• Polymer(Korea)
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• v.30 no.3
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• pp.224-229
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• 2006

Quaternary ammonium salt terminated silane was prepared from aminopropyldimethylethoxysilane with methyliodide and ionized 7,7,8,8-tetracyanoquinodimethane $(Li^+TCNQ^-)$ was prepared from TCNQ with methyliodide and lithium iodide. Quaternary ammonium salt silane-TCNQ adduct (ST) was prepared by reacting quaternary ammonium salt terminated silane with $Li^+TCNQ^-$ solution. Poly (dimethylsiloxane)-ST adduct (PST) was prepared by condensation of $\alpha,\omega-hydroxyl$ group terminated poly (dimethylsiloxane) (PDMS) with ST. Maleated polyethylene modified with PDMS (PST-g-MPE) was prepared by melt polymerization of maleated PE and PST in internal mixer and PST-g-MPE/carbon black (CB) and MPE/CB composites were prepared by compounding PST with MPE and PST-g-MPE, respectively. The thermal and mechanical properties of the composites were measured and dispersion characteristics of CB in matrix rosins show that the dispersion of CB in PST-g-MPE/CB was better than that of MPE/CB composite.

• Applied Chemistry for Engineering
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• v.8 no.1
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• pp.76-83
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• 1997

Blends of thermotropic liquid crystalline polymer(TLCP) with poly(ethylene terephthalate) (PET) were prepared by the coprecipitation from a common solvent. The blends were processed through a capillary die at $287^{\circ}C$ to produce a monofilament. Morphology and mechanical, thermal properties of blends and composites were examined by differential scanning calorimetry(DSC), tensile test, optical microscopy and scanning electron microscopy. Crystallization kinetics of the blends were investigated by the isothermal DSC method. The Avrami analyses were applied to obtain the information on the crystal growth geometry and factors controlling the rate of crystallization. In the blends, liquid crystalline phase did not reveal any significant macrophase separation and thermal degradation at the processing temperature. From scanning electron micrographs of cryogenic fracture surfaces of extruded fibers, the TLCP domains were found to be more or less finely dispersed with $0.1{\mu}m$ to $0.2{\mu}m$ in size. Interfacial adhesion between the TLCP and matrix polymer was excellent. Tensile strength and modulus of TLCP/PET in-situ fiber composites were enhanced with increasing draw ratio and LCP content.

• Spatial Information Research
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• v.10 no.2
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• pp.201-213
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• 2002

Chemical analyzes were carried out the samples from roadsides of the Gwangju city. The purpose of this research is to investigate the concentrations and distribution patterns of heavy metals due to urbanization and industrialization in the Gwangju city This study area is not significantly contaminated based on the concentrations of Cd, Cu, Fe, Mn, Pb and Zn. However, the concentrations of the chemical elements analyzed are locally higher than those of serious contamination level indicated by Ministry of environment. The dust pH is in the rage of 5.60-7.09 and was generally neutral, and there are no difference in pollution area and nonpollution area. Chemical analyses utilized are dilution by 0.1N HCl. In result of analysis by the method using 0.1N HCl, concentrations of Cd and Cu are a little high in Gwangchondong of Seo-Gu. Concentrations of Mn and Pb are a little high in Buk-Gu and Nam-gu, and Concentrations of Zn are generally higher than average of soils. Zn, in the study area, keeps polluting greatly as Zn concentration of average is 150.9ppm. All of P.I values are lower than 1, it means heavy metal pollution is not serious.

• Applied Chemistry for Engineering
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• v.28 no.2
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• pp.245-251
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• 2017

In this study, ZnO, which is widely known as a non $TiO_2$ photocatalyst, was synthesized using coprecipitation method and Ag was added in order to improve the catalytic performance. The physicochemical characteristics of the synthesized ZnO and Ag/ZnO particles were checked using X-ray diffraction (XRD), UV-visible spectroscopy, scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS), photoluminescence (PL), and photocurrent measurements. The performance of catalysts was tested by $H_2$ production using the photolysis of $H_2O$ with MeOH. By adding Ag which plays a role as an electron capture on the ZnO catalyst, the performance increased due to the recombination of excited electrons and holes. In particular, $8.60{\mu}mol\;g^{-1}$ $H_2$ was produced after 10 h reaction over the 0.50 mol% Ag/ZnO.

• Journal of the Korean Society of Radiology
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• v.14 no.6
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• pp.819-825
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• 2020

The purpose of this study was to evaluate the usefulness of the developed air mattress for reducing the deterioration of image quality due to the scattered radiation generated on the computed tomography equipment table. 5 cm and 10 cm thick air mattresses were developed and the image quality was measured by scanning the AAPM phantom according to thickness and thickness. Statistical significance was confirmed by One Way Analysis of Variance(ANOVA) Compared with the AAPM phantom scanned in the standard method, the image with the air mattress did not show any difference, but when the air mattress was not applied, the CT number and uniformity were low and the noise was high, and the spatial resolution Respectively. The developed air mattress has no harmful effect on the diagnostic image, it is very effective in improving the image quality and can increase the CT image quality by simply applying Air Mattress to existing equipment without using the technology applied to the latest and high-cost equipment.

