• Proceedings of the Korean Magnestics Society Conference
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• 2003.06a
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• pp.192-193
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• 2003

YIG 에피택시박막은 다른 강자성, 페리자성재료에 비해 수 GHz의 영역에서 매우 우수한 특성을 나타내고 있다. YIG 에피택시 박막은 고상에피택시 방법으로 제조할 경우 매우 편리하게 제조할 수 있는 것으로 알려져 있는데, 이 방법은 상온에서 Y-Fe-O 박막을 GGG(111)기판에 스파터한 뒤 공기 중에서 열처리하면 간편하게 얻을 수 있다. 이 방법은 통상과 같이 고온에서 아주 느린 속도로 에피택시박막을 성장시키는 스파터방법에 비해 매우 간편하고 경제적인 것으로, 본 연구에서는 보통의 분말소결공정으로 제작된 2.5인치 YIG 타겟을 사용하여 두께 2.5 $\mu\textrm{m}$ 비정질 Fe-Y-O 박막을 만든 뒤 550 - 1050 $^{\circ}C$의 공기 중에서 열처리하였다. 비정질 박막을 $600^{\circ}C$이하에서 10 시간동안 열처리하였을 경우 매우 약한 YIG상의 회절선만 관찰할 수 있었다. 반면에 온도를 $650^{\circ}C$로 올리면 매우 강한 (444) 또는 (888)회절선과 매우 약한 다른 회절선을 관찰 할 수 있었다. 이 시편의 경우 (888)회절선의 강도는 GGG기판의 (888)회절선의 강도와 비교할 정도로 매우 강하여 에피택시성장이 매우 잘 이루어질 수 있다는 가능성을 확인할 수 있었다. 그리고 YIG(888) 회절선의 록킹곡선의 반가폭이 0.14$^{\circ}$ 이었고, 이것은 에피택시성장이 매우 잘 이루어지고 있음을 의미하는 것이다. 열처리 온도가 감소함에 따라 YIG박막의 격자상수는 감소하였으며 YIG(888)회절선의 강도는 그림 1과 같이 넓어지고 그 강도는 약해진다.

• Journal of the Microelectronics and Packaging Society
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• v.12 no.2 s.35
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• pp.141-147
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• 2005

Nanomaterial $TiO_2-SiO_2$ was synthesized by hydrolysis and condensation process using 2-propanol(2-PrOH) and was characterized by FT-IR, DSC, XRD and FE-SEM. FT-IR spectra were measured to investigate Ti-0-Si absorption peak. DSC thermal analysis results appllied to Ozawa equation were used to calculate to activation energy of crystallization. It was found that the changes of X-ray diffraction patterns and FWHM obtained XRD measurement depended on calcination temperature. In FE-SEM analysis, particle size changed by quantity changes of Ti-alkokide.

• Journal of the Korean Society for Precision Engineering
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• v.17 no.1
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• pp.145-152
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• 2000

X-ray diffraction method detects change of crystal lattice distance under material surface using diffraction angle 2$\theta$. This technique can be applied to the behavior on slip band and micro crack due to material degradation. The relation between half-value breadth and number of cycle has three stages which constitute rapid decrease in initial number of cycles, slight decrease in middle number of cycles and rapid decrease in final number of cycles. The ratio of half-value breadth takes a constant value on B/B$_{0}$-N diagram with loading condition except early part of fatigue life. The ratio of half-value breadth B/B$_{0}$ with respect to number of cycle to failure N$_{f}$ has linear behavior on B/B$_{0}$-log N$_{f}$ diagram. Therefore, in this paper the estimation of fatigue life by average gradient method has much less estimated mean error than the estimation of fatigue life by log B/B$_{0}$-log N/N$_{f}$ relation.elation.ation.

