• Title/Summary/Keyword: 대체 시험법

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A Study on Developing of Soldering Flux (납땜 플럭스 개발에 관한 연구)

  • 이통영
    • Fire Science and Engineering
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    • v.14 no.2
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    • pp.33-38
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    • 2000
  • Flux, essentially used in soldering process of PCB (Printed Circuit Board) in electronics industry, contains IPA (Isopropyl alcohol) and methanol, which are highly inflammable and explosive. Hazard Chemical Controlling Law classified methanol as toxic material and Environmental Law classified methanol as VOC (Volatile Organic Compound). So there have been pressing needs of developing substitutes for the existing Flux. New solvent which is non-flammable and main component is DCP having same specific character of the existing Flux. It's been combirated with proper composition ratio adding stabilizer. As a result, it relieved working Environment Allowance thickness 200 ppm to 470 ppm, chance of not been soldered 0.083% to 0%, spread 85% to 87%, power saving resistance 1.0$\times$$10^{12}$$\Omega$ to 6.9$\times$$10^{12}$$\Omega$, which means a lot better than the existing Flux. Therefore, Flux confirmed the chance of improving productivity, safety, environment safety and quality. Also, Flux got a satisfied result after product quality test and product reliability test.

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The Effects of High Pressure Water Contact State on Hydraulic Fracturing (고압수 접촉상태가 수압파쇄에 미치는 영향)

  • Lee, Sang Hun;Lim, Jong Se;Jang, Won Yil
    • Tunnel and Underground Space
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    • v.26 no.5
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    • pp.409-417
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    • 2016
  • The shale gas is emerging as one of the oil and gas resources which can replace the traditional oil and gas resources. As the shale layer where the shale gas is deposited has low permeability, the hydrofracturing method is required to improve the productivity. This study is designed to conduct the laboratory hydrofracturing test on the samples which are modeled after the drilling hole having the general drilling hole and spiral groove. And compare the initial fracturing pressure and fluid contact between them in order to the result of the hydrofracturing depending on the shape of the drilling hole. In addition, the results were compared with the numerical modeling values from 3DEC and they were also compared with the data from the advance researches. It was found from the study that rather than the contact area of the high pressures water, the force concentration depending on the form of guide hole was more effective in the hydrofracturing.

Physical Properties and Sulfur Absorption Capacity of Spray-dried Solid Sorbents for Desulfurization of Syngas (합성가스 중 $H_2S$ 정제용 탈황제의 물성 및 반응특성)

  • Baek, Jeom-In;Lee, Joong-Beom;Kim, Ji-Woong;Eom, Tae-Hyoung;Ryu, Jeong-Ho;Jeon, Won-Sik;Ryu, Chong-Kul
    • 한국신재생에너지학회:학술대회논문집
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    • 2009.06a
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    • pp.880-883
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    • 2009
  • 석탄가스화복합발전(IGCC) 시스템에서 합성가스 중에 포함된 황화수소($H_2S$)는 후단의 가스 터빈과 같은 장치의 부식을 방지하고, 합성가스를 이용하는 연료전지 등의 연계 공정에서 요구하는 수준에 맞추어 정제되어야 한다. 본 연구에서는 $H_2S$ 정제공정 추가에 따른 IGCC 시스템의 효율저하를 최소화하기 위하여 고온고압에서 사용가능한 탈황제를 분무건조법을 이용하여 제조하고 제조된 탈황제에 대해 물성 및 황 흡수능 시험을 실시하였다. 형상, 내마모도, 평균입자크기, 충진밀도와 함께 제조된 탈황제가 적용되는 유동층 공정에 적합한 강도를 보유하는지 여부를 미국표준시험방법에 의하여 측정하였다. 황 흡수능은 열중량분석기를 반응기로 사용하여 모사 합성 가스 분위기에서 측정하였다. 분무건조 성형된 탈황제의 일부가 구형이 아닌 타원형 또는 도넛 형태를 나타내고 있어 형상 개선을 위한 제조방법 개선이 필요한 것으로 나타났다. 제조된 탈황제는 기공도가 65% 이상으로 macropore가 기공부피의 대부분을, mesopore가 비표면적의 대부분을 제공하고 있었다. 소성온도를 650 $^{\circ}C$에서 750 $^{\circ}C$로 증가시킴에 따라 대체로 강도가 감소하는 경향을 나타내었다. 열중량분석기로 측정된 황 흡수능은 약 10 wt%로 나타났다. 제조된 탈황제 중 일부는 유동층 공정에 적합한 물성을 보유하고 있었으며 반응성 또한 기존에 개발된 탈황제에 버금가는 성능을 나타내어 향후 공정 적용이 가능할 것으로 분석되었다.