• Journal of the Korean Society of Fisheries and Ocean Technology
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• v.26 no.3
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• pp.295-302
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• 1990

In this paper, a methodology for the automatic design of the optimal systolic arrays is proposed. Algorithm transformation is the main mathematical tool on which this methodology is based. Also, technique for partitioning algorithm into systolic arrays is presented. Algorithm partitioning is essential when the size of the computational problem is larger than the size of the array. This study results in (a) reduction of the design time of systolic arrays for given algorithms, (b) CRT display of the structures of systolic arrays, and (c) automatic designing of the optimal systolic array by the criteria such as the number of processing elements, bands, and communication paths. The procedure for these results was programmed using HP BASIC language on HP-9836 computer.

• Journal of the Korean Ceramic Society
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• v.41 no.3
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• pp.202-209
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• 2004

Hydroxyapatite(HA)/TiO$_2$ composite powders were prepared by mixing of spherical TiO$_2$ (10-15 nm, 500 nm) and needle-shaped HA (50-70 nm, 120-250 nm) powders which had been synthesized through precipitation, sol-gel and hydrothermal methods. From the three types of starting composite powders (HA/TiO$_2$ wt% of 75/25, 50/50, and 25/75), dense $\beta$-TCP/TiO$_2$ composites were prepared by hot-pressing at 800-100$0^{\circ}C$ for 30 min under the pressure of 30 ㎫ in Af atmosphere. The $\beta$-TCP/TiO$_2$ composites showed different microstructures and sintering densities depending on their powder morphology, composition and sintering temperature. With increasing the sintering temperature and the content of TiO$_2$, sintered density was increased and microstructure became more homogeneous.

• The Journal of Korean Institute of Electromagnetic Engineering and Science
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• v.20 no.11
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• pp.1186-1193
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• 2009

In this paper, we propose DDS(Direct Digital Synthesizer) as a new implementation method of chirp LO(Local Oscillator) for compressive receiver applied for RFID signal detection in UHF band. We designed a receiver whose input frequency range is 908.5~914 MHz, DDL(Dispersive Delay Line) bandwidth is 6 MHz, and dispersion delay time is $13\;{\mu}s$. Chirp LO based on DDS is designed to meet $26\;{\mu}s$ sweep time and 12 MHz bandwidth for complete compressive mechanism. The measured 3 dB pulse width of the compressed signal of the fabricated receiver is 260 ns and the frequency resolution for simultaneous input signals is below 200 kHz. These performances indicate that the proposed chirp LO based on DDS and the compressive receiver is suitable for RFID signal detection in UHF band.

• Journal of Korean Tunnelling and Underground Space Association
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• v.5 no.1
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• pp.13-21
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• 2003

To investigate the safety and stability of a concrete lining, numerous studies have been conducted over the years and several methods have been developed. Most signal processing techniques of NDT have been based on Fourier analysis. However, the application of Fourier analysis to analyze recorded vibrational signal shows results in the frequency domain only, and it is not enough to analyze transient waves precisely. In this study, Wavelet theory was employed for the analysis of non-stationary wave induced by mechanical impact on tunnel concrete lining. The Wavelet transform of transient signals provides a method for mapping the frequency spectrum as a function of time. To verify the availability of Wavelet transform as a time-frequency analysis tool, model experiments have been conducted and the thickness of the concrete lining was estimated based on the proposed theory. From this study, it was found that the contour map by Wavelet transform provides more distinct results than the power spectrum by Fourier transform and it was also found that Wavelet transform was also an effective tool for the analysis of dispersive waves in tunnel concrete linings.

• Polymer(Korea)
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• v.38 no.2
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• pp.240-249
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• 2014

Multi-walled carbon nanotube (MWNT) reinforced poly(ethylene terephthalate) (PET) composites are studied. To increase the interfacial interactions between PET and MWNTs, the MWNTs are functionalized with bishydroxy-ethylene-terephthalate (BHET). The functionalized MWNTs are melt blended into PET matrix using a twin screw extruder. The amount of MWNTs loaded in PET matrix ranges from 0.5 to 2.0 wt%. After compounding and spinning, the filaments are post-drawn and annealed. To verify the chemical modifications of carbon nanotubes, Raman, $^1H$ NMR, XPS, TGA and FE-SEM are used. The nanocomposites are also analyzed with DSC, TGA, and UTM. These tests show that crystallization temperature and thermal degradation temperature increase due to the functionalized MWNTs. Also, tensile test shows that yield strength and toughness increase more than 30% with addition of only 1 wt% of MWNTs. These results show that the introduction of BHET onto the MWNTs is a very effective way in manufacturing MWNT/PET composite.