• Transactions of the Korean Society of Mechanical Engineers
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• v.10 no.4
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• pp.477-486
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• 1986

본 연구에서는 SM20C를 모재로 하여 입경의 크기가 다른 3종의 복합조직강을 제작 동일한 분위기에서 저 및 고사이클 전영역에 걸쳐 피로특성을 검토하고져 한다. 제일보는 그 중 저사이클특성에 대한 보고이다. 일반적으로 저사이클 피로현상은 재 료가 탄소성 상태하에서 전위, 미소크랙, 보이드(void) 등의 인자가 복합적으로 작용 하여 발생함으로 변형률속도, 제어파형, 온도, 시험방법 및 분위기에 따라 많은 영향 을 받는다. 따라서 본 연구에서는 두가지 실험방법을 사용, 응력-변형율거동을 검토 복합조직강의 피로특성과 입경크기가 피로거동 및 강도에 미치는 영향을 비교 고찰하 였다.

• Journal of the Korean Society for Nondestructive Testing
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• v.13 no.2
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• pp.40-47
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• 1993

Composites composed of a precipitation harden 2124 alloy matrix reinforced by SiC whiskers, which are fabricated by powder metallugy, are suscepttible to fatigue damage due to the pile-up of moving dislocation and the microcrack initiation along SiC-Al interfaces, especially at the external surfaces of a body. The initial process, such as pile-up of dislocation or microcrack, that corresponds to the stage I during fatigue failure process are too small to be detected and characterized by conventional ultrasonic technique. This paper describes the applicability of an acoustic microscope with Line-Focus-Beam(LFB) lens of 225MHz to evaluate fatigue damage of SiC whiskers reinforced Al alloy. The specimens which were 6.6mm thick, 13mm wide, and 105mm long in the gage section were fatigued in tension-tension under load control. The velocity of leaky surface and leaky pseudosurface acoustic waves are obtained by FFT analysis technique from V(z) curve which is a record of output of piezoelectric transducer. These results are discussed with the change of number of fatigue cycles. The result obtained by acoustic microscope is compared with that by ultrasonic technique generated at 5MHz with conventional surface wave transducers.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2011.05a
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• pp.80-80
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• 2011

세계 기후 변화와 불안정한 유가 변화에 대응하고 국내산업의 저탄소 녹색성장을 위해 신재생에너지 개발이 활발하게 이루어지고 있다. 해양에너지 중에서 조류발전은 대규모 댐을 건설할 필요가 없어 비용이 적게 소요되고 특히 날씨 변화나 계절에 관계가 없고, 발전량이 예측 가능하므로 신뢰성 있는 에너지원으로 적용이 가능하다. 조류발전기 블레이드에 폴리머계 복합재료와 스테인리스강이 대부분인데, 이 재료는 특정 회사에서만 제작 가능하며, 충격에 약하고, 균열전파 속도가 빠르며, 대단히 고가이며, 수입에 의존하고 있는 실정이다. 이러한 조류발전에 사용되는 블레이드는 가혹한 부식, 캐비테이션 그리고 침식환경에 노출되어 있어 내구성이 우수한 제품개발이 대단히 중요하며, 조류발전 블레이드를 동합금으로 제작시, 내식성이 뛰어나며 구리의 특성상 해양생물 서식을 방지할 수 있고, 내캐비테이션 특성, 내구성, 가공성 및 유지보수가 용이한 장점이 있다. 이러한 동합금에 WC-27NiCr와 WC-10Co4Cr를 초고속 화염용사(HVOF)를 이용하여 코팅층의 캐비테이션 특성 및 전기화학적 거동을 연구하였다. 본 연구에서는 조류발전용 블레이드의 재료로 사용하려는 동합금에 WC-27NiCr와 WC-10Co4Cr이 용사코팅된 시험편을 사용하였다. 다채널 부식시험기인 WonA-tech WMPG-1000을 이용하여, 자연전위를 측정하였으며, 분극실험은 자체 제작한 홀더를 사용하여 $0.3318cm^2$를 노출 시켜 실험하였다. 기준전극은 은/염화은 전극을, 대극은 백금 전극을 사용하였다. 양분극과 음분극 실험을 통해 개로전위에서의 부식거동을 확인하였고, 정전위 실험도 실시하였다. 실험 종료 후 3D현미경 및 전자주사현미경(SEM)을 사용하여 코팅층 표면의 손상거동을 관찰하였다. 캐비테이션 실험은 ASTM-G32 규정에 의거하여 압전효과를 용한 진동발생 장치(RB 111-CE)를 사용하였다. 수조는 전기화학적 부식의 영향을 고려하여 아크릴로 제작하였고, 시험편은 실험장비에 맞게 파인커팅머신을 이용하여 $20mm{\times}20mm$로 절단하여 사용하였으며 혼과 대향하도록 하여 1mm 간격을 두어 실험하였다. 실험 실시 전, 미소전자저울을 사용하여 무게감소량을 측정하였으며 표면관찰을 통하여 캐비테이션 거동을 관찰하였다.

