• Journal of the Society of Cosmetic Scientists of Korea
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• v.39 no.2
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• pp.89-96
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• 2013

This study demonstrate that polymeric microspheres composed of poly (ethylene adipate) (PEA) and poly (methyl methacrylate) (PMMA) can encapsulate and remarkably stabilize Broussonetia kazinoki root extract. We compared the long-term stability and the activity of Broussonetia kazinoki root extract in polymeric microspheres fabricated with different polymer ratio of PEA and PMMA. PMMA was incorporated to the PEA microsphere in order to reinforce the physical strength of microsphere, and there was no noticeable negative effect on the activity of Broussonetia kazinoki root extract. Optical microscope (OM), polarized microscope (PM), and scanning electron microscope (SEM) results showed that PMMA incorporated microspheres were very spherical and had smoothsurface. On the other hand, PEA microspheres showed relatively irregular morphology due to the low physical strength of microspheres. Moreover, the mushroom tyrosinase activities were measured for testing the inhibitory activity of Broussonetia kazinoki root extract encapsulated in polymeric microspheres, and these microspheres showed the effective suppression of mushroom tyrosinase activity. Consequently, polymeric microspheres produced in this study may be beneficial for the research of improving stability and protecting labile substances incorporated into the polymeric microspheres.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2009.06a
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• pp.384-384
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• 2009

에폭시 수지에 유기화된 층상실리케이트 나노입자를 1wt% 충진한 경우 나노콤포지트와 마이크로 입자를 50wt% 충진한 경우 마이크로 콤포지트를 제조하였다. 초음파 분산법을 이용하여 나노 및 마이크로입자를 120분 동안 분산시킨 에폭시- 나노/마이크로 콤포지트이다. 나노콤포지트와 마이크로콤포지트의 단시간 교류절연파괴특성을 조사하기 위해 와이블 분포 plot을 통하여 나타내었다. 와이블 plot은 기울기로서 형상파라미터를 나타낸 경우로서 이는 파괴강도의 균질성을 의미하게 된다. 63.2% 누적분포함수를 나타낸 경우 척도파라미터로서 나타내어진다. 마이크로 콤포지트의 경우 형상파라미터가 2.99, 나노콤포지트는 8.96를 나타내었다. 또한 마이크로 콤포지트 및 나노콤포지트 스케일 파라미터는 164.25kV/mm, 245kV/mm를 얻었다. 또한 B10수명의 경우 마이크로콤포지트와 나노콤포지트의 경우 77.57kV/mm, 139.3 6kV/mm로서 나노콤포지트의 경우 완전하게 박리가 일어난 경우이다. 마이크로 입자를 분산시켜 입자간거리와 나노입자를 분산시켜 박리가 일어난 경우 입자간거리는 대단히 큰 차이를 나타내고 있다. 나노입자가 교번전계 하에서 주입된 전하 및 케리어 이동을 억제하는 경우로 이와같은 결과를 얻을 수 있다.

• Applied Chemistry for Engineering
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• v.35 no.2
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• pp.96-99
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• 2024

A sintering paste for bonding copper plates was synthesized using Cu formate nanofibers on Cu microparticles, mixed with formic acid. Copper oxide nanofibers of 10 ㎛ grown at 400 ℃ on Cu microparticles on the surface were transformed into copper formate nanofibers through the mixing of formic acid. Compared to Cu bulk particles or nanoparticles, Cu formate on Cu microparticles decomposed into metallic Cu at a lower temperature of 210 ℃, facilitating the sintering of copper paste. The growth of nanofiber on Cu microparticles allowed for an increase in the reaction rate of formation to copper formate, aggregating surface area, and decomposition rate of copper formate, resulting in fast sintering.

• Proceedings of the Optical Society of Korea Conference
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• 2002.07a
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• pp.108-109
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• 2002

Optical tweezers는 광압(radiation pressure)을 사용하여 입자들을 포획하거나 조절할 수 있다는 점에서 마이크로스케일의 유전체구뿐만 아니라 세포에서도 널리 사용되고 있다. 일반적으로 빛이라는 것은 광자들의 집합체로서 광자의 입자성으로 인하여 외부의 물체와 충돌시 운동량을 전달하게 되고 이것을 광압(radiation pressure)이라고 하며 optical tweezers [1]는 이 광압을 이용한 방법중 하나이다. 레이저빔을 입자에 집속 시켜 주게 되면 입자는 광압에 의해서 gradient force와 scattering force의 힘을 받게 된다. (중략)