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Basic Characteristics and Application of Modern Dancheong Pigment Jangdanyuksaek (Incarnadine) (현대 단청용 장단육색의 기본 특성 및 사용 기준 연구)

  • Kim, Eun Ji;Chung, Kwang Yong
    • Journal of Conservation Science
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    • v.31 no.4
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    • pp.457-476
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    • 2015
  • This study is expected to present instructions and analysis of Modern Dancheong pigments by its physical characteristics. Search pigments currently used and experiments proper mixing ratio of Jangdanyuksaek(Incarnadine). Samples are made by based on presented a mixture ratio which is less exfoliation, cracks and color change. And put into accelerated weathering test and ultraviolet ray degradation test. As a result in case of Jidang($TiO_2$) Rutile type is superior in discoloration and durability. Rutile type makes color difference remarkably because of oil absorption difference while mixing with Jangdan. Water paints which are used as a alternative present yellowness which means water paints lack in durability. whiting should be taken carefully as it has high brightness after degradation.

Studies on the evaluation of efficacy of functional cosmetics(I) -Studies on the in vitro SPF test method of sunscreen products (기능성화장품의 기능성평가에 관한 연구(I) -자위선차단화장품의 in vitro 시험법 연구)

  • 손경훈;김영옥;이정표;양성준;백옥진;김원희;김종갑;허문영;최상숙
    • Journal of the Society of Cosmetic Scientists of Korea
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    • v.28 no.3
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    • pp.171-184
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    • 2002
  • The present study was undertaken to develop the in vitro sunprotection factor(SPF) measurement method having good correlation with in vivo method. As in vitro method, 8% homomentyl salicylate, P3 reference standard and sunscreens on market were measured using SPF 290 analyzer and were compared the SPF with labed value. In vitro SPF of 8% HMS and P3 reference standard were 4.59 $\pm$ 0.12 and 14.94 $\pm$ 0.83. There are good correlation, correlation factor were 0.9506 and 0.9769 respectively, between the in vitro and in vivo SPF for the sunscreen creams and lotions examined. Correlation factors of makeup base & liquid goundation, lotion labled with “shake before use”, compact powder were 0.8812, 0.8632 and 0.5984. The best sample applied method of compact powder was 1:0.8 mixture with cream base. These results suggest that the in vitro test method could be used as an alternative method for SPF.

Evaluation of Local Lymph Node Assay as an Alternative Method for Skin Sensitization Potential in Baltic Mice (Balb/c 마우스에서 Local Lymph Node Assay(LLNA)를 01용한 피부 감작성 시험 대체시험법 연구)

  • 이종권;황인창;박재현;김형수;정승태;엄준호;오혜영
    • Toxicological Research
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    • v.18 no.2
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    • pp.175-181
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    • 2002
  • Allergic contact dermatitis (skin sensitization) may be caused by a wide variety of chemicals. A murine local lymph node assay (LLNA) has been developed as an alternative to guinea pig models for assessing the contact sensitization potential of chemical. This study was carried out to evaluate the skin sensitization potential for chemicals in Balb/c mice by LLNA. Contact allergen, dinitrochlorobenzene (DNCB), respiratory allergen, toluene diisocyanate (TDI) and a weak allergen, $\alpha$-hexlycinnamaldehyde (HCA) were wed as positive chemicals and irritant, sodium lauryl sulfate(SLS) also wed as a reference chemical in this study. The weights of lymph node in the mice treated with DNCB, TDI, and HCA were increased compared to vehicle control. There was a significant increase in lymph node weight of mice treated with high concentration of SLS compared to vehicle control. The stimulation index (SI) of Lymph node cell in the mice treated with DNCB, TDI, and HCA revealed over three-fold increase compared to vehicle control by $3^H$-thymidine uptake. All allergens correctly identified in this LLNA study wing Balb/c mice. These results suggest that LLNA wing Balb/c mice could be a useful method for screening the allergenic potential of chemicals. The expression of IL-2 mRNA was slightly increased in draining auricular lymph node cell of the mice treated with TDI and HCA by RT-PCR. However the IL-2 levels in DNCB and SLS of treated animals were not significantly changed.

Reliability assessment of RPCB and FPCB Joints bonded using Thermo-compression (열 압착으로 접합된 RPCB와 FPCB 접합부의 신뢰성 평가)

