• Journal of the Korean Society for Nondestructive Testing
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• v.25 no.4
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• pp.239-246
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• 2005

In this study, a finite element analysis and a vibration test were performed to estimate the natural frequencies of mouse femurs with osteoporosis. Three groups of the femurs include the osteoporotic group, the treated group and the normal group. For the finite element analysis, the micro finite element model of the femur was reconstructed using the Micro-CT images and the Voxel mesh generation algorithm. In the vibration test, the natural frequencies were measured by the mobility test. from the results, the averaged natural frequencies in the osteoporotic group were the highest, followed by those in the treated group. The finite element models were validated within 15% errors by comparing the natural frequencies in the finite element analysis with those in the vibration test. The developed Micro-CT system, the Yokel mesh generation algorithm, the presented finite element analysis, and vibration test could be useful for the investigation of the structural change of the bone tissue, and the diagnosis and the treatment in the osteoporosis.

• Journal of the Korea Concrete Institute
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• v.14 no.1
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• pp.118-125
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• 2002

Hydration is the main reason for the growth of the material properties. An exact parameter to control the chemical and physical process is not the time, but the degree of hydration. Therefore, it is reasonable that development of all material properties and the formation of microstructure should be formulated in terms of degree of hydration. Mathematical formulation of degree of hydration is based on combination of reaction rate functions. The effect of moisture conditions as well as temperature on the rate of reaction is considered in the degree of hydration model. This effect is subdivided into two contributions: water shortage and water distribution. The former is associated with the effect of W/C ratio on the progress of hydration. The water needed for progress of hydration do not exist and there is not enough space for the reaction products to form. The tatter is associated with the effect of free capillary water distribution in the pore system. Physically absorption layer does not contribute to progress of hydration and only free water is available for further hydration. In this study, the effects of chemical composition of cement, W/C ratio, temperature, and moisture conditions on the degree of hydration are considered. Parameters that can be used to indicate or approximate the real degree of hydration are liberated heat of hydration, amount of chemically bound water, and chemical shrinkage, etc. Thus, the degree of heat liberation and adiabatic temperature rise could be determined by prediction of degree of hydration.

• Transactions of the Korean hydrogen and new energy society
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• v.24 no.3
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• pp.237-241
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• 2013

The correlation between NiO-YSZ microstructure and its electrical property used for SOFC anode was critically evaluated with image processing and direct measurement techniques. These innovative processing techniques were employed to quantify the contiguity of the anode constituent phase. The calculated contiguities were then correlated with electrical conductivity attained from 4-probe DC method. This investigation described that contiguity of nickel oxide phases of an anode has a linear relationship with its electrical conductivity. We observed that the contiguity of NiO increased from 0.18 to 0.50 then electrical conductivity attained was significantly increased from 520 S/cm to 1468 S/cm at $900^{\circ}C$.

• Composites Research
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• v.17 no.3
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• pp.1-7
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• 2004

In the vacuum assisted RTM (VARTM) process that has become the center of attention for manufacturing massive composite structures, a good evacuation of air in the fiber preform is recognized as the prime factor. The microvoids, or the dry spots, are formed as a result of improper gate/vent locations and the mold geometry. The non-uniform resin velocity at the flow front leads to the formation of microvoids in the fibers, whereas the air in the microvoids can migrate along with the resin flow during mold filling. The residual air in the internal voids of a composite structure may cause a degradation of the mechanical properties as well as the structural failure. In this study, a unified macro- and micro analysis methods were developed to investigate the formation and transport of air in resin during VARTM process. A numerical simulation program was developed to analyze the three-dimensional flow pattern as well as the macro- and microscopic distribution of air in a composite part fabricated by VARTM process.

• Transactions of Materials Processing
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• v.14 no.4 s.76
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• pp.384-391
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• 2005

The nickel-based alloy Nimonic 80A possesses the excellent strength, and the resistance against corrosion, creep and oxidation at high temperature. Its products are used in aerospace engineering, marine engineering and power generation, etc. Control of forging parameters such as strain, strain rate, temperature and holding time is important because change of the microstructure in hot working affects the mechanical properties. Change of the microstructure evolves by recovery, recrystallization and grain growth phenomena. The dynamic recrystallization evolution has been studied in the temperature range of $950\~1250^{\circ}C$ and strain rate range of $0.05\~5s^{-1}$ using hot compression tests. The metadynamic recrystallization and grain growth evolution has been studied in the temperature range of $950\~1250^{\circ}C$ and strain rate range $0.05,\;5s^{-1}$, holding time range of 5, 10, 100, 600 sec using hot compression tests. Modeling equations are proposed to represent the flow curve, recrystallized grain size, recrystallized fraction and grain growth phenomena by various tests. Parameters in modeling equations are expressed as a function of the Zener-Hollomon parameter. The modeling equation for grain growth is expressed as a function of the initial grain size and holding time. The modeling equations developed were combined with thermo-viscoplastic finite element modeling to predict the microstructure change evolution during hot forging process. The grain size predicted from FE simulation results is compared with results obtained in field product.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.34 no.12
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• pp.1909-1915
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• 2010

