• Clean Technology
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• v.28 no.2
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• pp.103-109
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• 2022

Nd-Fe-B waste permanent magnet contains about 20~30% rare earth elements and about 60~70% iron elements, and the rare earth and iron components were recovered through sulfuric acid leaching and fractional crystallization. Oxidation roasting was not performed for separation and recover of the rare earth and iron elements. The leaching characteristics were confirmed by using as variables the sulfuric acid concentration and the mineral solution concentration ratio. Sulfuric acid leaching was carried out for 3 hours for each sulfuric acid concentration. The leached solid phase was characterized for its crystalline phase, composition, and quantitative components by XRD and XRF analysis, and the filtrate was analyzed for components by ICP analysis. With sulfuric acid leaching at 3M sulfuric acid concentration, neodymium compounds were formed, the iron content was the least, and the recovery rate was high. After the filtrate remaining after sulfuric acid leaching was subjected to fractional crystallization through evaporation and concentration, the neodymium component was found to be concentrated 7.0 times and the iron component 2.8 times. In this study, the recovery rate of waste permanent magnets through sulfuric acid leaching and a fractional crystallization method without an oxidation and roasting process was confirmed to be about 99.4%.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.9 no.1
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• pp.119-125
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• 1999

This research has been studied in terms of investigating the reaction behavior of pyrite with a cyclone reactor. The Mathematical model has developed pyrite oxidation and lime sulfation in this reactor. The model assumes a chemical control shrinking core behavior for the pyrite and a fluid film control shrinking core behavior for the lime. The model was solved and characterized numerically. Experiments have been performed to study the influence of reaction parameters such as reactor temperatures, pyrite particle sizes, air flow rates, feeding rates, and mixing ratio of pyrite and lime. The oxidation and sulfation products were characterized chemically and physically.

• Korean Journal of Materials Research
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• v.15 no.5
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• pp.313-317
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• 2005

The relation between bulk microdefect (BMD) and mechanical strength of $P/P^-$ epitaxial silicon wafers (Epitaxial wafer) as a function of nitrogen concentrations was studied. After 2 step anneal$(800^{\circ}C/4hrs+1000^{\circ}C/16hrs)$, BMD was not observed in nitrogen undoped epitaxial silicon wafer while BMD existed and increased up to $3.83\times10^5\;ea/cm^2$ by addition of $1.04\times10^{14}\;atoms/cm^3$ nitrogen doping. The slip occurred for nitrogen undoped and low level nitrogen doped epitaxial wafers. However, there was no slip occurrence above $7.37\times10^{13}\;atoms/cm^3$ nitrogen doped epitaxial wafer. Mechanical strength was improved from 40 to 57 MPa as nitrogen concentrations were increased. Therefore, the nitrogen doping in silicon wafer plays an important role to improve BMD density, slip occurrence and mechanical strength of the epitaxial silicon wafers.

• Textile Coloration and Finishing
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• v.6 no.2
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• pp.47-54
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• 1994

Cotton fiber, NaOH-mercerized cotton fiber, cotton fabric, and NaOH-mercerized cotton fabric have been treated by liquid ammonia at -33.4$^{\circ}C$. The fine structures, bending properties, tensile strengthes, shrinkages for laundering, and wrinkle recoveries were studied. The treatment of cottons with liquid ammonia brought about the transition of crystal lattice ; transforming cellulose I crystal of original cotton to cellulose I and III crystal, and cellulose II crystal of mercerized cotton to cellulose II and III crystals. The degree of crystallinities were decreased in the order of liquid ammonia>NaOH/liquid ammonia>NaOH-treated cotton. However moisture regain and water absorbency for liquid ammonia-treated cotton were lower than that of NaOH-treated cotton because of a difference in swelling actions of the agents. It seems caused by intermicrofibrillar pores produced in swelling processes. The bending rigidity and bending hysteresis were decreased remarkly by liquid ammonia treatment. Therefore softness and dimensional stability were improved. The liquid amminia and NaOH/liquid ammonia-treated cottons moreover show excellent properties in tensile strength, anti-shrinkage for laundering, and wrinkle recovery.

• 한국어정보학회:학술대회논문집
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• 2016.10a
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• pp.226-230
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• 2016

본 연구는 초등 저학년 읽기부진아동을 위한 한글 파닉스 교육의 기반을 확립하고자 1-2학년 교과서 고빈도 어절 531개를 기반으로 자소 및 음운규칙을 분석하였다. 연구결과, 자소-음소 일치 어절을 기반으로 하였을 때 초성에서 50번 이상 나타난 자소는 /ㄱ/, /ㄹ/, /ㄴ/, /ㅅ/, /ㅎ/, /ㅈ/이다. 중성에서 50번 이상 나타난 자소는 /ㅏ/, /ㅣ/, /ㅗ/, /ㅡ/, /ㅜ/이다. 종성에서 50번 이상 나타난 자소는 /ㄹ/, /ㄴ/, /ㅇ/이다. 자소와 음소가 불일치 된 어절을 기반으로 하였을 때 가장 많이 출현하는 음운규칙은 연음화 규칙이었다. 본 연구결과를 바탕으로 교과서를 기반으로 한 한글 파닉스 교육에 유용하게 사용될 수 있을 것이다.