• Journal of the Korean Institute of Gas
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• v.7 no.2 s.19
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• pp.48-53
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• 2003

This study is to look at the effect for deformation of carbon steel for high-presure pipe, on the AE signals produced by tensile test. Acoustic emission(AE) has been widely used in various fields because of its extreme sensitivity, dynamic detection ability and location of growing defects. We investigated a relationship failure mode and AE signals by tensile test, From the tensile test, we could divide into four ranges of the failure modes of elastic range, yield range, plastic range before $\sigma$u, plastic range after $\sigma$u. And failure behaviors of elastic range, yield range, plastic range before $\sigma$u, plastic range after $\sigma$u could be evaluated in tensile test by AE counts, accumulation counts and time frequency analysis. It is expected to be basic data that can protect a risk according to tensile test and bending of pipe material for pressure vessel, as a real time test of AE.

• Nuclear Engineering and Technology
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• v.24 no.2
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• pp.141-153
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• 1992

Excess tritium analysis was peformed to verify whether or not cold fusion occurs during electrolysis of heavy water in the current density range of 83~600 mA/$\textrm{cm}^2$ for a period of 24 ~ 48 hours with use of palladium electrodes of seven different processing treatments and geometries. The extent of recombination of D$_2$ and $O_2$gases in the electrolytic cell was measured for the calculation of accurate enthaplpy values. The behavior and interaction of hydrogen atoms with defects in Pd electrodes were examined using the Sieverts gas charging and the positron annihilation(PA) method. Slight enrichment of tritium observed was attributed to electrolytic enrichment but not to the formation of a by-product of cold fusion. The extent of recombination of D$_2$and $O_2$gases was 32%. Hence the excess heat measured during the electrolysis was considered to be due to the exothermic reaction of recombination but not to nuclear fusion. Lifetime results from the PA measurements on the Pd electrodes indicated that hydrogen atoms could be trapped at dislocations and vacancies in the electrodes and that dislocations were slightly more preferred sites than vacancies. It was also inferred from R parameters that the formation of hydrides was accompanied by generation of mostly dislocations. Doppler broadening results of the Pd electrodes indicated that lattiec defect sites where positrons were trapped first increased and then decreased, and this cycle was repeated as electrolysis continued. It can be inferred from PA measurements on the cold-rolled Pd and the isochronally annealed Pd hydride specimens that microvoid-type defects existed in the hydrogen-charged electrode specimen.

• Korean Journal of Materials Research
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• v.8 no.1
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• pp.27-32
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• 1998

In-Sit반응소결에의해 Si과 AI금속분말을 이용하여 Si$_{3}$N$_{4}$-AIN 복합세라믹스를 합성하였다. 합성된 Si$_{3}$N$_{4}$-AIN복합세라믹스의 미세조직과 결정구조를 해석하기 위해, OM, TEM, XRD및 EDX를 이용하였으며, Si$_{3}$N$_{4}$-AIN -20wt.%AIN복합세라믹스에서 Si의 질화율은 97%로 가장 높았다. Si$_{3}$N$_{4}$-AIN 복합세라믹스에서 Si의 질화율은 AI첨가량 증가에 따라 감소하였다. 대부분의 AI입자들은 다결정 AI입자들은 다결정 AIN(4-H구조)로 완전질화되었으며, 따라서 잔류 AI상은 반응소결체내에서 관찰되지 않았다. Si$_{3}$N$_{4}$의 결정구조는 $\alpha$와 $\beta$구조가 혼재된 상태이며, 잔류 Si입자내에서는 미소균열 및 전위가 관찰되었다. AI/Si$_{3}$N$_{4}$와 Si$_{3}$N$_{4}$ 두계면에서 이들은 거친 형상을 보이지만, 계면반응상은 관찰되지 않았다.