• Proceedings of the KIEE Conference
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• 2009.07a
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• pp.1375_1377
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• 2009

PD의 저항성은 에폭시원형을 포함한 3종류 즉, 에폭시 마이크로 콤포지트를 실란처리 및 미처리한 경우 그리고 나노-마이크로입자가 혼합된 콤포지트의 부분방전저항성을 연구하였다. 이들 재료들은 rod - gap - plane 전극 하에서 PD가 적용되었다. 원형에폭시수지보다 마이크로 콤포지트가 부분방전저항성이 우월하였다. 더욱이 SiO2 나노입자-마이크로 혼합된 콤포지트가 더욱더 큰 저항성을 얻었다. 이는 마이크로 입자사이로 나노입자가 치밀한 조직을 갖고 있기에 이러 우월한 특성을 나타낸 것으로 판단된다.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.19 no.6
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• pp.147-153
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• 2018

PLGA microcapsule particles encapsulating BSA aqueous solutions were prepared using a water-in-oil-in-water emulsion method. The morphology, particle size, BSA encapsulating efficiency, and in-vitro release test were also studied using the microcapsule particles. In the outer aqueous phase, an emulsifier, e.g., PVA, was replaced with metal salts for surface solidification. Scanning electron microscopy (SEM) showed that the microcapsule particles had smooth surfaces and were between $1{\mu}m$ and $7{\mu}m$ in size. The microcapsule particle morphology was affected directly by the ratio between the polymer solution and inner aqueous solution, and composition of the outer aqueous solution. The factors also partially affected the BSA encapsulation efficiencies and in-vitro release rates. All the microcapsule particles showed an initial burst release through the in-vitro release test. On the other hand, the particles also showed a relatively long release period. Metal salts could be good choices to replace the emulsifier to solidify the microcapsule particle surfaces.

• Analytical Science and Technology
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• v.29 no.5
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• pp.225-233
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• 2016

The chemical engrafting of polymers on particle surface, plays an important role on selective partitioning of micro/nano-particles in the separated layers of liquid media, such as aqueous two phase systems (ATPSs). Three polymers, dextran, poly (ethylene glycol) and albumin were chosen and chemically conjugated to the polystyrene (PS) magnetic microparticle surface. The attachment of long-chained polymer chains which may switch the partition behavior, can be simply performed by S_N2 substitution of various polymers having primary amine functional groups, with p-toluenesulfonyl (tosyl)-activated polystyrene magnetic micro-particles. The surface modification of microparticle was probed by infrared microscopy. The distinctive peak represents N-H stretching vibration mode for microparticles after the reaction and it is common for all three polymers examined. The locations of main peaks are similar for all micro-particles but different and distinguishable in fingerprint region.

• Journal of the Korean Society of Propulsion Engineers
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• v.15 no.6
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• pp.15-25
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• 2011

One dimensional combustion modeling of aluminum combustion behavior is proposed. Combustion model is assumed that region consists as follows ; preheat, reaction, post reaction region. Flame speed as a function of particle size, equivalence ratio for unitary particles and fraction ratio of micro to nano particle size for binary particles were investigated for lean burn condition at 1 atm. Results were compared with experimental data. For unitary particles, flame speed increase as particle size decreases, but opposite trend with equivalence ratio. For binary particles, flame speed increases proportionally as nano particle fraction increases. For flame structure, separated or overlapping flames are observed, depending on the fraction of nano sized particles.

• Proceedings of the Korean Society of Laser Processing Conference
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• 2002.11a
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• pp.105-108
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• 2002

• Proceedings of the International Microelectronics And Packaging Society Conference
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• 2001.11a
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• pp.185-188
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• 2001

본 연구는 알루미늄 기판 위에 징케이트 처리 시 생성되는 아연 입자들의 성장거동에 관하여 연구하였다. 알루미늄 기판 상에서 아연입자들은 기판 표면의 요철 꼭지점이나 모서리에서 먼저 생성되었고, (0001)면들이 적층되어 성장하였다. 또한 온도를 증가에 따른 성장속도를 증가시켜 징케이트 처리를 실시하였을 때 육방정계을 갖는 아연 입자의 경우 <1100> 결정방향으로 성장이 이루어져 불가사리 형태의 입자형태를 나타내었으며 초음파 교반에 의한 징케이트 처리를 하였을 경우 조밀하고 균일한 아연 막을 형성하였다.