를 제작하여 미트론 자기비드를 검출하였다. 여기서 자기비드를 떨어뜨리기 전과 후의 자기저항비, 교환결합력, 보자력은 각각 0.9%, 3 Oe, 2 Oe의 값을 나타내었다. 이것으로 미크론단위의 바이오센서로서 활용할 수 있는 가능성을 보여주었다.

• Proceedings of the KWS Conference
• /
• 2009.11a
• /
• pp.28-28
• /
• 2009

최근 전세계적으로 유가 상승 및 배기가스 배출 저감과 관련된 각종 환경규제에 대응하기 위하여 선진 자동차회사들은 $CO_2$ 배출 저감 기술과 기존 내연기관 차량의 연비향상을 위해 엔진성능 개선, 구동시스템의 최적화, 차량 경량화, 공기저항 감소 등에 초점을 맞춰 차량의 연비향상과 배기가스 규제에 대응하고 있다. 특히, 자동차 중량의 30%를 차지하는 차체의 경량화는 엔진효율을 높여 자동차의 성능향상을 극대화시키고, 그로 인해 연비향상을 도모할 수 있으므로 환경오염 방지와 연료절감에 가장 적합하고 효과적인 방법이다. 이에 기존의 강재에 비해 비중이 낮으면서 유사한 강도와 내식성이 뛰어난 알루미늄 합금의 차체 적용에 대한 연구가 진행되고 있다. 본 연구에서는 자동차 Door에 알루미늄 합금(Al 5052)의 적용 가능성을 판단하기 위해 반응표면분석법(Response surface methodology)을 이용하여 저입열 Pulse MIG 용접 공정변수를 최적화하였다. 첫째, 저입열 Pulse MIG 용접에서 용접 공정 변수(용접전압, 용접속도, Gap)의 변화가 비드 형상에 미치는 영향에 대해 평가하였다. 요인분석법을 이용하여 용접 공정 변수와 비드 형상 변수와의 주효과와 교호작용효과를 분석하였고, 이를 통해 비드 형상 변수에 영향을 크게 미치는 용접 공정변수를 선별하여 다중회귀분석을 통해 용접 공정 변수 변화에 따른 비드형상 예측 회귀모델을 제안하였다. 둘째, 자동차 Door 생산 현장에서 박판 알루미늄 합금 겹치기 용접 이음부의 0~1 mm 갭 발생에 대해 강건한 용접조건을 제시하기 위해 반응표면법(Response surface methodology)을 이용하여 저입열 Pulse MIG 용접 공정 변수를 최적화하였고, 그 적용 가능성을 확인하였다.

• Journal of the Korea Academia-Industrial cooperation Society
• /
• v.10 no.11
• /
• pp.3269-3273
• /
• 2009

In this study, recycling methods of nano $TiO_2$-coated silica-bead were conducted in order to solve a deactivation problem of bead that had been invented for decomposition of pollutants in aqueous solution. Surface cleansing was selected as the recycling method for used beads. The surface cleansing was done with four different solutions such as distilled water, surfactant, acetone, and ethyl alcohol(ethanol). The recycling process consists of cleansing and calcination. After cleaning the used (deactivated) beads, calcination was done at $100^{\circ}C$, $200^{\circ}C$ and $300^{\circ}C$ for 30 minutes, respectively. This process was repeated three times. The activity of the recycled bead was measured by photo-degradation of methylene blue. The result shows that acetone cleansing and calcination at $100^{\circ}C$ for 30 minutes was the most efficient recycling method.

• Proceedings of the Computational Structural Engineering Institute Conference
• /
• 2010.04a
• /
• pp.624-627
• /
• 2010

최근 자동차 업계서는 차량의 온실가스 배출량을 줄이고 연비를 개선시킬 수 있는 방법 중의 하나로 경량화 소재를 사용하여 차체의 중량을 줄이는 연구가 활발히 진행 중에 있다. 특히 알루미늄 합금의 경우 기존 강재에 비해 비중이 낮아 가볍고 부식에 대한 저항성이 높아 많이 사용되어지고 있는 추세이다. 본 연구에서는 먼저, 저입열 용접공정을 적용하여 용접 변수와 토치의 각도에 따른 인장강도 특성을 비교하여 적정 용접 범위를 산정하였으며, 인장강도와 비드형상의 관계를 다중 회귀 분석을 이용하여 비드 예측 회귀 모델을 제시하였다. 또한 호감도 함수를 적용한 반응표면분석법을 이용하여 자동차 생산 현장에서 겹치기 용접 이음부의 강건한 용접 품질을 가질 수 있는 최적용접 공정 조건을 도출할 수 있는 효과적인 방법을 제안하고자 한다.

• Transactions of the Korean Society of Mechanical Engineers
• /
• v.19 no.8
• /
• pp.1844-1853
• /
• 1995

Theoretical and experimental drawing characteristics for the single circular and square drawbeads are discussed. During the blank holding process, the strain distributions of upper and lower skins of specimens, and the die reactional forces are analysed by F. E. M., and they are compared with the experimental results. The drawbead restraining forces and strain distributions for the drawn specimens by the various drawing length are also analysed and compared with the experimental results. It is concluded that the theoretical simulations and results could be very useful for the prediction of real cases.

• Transactions of the Korean Society of Machine Tool Engineers
• /
• v.16 no.4
• /
• pp.79-86
• /
• 2007

The shape of excessive penetration mainly depends on welding conditions(welding current and welding voltage), and welding process(groove gap and welding speed). These conditions are the major affecting factors to width and height of back bead. In this paper, back-bead prediction and weldability estimation using artificial neural network were investigated. Results are as follows. 1) If groove gap, welding current, welding voltage and welding speed will be previously determined as a welding condition, width and height of back bead can be predicted by artificial neural network system without experimental measurement. 2) From the result applied to three weld quality levels(ISO 5817), both experimented measurement using vision sensor and predicted mean values by artificial neural network showed good agreement. 3) The width and height of back bead are proportional to groove gap, welding current and welding voltage, but welding speed. is not.