• Korean Journal of Materials Research
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• v.9 no.10
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• pp.1000-1005
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• 1999

To investigate the effects of V and Sb on the recrystallization of Zr-0.8Sn alloy, the microstructure of heat-treated specimens was observed by optical microscope, SEM, and TEM. Microhardness tests were also carried out for the annealed specimens. From microstructural studies, the V or Sb additions were found to delay recrystallization process as well as grain growth. Especially, Sb was more effective in delaying the recrystallization. This delay of recrystallization and grain growth by V or Sb additions may be due to the interference in the movement of dislocation and crystal interface by V or Sb precipitates.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.2 no.2
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• pp.77-82
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• 1992

When a crystal is grown by FZ process, the melt zone is located at between the solid of upper and lower side and is kept by the solid-liquid interface tension. On the surface of the melt zone, a surface tension gradient is occured by the difference of temperature and solute concentration, it is the driving force of marangoni flow. The crystal even in the steady state growth can become imperfect for the dislocation distribution and the solute concentration in the peripheral region of the crystal are higher than those in the inner part and the probability of the formation of the defects such as voids, bubble penetration, secondary phase creation and crack is high near the solid-liquid interface. This is because the solid -liquid interface becomes irregular because of the local variation of temperature in that region due to marangoni convection.

• Korean Journal of Materials Research
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• v.11 no.2
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• pp.104-114
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• 2001

To investigate the effects of the addition of Nb and Sn on the recrystallization of Zr- Sn-Nb alloys, both Vickers micro-hardness test and TEP measurement were carried out on cold-worked specimens annealed at various temperatures from $300^{\circ}C$ to 75$0^{\circ}C$. The microstructures of heat treated specimens were analyzed by optical microscope, SEM, and TEM. The study of microhardness and microstructures showed that both recrystallization process and grain growth were retarded as the activation energy was increased by the addition of Nb and Sn. Especially, the addition of Sn was more effective on retarding recrystallization. Precipitates were formed more easily when Nb was added because the solubility of Nb into Zr is lower than that of Sn. However, the recrystallization process was affected more by Sn than Nb because the strain field formed by substitutional Sn repressed the dislocation movement. TEP was increased due to the decrease of electron scattering as recovery and recrystallization were proceeded and saturated when the recrystallization completed. However, when precipitates formed, TEP was increased because the decrease of solute concentration near the precipitates caused the decrease of electron scattering.

• Journal of the Korea Concrete Institute
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• v.19 no.6
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• pp.785-793
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• 2007

An electrochemical transient response technique was used to study the corrosion of reinforcing steel bar in the concrete. Analysis of the transient electrochemical potential response in a corrosion interface to an applied current has enabled the separate components that make up the measured transient response to be isolated. These components display a range of resistances and capacitances, dependent on the corrosion conditions of the reinforcing steel, which may be attributed to the corrosion process, to effects within the concrete cover or to film effects on the surface of the concrete. In this technique, the corrosion rate was evaluated by summing all of the resistances in the separate components to obtain an aggregated corrosion resistance. However, it is possible that not all resistances identified are associated with the corrosion process. The results obtained show that the corrosion rates are significant dependent on the assignment of the separate components to either corrosion or to other processes. The assignment of resistive components associated with the corrosion rate can be clearly identified by taking a series of the transient measurement at different lateral distances from the corroding reinforcing steel. An inappropriate selection of measurement time however may result in an additional resistance, which is not associated with corrosion, being included or part of the resistance associated with corrosion being left out.