• Textile Coloration and Finishing
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• v.4 no.2
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• pp.76-83
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• 1992

Wool tropical and nylon taffeta were treated with low temperature plasma of $O_2$, $N_2$, NH$_3$, CF$_4$ and CH$_4$ for the intervals of 10 to 300 sec, and then dyed with leveling and milling type acid dyes in presence or absence of buffer solution. From the color depth of dyed fabrics, effect of plasma gases, treated time, dyeing time and temperature on dyeing property was studied. The results of the experiment can be summarized as follows: 1) The plasma treatments except methane gas increased the color depth of dyed wool fabrics, but not that of dyed nylon fabrics regardless of the plasma gases used. 2) The color depth of wool fabrics dyed in the dye bath without buffer solution was increased by the low temperature plasma, especially increased much more by CF$_4$ plasma treatment. It is found that with the identification of F- ion in the residual dye bath the hydrogen fluoride gas was adsorbed on wool fabrics in the plasma treatment. 3) The color depth of wool fabrics was increased with the time of $O_2$ and CF$_4$ plasma treatments. 4) In both cases of the leveling and milling type acid dyes, the rate of dyeing was increased in the low temperature plasma treatments, and it is found that the leveling type acid dye increased the color depth at relatively low temperature below 4$0^{\circ}C$, compared with the milling type acid dye.

• Korean Journal of Optics and Photonics
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• v.9 no.3
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• pp.175-180
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• 1998

Nd:YAG single crystal widely used as solid state laser was grown by Czochralski method. <111> single crystal with 0.9at% of $Nd^{3+}$ was grown from the Czochralski furnace with a automatic diameter control system. The vertical temperature gradient in the liquid was the major factor that influence the crystal quality, and the crystal diameter was controlled by the home made computer program. The crystal boule with $\phi$50mm$\times$ι100mm effective size was cut, polished, and antireflection coated. The optical evaluation such as absorption spectrum, fluorescence spectrum coincide with typical features of Nd:YAG single crystal. The laser rod was assembled into the CW laser generator with a Kr lamp. The maximum CW laser output was 70 W and the threshold power and efficiency was 1.3kW and 1.64% respectively.

• KIEAE Journal
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• v.8 no.2
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• pp.65-70
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• 2008

Recently, there has been growing interest in barrier-free design which makes safe and convenient space for every pedestrian, not only the non-disabled but also the disabled. The purpose of this study is to suggest the data on the pavement materials of barrier-free pedestrian environment in view of universal design. In order to this, the research is focused on evaluating the visual preference and preference factors for pavement scenery, which can be changed by pavement materials. And this research is also comparing the visual preference and preference factors of the disabled with that of the non-disabled. A multi-regression analysis method is adopted to analyse the correlation between the visual preference for pavement scenery and preference factors in this study. The result of this analysis is as follows. Firstly, there are some differences of visual preference for the pavement material between the disabled and the non-disabled. Secondly, independent variables influencing on preference are similar between two groups. Thirdly, there are some differences in the priority of preference between the disabled and the non-disabled. This study will contribute to the field of barrier-free design and sustainable development projects in order to maximize the human being's satisfaction.

• Speech Sciences
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• v.12 no.2
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• pp.139-149
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• 2005

The purpose of this study was to propose a preliminary norm for 'Korean-Test of Articulation for Children(K-TAC)'. The K-TAC was designed to test 19 Korean consonants in various phonetic contexts through 37 words. We collected the data of 220 normally developing children aged 2;6(years;months) to 6;5. We analyzed the mean percentage of consonants correct and the age of acquisition for K-TAC. The results were as follows: first, The mean percentage was over 60% at late 2 years of age, over 80% at th age of 3, and over 90% after the age of 4. There were significant differences among age groups. Second, based on the criterion of correct production by 75% of children, Korean children acquired stops and nasals except for SF velars, glottal fricative, SF liquid and affricates by late 2 or 3 years of age. After that they acquired SF velars at the age of 4 and SI liquid at the age of 5. However, they could not acquire alveolar fricatives by the age of late 6. Third, if the distorted sounds were scored as correct, they acquired SI liquid at 4 years of age and alveolar fricatives at 5 years of age.

• Speech Sciences
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• v.7 no.2
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• pp.37-50
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• 2000

This paper describes a test of everyday speech understanding ability, in which a listener's utilization of the context-situational information of speech is assessed, and is compared with the utilization of acoustic-phonetic information. The test items are sentences which are presented in a babble type of noise, and the listener response is the key word in the sentence. The key words are always two-syllabic nouns and the questioning sentences are added to obtain the responding key words. Two types of sentences are used. One is the high-predictable sentences for which the key word is somewhat predictable from the context. The other is the low-predictable sentences for which the key-word cannot be predicted from the context. Both types are included in six 40-item forms of the test, which are balanced for intelligibility, key-word familiarity and predictability, phonetic content, and length. Performance of normally hearing listeners shows significantly different functions for various signal-to-noise ratios. The potential applications of this test, particularly in the assessment of speech understanding ability in the hearing impaired, are discussed.