• Journal of architectural history
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• v.3 no.2 s.6
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• pp.47-66
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• 1994

Chosun dynasty had accepted the Confucianism as a means of governing whole society and in its practical aspect ${\ulcorner}$Garye${\lrcorner}$ and the ceremonies of family ritual regarded as important. As a result, after mid-Chosun dynasty family ritual was begun to popularized on a national scale, and the socio-culture system which was interrelated with it changed into confucian ones. These fill-scaled change, on the other hand, resulted into the change of spatial use and plan type of yangban houses. In this aspect, this study intends to clarify the influence of family ritual on spatial use of yangban houses through the comparison between ideal pattern and behavioral one of family ritual. And this study made Gwanhonrye except Sangjerye an object because these two ceremonies were peformed in sucession in those day's behavior. The research setting is the Korean traditional society prior to modernization. The collected materials are based on ethnographic information as well as personal documents, public records, field works and the books on family ritual. The methodology for the present study is primarily based on the comparison study between available documents and field work. Especially, as the books on family ritual include some explanatory diagrams of the ideal pattern, these diagrams are compared with another ones made by the author of the behavioral pattern. The major findings are as follows. Firstly, in the aspect of Gwanhonrye's process, the ideal pattern is similar to the behavioral one. But even the essential course of the ideal pattern of Honrye is 'chinyoung', it has never been accepcted in Chosun dynasty on account of 'seoryubuga'. Secondly, even though the names of the performing space of family ritual are different each pattern, the methods of spatial use in processing these two ceremonies are similar. In other words, according to the books on family ritual the major performing spaces of Gwanhonrye are 'chungsa' and 'jungchim', but in practical process of both ceremonies 'sarangchae' and 'anche' are used. Lastly, as family ritual like Gwanrye and Honrye had been practiced at yangban houses after mid-Chosun dynasty as mentioned above, the spatial arrangement had to be changed to a certain extent.

• Journal of architectural history
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• v.17 no.1
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• pp.85-102
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• 2008

As a result of analyzing the floor plan shown in the three drafts, there were a great deal of differences in composing the space of the inner main hall. The inner room facing to the east with the arrangement crossing the inner floor at right angles in the 'Baekdangguje Draft' faces to the south in the east or west in front of the main house thereafter. This represents that it reflects the intent of the owner of the architecture emphasizing the size increase and ceremonies of the main house in the 'ㅁ shape', which has changed to the directions of easily accommodating the Confucian ceremonial activities in the floor plan of the inner house as the size of the main house was gradually increasing from 24 sections to 30 or 38 sections. The expansion in the size of main house further divided the functions of floor into one for daily life and the other for ceremonies as well. In other words, the 30 Sections in Yijeong Draft as being the first planned draft for reconstruction had a hall for memorial services in the main hall of the inner house, whereas the 'Draft with 38 Sections' as being the second planned draft for reconstruction was planning a room with a floor (two sections of Bangdang) for memorial purpose in the back of the inner main hall. The variations in the guest house (or space for men) shown in the drafts confirms the establishment of space for men as the size of the main house increases. We can see the change that a large guest house is placed over the south and in the south and east of the main house as the number of main house increases by 30 sections or 38 sections. Especially, a guest house with a wide space in a 'ㄴ shape' is arranged from the south of main house to the east wing in the Draft with 38 Sections. In addition, the backward sections are advanced in the front and back of guest house in the drafts with 30 and 38 sections, while a back floor or a back floor connecting to the back room or sleeping room or inner house is installed in the backward sections.

• Journal of the Korean Ceramic Society
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• v.39 no.1
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• pp.33-37
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• 2002

The phosphorescence powder, $SrA1_2O_4:Eu^{2+}$, synthesized by a Polymerized Complex Method(PCM), has been compared with that by a Solid-State Reaction(SSR), and their luminescence characteristics have been studied. The PCM powders were synthesized at $900^{\circ}C$ and the SSR powders at $1200^{\circ}C$. The size of PCM powders was about $0.1{\mu}m$ and one tenth of that of the SSR powders, which was due to the lower synthesized temperature. On the other hand, residual carbon in the PCM powders decreased with an increase in the crystallinity of host lattice, which was responsible for the non-white color of the powders. Both powders showed the maximum luminescence peaks around 520nm in the wave length at room temperature. However, the peak position for the PCM powders was shifted to a slightly lower wavelength and the value of half-width of the peak was broad comparing to that of the SSR powders, and the peak intensity decreased significantly. Such a change in the luminescence characteristics was due to the large difference in size for two types of powders and partly the residual carbon in the PCM powders.