  • Jang, Jin-Kyu;Lee, Jong-Gun;Lee, Jong-Bum;Ha, Sang-Su;Jung, Seung-Boo
    • Proceedings of the KWS Conference
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    • 2009.11a
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    • pp.81-81
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    • 2009
  • 최근 휴대폰, 노트북 등과 같은 소형 멀티미디어 기기의 사용이 증가함에 따라 전자 패키징 산업은 경박단소화를 요구하고 있습니다. 더불어 전기적 신호의 손실을 줄이기 위해 전기, 전자산업체에서는 가볍고 굴곡성이 우수한 연성인쇄회로기판(Flexible Printed Circuit Board, FPCB)과 가격이 싸고 신뢰성이 입증된 경성인쇄회로기판(Rigid Printed Circuit Board, RPCB)의 전극간 접합에 많은 관심을 보이고 있습니다. 기존에 연성인쇄회로기판과 경성인쇄회로기판을 접합하는 방식으로는 connector를 이용한 체결법이 사용되고 있지만 완성품의 부피가 커지고 자동화 공정이 힘들며 I/O 개수가 제한적이어서 신호전달에 취약한 단점이 있습니다. 또한, 최근 FPCB를 RPCB에 접합하는데 interconnection으로 이방성 도전 필름(Anisotropic conductive film, ACF) 또는 비전도성 필름(Non-conductive film)이 널리 사용되고 있습니다. 하지만 필름의 가격이 비싸고, 낮은 전기 전도도를 보이며, 신뢰성 특성이 낮다는 단점을 가지고 있습니다. 본 실험에서는 기존의 connector 방식과 접착 필름을 이용한 방식을 대체하기 위하여 솔더를 interlayer로 이용하여 열과 압력으로 접합하는 방법에 대하여 연구하였습니다. 실험에 사용된 솔더의 조성은 Sn-3.0Ag-0.5Cu (in wt%)이고, RPCB와 FPCB의 표면처리는 ENIG로 하였습니다. 접합 온도와 접합 시간에 따라 최적의 접합 조건을 도출하고자 하였고, 접합된 시편을 가지고 신뢰성 테스트를 진행하였습니다. $85^{\circ}C$/85% 고온고습 시험과 고온 방치 시험을 통하여 접합부의 신뢰성을 테스트 하였고, 90도 Peel test로 기계적 접합 강도를 측정하였고, 파괴 단면을 Scanning Electron Microscopy (SEM), Energy-dispersive spectroscopy (EDS), X-ray photoelectron spectroscopy (XPS)로 분석하였습니다.

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Analytical and Experimental Study for Development of Composite Coil Springs (복합재 코일스프링 개발을 위한 수치해석 및 실험적 연구)

  • Oh, Sung Ha;Choi, Bok Lok
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.38 no.1
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    • pp.31-36
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    • 2014
  • This paper shows the feasibility of using carbon-fiber-reinforced polymer (CFRP) composite materials for manufacturing automotive coil springs. For achieving weight reduction by replacing steel with composite materials, it is essential to optimize the material parameters and design variables of the coil spring. First, the shear modulus of a CFRP beam model, which has $45^{\circ}$ ply angles for maximum torsional stiffness, was calculated and compared with the test results. The diameter of the composite spring was predicted to be 17.5 mm for ensuring a spring rate equal to that when using steel material. Finally, a finite element model of the composite coil spring with $45^{\circ}$ ply angles and 17.5 mm wire diameter was constructed and analyzed for obtaining the static spring rate, which was then compared with experimental results.

Antimicrobial Effects of Essential Oils for Multidrug-Resistant Acinetobacter baumanii (다제내성 아시네토박터 바우마니의 에센셜 오일에 대한 항균효과)

  • Park, Chang-Eun;Kwon, Pil Seung
    • Korean Journal of Clinical Laboratory Science
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    • v.50 no.4
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    • pp.431-437
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    • 2018
  • Acinetobacter baumannii is categorized as a red alert pathogen that is increasingly associated with a high mortality rate in infected patients because of its resistance to extensive antibiotics. This study evaluated the antibacterial activities of some essential oils (tee tree, rosemary, and lavender oils) against 18 clinical isolates of multidrug-resistant A. baumannii (MRAB). The carbapenemase screening Hodge test showed that all 20 strains of A. baumannii were resistant to imipenem. The identification of multidrug-resistant microbes was carried out using the VITEK system. The antimicrobial activity of essential oils was tested by a disk diffusion method against MRAB. In the disk diffusion method, tea tree showed the largest increase in inhibition size compared to lavender oil, and rosemary had no antibacterial effect. These results proved the antimicrobial effect of multidrug resistance A. baumannii. Tee tree oil would be a useful alternative natural product for the treatment and prevention of most common human pathogens and MRAB infections. This is expected to be used as an antimicrobial agent, such as hand disinfectant using natural essential oil in the future.

A Study on the Improvement of the Stability of Small-Scale Manpower Tunnels for Food Storage (식품저장용 소규모 인력터널의 안정성 향상을 위한 방안 연구)

  • Byung Jo Yoon;Sung Yun Park;Ryung Hwan Kim
    • Journal of the Society of Disaster Information
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    • v.18 no.4
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    • pp.746-753
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    • 2022
  • Purpose: The purpose of this study is to review the safety of small tunnels for food storage excavation in the 1960s~1970s and to improve the stability of small tunnels. Method: A visual inspection and a hammer test were used to conduct safety tests, and the visual inspection is one of the tests conducted for non-destructive testing, and the hammer test is one of the types of hitting methods of rebound hardness. Result: According to the integrated analysis of the survey area data, there are generally good appearance, but there are many small cracks and complex geological conditions, requiring continuous observation and attention. Seven of the 23 tunnels require safety diagnosis, one collapse, one safe, and 14 require continuous observation and attention. Conclusion: All parts of small tunnels should be checked and recorded from time to time, and stability is expected to be improved when reinforcing small tunnels proposed in this study.