The material properties of gas turbine components change during the daily start/stop thermal cycle because of exposure to the hot combustion gas. Recently, single-crystal Ni-based superalloys have been used to manufacture many hot-gas components for gas turbines. However, the user needs to depend on the manufacturer for maintenance issues because of the lack of data required for predicting blade life and material degradation. In this study, we investigate the time-dependent degradation of first-stage blades at various operating facilities to collect the basic data for life assessment and damage analysis. The blade material is a single-crystal Ni-based superalloy, CMSX-4, and the EOH (equivalent operating hours) are 25,000 and 52,000, respectively. We prepared the test specimen directly from used blades and carried out mechanical tests and microstructural observations.

• Transactions of the Korean hydrogen and new energy society
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• v.28 no.5
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• pp.521-530
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• 2017

Improving the microstructure of NiO/YSZ is one of several approaches used to enhance the electrical and mechanical properties of an anode support in Solid Oxide Fuel Cells (SOFCs). The aim of the work reported in this paper was to predict the relationship between these microstructural changes and the resulting properties. To this end, modification of the anode microstructure was carried out using different sizes of Poly (Methyl Methacrylate) (PMMA) beads as a pore former. The electrical conductivity and mechanical strength of these samples were measured using four-probe DC, and three-point bend-test methods, respectively. Thermal etching followed by high resolution SEM imaging was performed for sintered samples to distinguish between the three phases (NiO, YSZ, and pores). Recently developed image analysis techniques were modified and used to calculate the porosity and the contiguity of different phases of the anode support. Image analysis results were verified by comparison with the porosity values determined from mercury porosimetry measurements. Contiguity of the three phases was then compared with data from electrical and mechanical measurements. A linear relationship was obtained between the contiguity data determined from image analysis, and the electrical and mechanical properties found experimentally. Based upon these relationships we can predict the electrical and mechanical properties of SOFC support from the SEM images.

• Journal of Welding and Joining
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• v.28 no.3
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• pp.104-113
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• 2010

In this study, to predict the microstructure in weld HAZ of low alloyed steel, prediction model for the phase transformation considering the influence of prior austenite grain size and cooling rate was developed. For this study, six low alloyed steels were designed and the effect of alloying elements was also investigated. In order to develop the prediction model for ferrite transformation, isothermal ferrite transformation behaviors were analyzed by dilatometer system and 'Avrami equation' which was modified to consider the effect of prior austenite grain size. After that, model for ferrite phase transformation during continuous cooling was proposed based on the isothermal ferrite transformation model through applying the 'Additivity rule'. Also, start temperatures of ferrite transformation were predicted by $A_{r3}$ considering the cooling rate. CCT diagram was calculated through this model, these results were in good agreement with the experimental results. After ferrite transformation, bainite transformation was predicted using Esaka model which corresponded most closely to the experimental results among various models. The start temperatures of bainite transformation were determined using K. J. Lee model. Phase fraction of martensite was obtained according to phase fractions of ferrite and bainite.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.24 no.9 s.180
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• pp.2381-2386
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• 2000

Surface replication is playing an important role in the assessment of creep damage and remaining life of high temperature components. As the replication procedures, however, have not been standardized in domestic industry, its standardization is proposed in this study. For this purpose, the 2.25Cr-IMo steel was heat treated(5 min at 1,300 0C and oil quenched) to produce a simulated HAZ microstructure, and crept in air at 575 0C and under 120 MPa to produce artificial cavities. Then, the effect of surface preparation procedures on the quality of replicas was investigated using this sample. As a result, it was demonstrated that the presence of cavities may be observed readily or missed depending on the surface preparation procedures followed. Therefore it is essential to repeat three polishing/etching cycles at least in order to reveal cavitation damage accurately, even though it may be tedious or time-consuming.

• Transactions of Materials Processing
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• v.9 no.1
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• pp.72-79
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• 2000

Dynamic recrystallization (DRX), which may occur during hot deformation, is important for the microsturctural evolution of 304 stainless steel. Especially, the current interest in modelling hot rolling demands quantitative relationships among the thermomechanical process variables, such as strain, temperature, strain rate, and etc. Thus, this paper individually presents the relationships for flow stress and volume fraction of DRX as a function of processing variables using torsion tests. The hot torsion tests of 304 stainless steel were performed at the temperature range of 900~110$0^{\circ}C$ and the strain rate range of 5x10-2~5s-1 to study the high temperature softening behavior. For the exact prediction of flow stress, the equation was divided into two regions, the work hardening (WH) and dynamic recovery (DRV) region and the DRX region. Especially, The flow stress of DRX region could be expressed by using the volume fraction of DRX (XDRX). Since XDRX was consisted of the critical strain($\varepsilon$c) for initiation of dynamic recrystallization (DRX) and the strain for maximum softening rate ($\varepsilon$*), that were related with the evolution of microstructure. The calculated results predicted the flow stress and the microstructure of the alloy at any deformation conditions well.