• Journal of the Korean Ceramic Society
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• v.40 no.5
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• pp.481-487
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• 2003

A technique for determination of proportions of char, coal ana coke is needed in order to monitor pulverized coal injection performance in operating blast furnace. Quantitative X-ray powder diffraction analysis can be applied to the problem providing that structural information on carbonaceous materials, coal, char, coke and their mixture are known. Chars were prepared from a coal at different temperatures (1000∼1400$^{\circ}C$) and were characterised by X-Ray powder Diffraction (XRD). The XRD result gave crystallite size (height Lc and diameter, La), aromaticity, number of (002) plane in carbon, and d-spacing. As a result, with increasing heat treat temperature of char, Lc$_{(002)}$, La$_{(10)}$ and number of (002) plane in carbon were increased, and d-spacing and FWHM(Full With Half Maximum) were decreased. Result of prediction of amount of char from the mixtures (char, coke and ore) based on the Lc$_{(002)}$ information of two mixtures (coke and char) showed very close values expected.

• Journal of the Korean Ceramic Society
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• v.40 no.5
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• pp.423-427
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• 2003

Effect of the thermal poling on the 1.55 fm emission spectra in various Er$^{3+}$ -doped glasses was investigated with a special attention on the changes in the values of FWHM(Full Width at Half Maximum) intensity. Tellurite glasses poled at 28$0^{\circ}C$ with an electric voltage of 4 kV resulted in an approximately 6% increase in FWHM values compared with their unpoled counterparts. On the other hand, values for glasses, such as aluminosilicate, sulfide and chalcohalide, either decreased or remained unchanged. The characteristic results from tellurite glasses are most probably due to the presence of lone-pair electrons in the TeO$_4$ hi-pyramidal units that form the main network structure of tellurite glasses.

• Journal of the Korea Institute of Information and Communication Engineering
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• v.10 no.12
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• pp.2251-2257
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• 2006

We fabricated ZnO thin film successfully by using RF magnetron sputtering and investigated its potential for being utilized as the key material of piezoelectric device with the characterization of ZnO thin film such as such as crystallinity, surface morphology, c-axis orientation, film density. In thin study, $Ar/O_2$ gas ratio is fixed 70/30, RF power 125W, working pressure 8mTorr, distance between substrate and target 70mm, but the substrate temperature is varied from room temperature to $400^{\circ}C$. The relative intensity ($I_{(002)}/I_{(100)}$) or (002) peak in ZnO thin film deposited at $300^{\circ}$ was exhibited as 94%, then its FWHM was $0.571^{\circ}C$. Also, from the surface morphology evaluated by SEM and AFM, the film deposited at $300^{\circ}C$ showed uniform particle shape and excellent surface roughness of 4.08 m. The tendency of ZnO thin film density was exhibited to be denser with increasing substrate temperature but slightly decreased at near $400^{\circ}C$.

• Journal of the Korean Society for Nondestructive Testing
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• v.16 no.1
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• pp.10-18
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• 1996

This study verified the relationship between fracture mechanics parameters and X-ray parameters for normalized SS41 steel with homogeneous crystal structure and M.E.F. dual phase steel(martensite encapsulated islands of ferrite). The fatigue crack propagation test were carried out and X-ray diffraction technique was applied to fatigue fractured surface. The change in X-ray parameters(residual stress, half-value breadth) according to the depth of fatigue fractured surface were investigated. The depth of maximum plastic zone, $w_y$, were determined on the basis of the distribution of the half-value breadth for normalized SS41 steel and that of the residual stress for M.E.F. dual phase steel. $K_{max}$ could be estimated by the measurement of $w_y$.