• Journal of the Korean Ceramic Society
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• v.40 no.5
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• pp.447-454
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• 2003

Samples were prepared by the solid-state reaction method. The nominal composition of the samples was B $i_{1.84}$P $b_{0.34}$S $r_{1.91}$C $a_{2.03}$C $u_{3.06}$ $O_{10+{delta}$ prepared from powder of B $i_2$ $O_3$, PbO, SrC $O_3$, CaC $O_3$, and CuO. They were pulverized, mixed with AgO, A $u_2$ $O_3$and MgO of 50 wt%. Finally, they were sintered at 820 to 85$0^{\circ}C$ in air. The structural characteristics, the microstructure of surface and the critical temperature with respect to the each samples were analyzed by XRD, $T_{c}$, SEM and EDS respectively. It was found that the the critical temperature of the silver oxide additive samples (99.58 K) is higher than those of gold or magnesium oxides additive samples, but all those values are lower than that of pure Bi-2223 phase. The microstructure of surface showed the tendency which the AgO additive samples become more minuteness than A $u_2$ $O_3$ and MgO additive samples.s.samples.s.

• Resources Recycling
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• v.17 no.2
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• pp.70-75
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• 2008

A study on the cementation for the recovery of tin with aluminium in the hydrochloric acid solution was carried out. Parameters, such as aluminium metal equivalent, pH, reaction time, reaction temperature and the concentration of chloride ions were investigated. The experimental results showed that the cementation rate of Sn(II) ions increased with increase of the addition amount of aluminium powders, temperature, pH and the concentration of chloride ions in hydrochloric acid solution. From the results, the optinum conditions for recovery of metallic tin by cementation with aluminium metal powders were proposed.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.24 no.12
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• pp.2972-2979
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• 2000

Dynamic characteristics of powder metal is very important to mechanical structures requiring high strength or endurance for impact loading. But owing to distinctive property of powder metal, that is relative, it has been investigated restrictively compared to static characteristics. The objectives of this study is to investigate dynamic characteristics of powder metal and compare it to a fully density material. To find the characteristics, an explicit finite element method is used for simulation of Split Hopkinson Pressure Bar experiment based on the stress wave propagation theory. We obtained a dynamic stress-strain relationship and dynamic behavior of powder metal, as well as the variation of material properties during dynamic deformation.

• Korean Journal of Crystallography
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• v.9 no.1
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• pp.44-47
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• 1998

A reduction/oxidation reaction between A1 metal powder and SiO2 powder was performed by Self-propagating High-temperature Synthesis (SHS) reaction induced by microwave energy to produce a composite of Al2O3 and Si powders by using a 2.45 GHz kitchen model microwave oven. A Microwave Hybrid Heating(MHH) method was applied by using SiC powders as a suscepting material to raise the temperature of the disk samples and the heat increase rate of over 100℃/min were obtained before the reaction. The reaction started around 850℃ and the heat increase rate jumped to over 200℃/min after the reaction took place.

• Journal of the KSME
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• v.32 no.1
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• pp.46-56
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• 1992

이 글에서는 현재까지 개발된 금속복합재료의 제조공법 중에서 비교적 보편화되어 있는 분말야 금법, 가압용침법, 복합주조법 등에 대하여 소개하였고, 제조된 재료가 가지는 일반적인 기계적 성질에 대하여 설명하였다. 그리고 금속복합재료의 대표적인 응용분야와 현재 국내에서도 큰 관심을 끌고 있는 자동차엔진의 부품소재로서 금속복합재료의 응용기술에 대해 소개하였다. 국 내에서 금속복합재료의 관련 연구는 주로 학교와 연구소를 중심으로 발전되어 왔으나 근년에 자동차 산업의 비약적인 발전과 항공산업 분야에서 잠재적인 수요가 예측되면서 일부 기업체에서 응용 연구를 시작하였다. 그러나 금속복합재료의 기초 소재가 되는 경합금과 보강재의 제도기 술은 선진국에 비해 크게 뒤져 있다. 현재까지 국내에서의 연구동향은 주로 금속복합재료의 제조공정개발과 물성 평가에 치중하여 왔다. 기계공업이 발전하면서 점점 더 고기능성 소재가 요구되어지는 현황을 감안할 때 금속복합재료의 실질적 응용분야의 개척과 함께 기초 소재의 개발 연구는 시급한 과제이다.

• Korean Journal of Materials Research
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• v.5 no.2
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• pp.223-231
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• 1995

Mechanical alloying behavior of the PbTe intermetallic compound, which is used for thermoelectric generation, has been investigated with milling time and ball-to-powder weight ratio. Formation of PbTe alloy was completed by mechanical alloying of the as-mixed Pb and Te powders for 2 minutes at ball-to-powder weight ratio of 2 : 1. In situ measurement of the abrupt temperature rise during the ball milling process indicated that the PbTe intermetallic compound was formed by a self-sustained reaction rather than diffusional reactions. Lattice constant of PbTe alloy fabricated by mechanical alloying, 0. 6462nm, was not varied with milling time and ball-to-powder weight ratio. This value of the lattice parameter is in excellent agreement with 0.6459nm, which was reported for PbTe powders processed by melting and grinding.

• Applied Chemistry for Engineering
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• v.34 no.4
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• pp.450-454
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• 2023

Chloride ions in the alloy powder used as flux in Flux Cored Arc Welding (FCAW) can cause pores on the bead surface of the welding metal to cause defects, or chloride remaining in the alloy powder can cause corrosion of the metal. Combustion-ion chromatography is mainly used to quantify the chloride ions in alloy powder, but there is a limitation in that the equipment is expensive and requires a high degree of expertise. Therefore, this study aims to find an easy and accurate quantification method in the field by comparing combustion-ion chromatography (C-IC), which is mainly used for chloride ion quantification of alloy powder, X-ray fluorescence analysis (XRF), and potentiometric titration. In this article, magnesium-aluminum alloy powder is applied to the quantification of chloride ions because it is most commonly used as flux. This study confirmed that potentiometric titration can be applied to the quantification of chloride ions in the alloy powder in the industry field.

• Journal of Powder Materials
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• v.20 no.1
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• pp.60-67
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• 2013

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2005.04a
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• pp.68-69
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• 2005

• Proceedings of the Korean Magnestics Society Conference
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• 2002.12a
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• pp.116-117
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• 2002

High energy mi]ling은 mechanical alloying을 일컫는 분말 제조 공정으로서 금속 뿐 아니라 세라믹스 분말 합성에도 많이 응용되고 있으며, 입자크기의 나노화와 일반적인 세라믹 분말의 특성을 개질할 수 있다는 특징을 갖고 있어서 다양한 연구 결과가 보고되고 있다[1-2]. Ba 및 Sr 페라이트와 같은 육방정 페라이트는 보자력(high coercivity)이 높은 특성을 가지므로 영구자석용, 기록재료용 등으로 광범위하게 사용되어온 재료이다. 이와 같은 높은 보자력을 유지하기 위해서는 입자크기가 단자구 입경(<1 $\mu\textrm{m}$) 보다 작아야 하기 때문에, 초미립자 합성에 관한 많은 연구가 진행되어 왔다[3-4]. (중략)