• Journal of the Korean Applied Science and Technology
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• v.24 no.2
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• pp.174-181
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• 2007

In this study, $SiO_2/poly(ethylene-co-vinyl$ alcohol)(EVOH) hybrid coating materials with gas barrier property could be produced using sol-gel method. The biaxially oriented polypropylene (BOPP) substrate with surface pretreatment was coated with the prepared hybrid sols containing various inorganic silicate component by a spin coating method. Crystallization behavior of the hybrids was investigated in terms of analysis of X-ray diffraction and cooling thermogram from DSC experiment. From the morphological observation of the $SiO_2/EVOH$ hybrid gel, it was confirmed that there existed an optimum content of inorganic silicate precursor, Tetraethylorthosilicate (TEOS), to produce hybrid materials with dense microstructure, exhibiting uniformly dispersed silica particles with average size below 100 nm. When TEOS was added at below or above the optimum content, particle clusters with large domain were observed, resulting in phase separation. This morphological result was found to be in good agreement with that of oxygen permeability of the hybrid coated films. In the case of film coated with hybrid prepared from addition of 0.01 - 0.02mol of TEOS, a remarkable improvement in barrier property could be obtained, however, with the addition of TEOS more than 0.04 mol, the barrier property was dramatically reduced because of phase separation and micro-crack formation on the film surface.

• Journal of the Korean Ceramic Society
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• v.31 no.5
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• pp.513-519
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• 1994

Alumina composite was fabricated by introducing tetragonal ZrO2 in alumina composite of $\alpha$-alumina reinforced with in-situ formed La-$\beta$-aluminate (LaAl11O18). The powder mixture of composition (100-x)[88 Al2O3+(La2O3+11 Al2O3)]+x vol% ZrO2 was prepared with x from 0 to 40. Dense composites fabricated by hot-pressing exhibited bending strength up to 1200 MPa. The gain growth inhibiting effect of ZrO2 grains and La-$\beta$-aluminate platelets, and possibly the stress-induced phase transformation of ZrO2 have resulted in the high bending strength. The fracture toughness of the composite also increased up to 8.5 MPa.m1/2. The enhancement in toughness can be explained by transformation and microcrack toughening of ZrO2 and by crack deflection and bridging of La-$\beta$-aluminate platelets and ZrO2.

• Korean Journal of Materials Research
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• v.10 no.2
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• pp.111-116
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• 2000

Fracture mode and carbide reactions of cast alloy 738LC during thermal exposure and creep at 816$^{\circ}C$/440MPa and 982$^{\circ}C$/152MPa were investigated. Crystallographic transgranular failure was observed in the specimen crept at 816$^{\circ}C$ due to shearing on the slip plane. Because selective oxidation at the grainboundaries which was exposed at the surface leads reduction in surface energy, however, early initiation of crack at the grainboundaries and intergranular failure were observed in the specimen crept at 982$^{\circ}C$/152MPa. As a result of decomposition of MC carbide at the tested temperatures, M(sub)23C(sub)6 carbide precipitated either on the grainboundaries or on the deformation band. The applied stress enhanced decomposition of MC. $\sigma$phase nucleated from Cr(sub)23C(sub)6 then grew to the ${\gamma}$+${\gamma}$\\` matrix. Precipitation of $\sigma$was accelerated by increasing temperature and applied stress.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.22 no.3
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• pp.579-587
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• 1998

In this study, fatigue behavior of the optical fiber sensor embedded in composite laminate was investigated. Static tensile and fatigue tests were performed for three types of laminated composite specimens with embedded optical fiber sensor in the neutral plane ; [0/sub 6//OF/0/sub 6/]/sub T/, [0/sub 2//90/sub 4//OF/90/sub 4//0/sub 2/]/sub T/ and [0/sub 3//90/sub 3//OF/90/sub 3//0/sub 3/]/sub T/. The fracture of the embedded optical fiber sensor was detected by the intensity drop off of laser signal transmitted through the optical fiber sensors embedded within laminated composite specimen. The maximum fatigue stress applied to laminated specimen was compared with the average tensile stress at which the fracture of the embedded optical fiber within the laminate occurred under static tensile loading. From the experiments, firstly it is observed that the decrease in the life of optical fiber sensors embedded within unidirectional-ply laminate by the fatigue loading is relatively small compared to that of cross-ply laminate. Secondly, the optical fiber embedded in unidirectional-ply laminate is fractured by the fatigue damage due to the growth of internal defects of optical fiber, however the optical fiber embedded in cross-ply laminate is fractured by the growth of transverse matrix crack.

• Composites Research
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• v.15 no.2
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• pp.11-17
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• 2002

The piezoelectric thin film sensor can be used to interpret variations in structural and material properties, e.g. for structural integrity monitoring and assessment. To illustrate one of this potential benefit, PVDF (polyvinylidene fluoride) film sensors are used for monitoring impact damage in Gr/Ep composite panels. Both PVDF film sensors and strain gages are attached to the surface of Gr/Ep specimens. A series of impact tests at various impact energy by changing impact mass the height are performed on the instrumented drop weight impact tester. The sensor responses are carefully examined to predict the onset of impact damage such as indentation, matrix cracking, and delamination, etc. Test results show that the particular waveforms of sensor signals implying the damage initiation and development are detected above the damage initiation impact energy. As expected, the PVDF film sensor is found to be more sensitive to impact damage initiation event than the strain gage.

• Polymer(Korea)
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• v.24 no.4
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• pp.564-570
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• 2000

The waste FRP occured in the fabrication of SMC (sheet molding compound) bathtubs and the waste polyurethane foam occured in electronic manufacture and waste insulator were applied as a soundproof and light weight pannel in the waste FRP unsaturated polyester matrix resin composites to recycle. The effect of filler contents on the mechanical properties and interfacial phenomena of the filler and matrix on the composites was evaluated. The tensile strength of composites reached its maximum value of 82.34 MPa when the filler content was 70 wt%, and the more content of reinforcement is increased, the more tensile modulus was decreased. The flexural strength and modulus of composites, reinforced 70 wt% with filler content, were dominant compared to the other samples to 72.5 MPa, 958.4 MPa respectively. When composite of reinforced 70 wt% with filler content, it was confirmed that pull out phenomena and cracks did not occur in the interface of reinforcement and matrix resin through the SEM observation. Also, waste FRP and urethane foam were dispersed well into matrix resin as filler.

• Journal of the Korean Institute of Gas
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• v.5 no.2 s.14
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• pp.14-21
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• 2001

In order to investigate the damage mechanism of the coupler transferring LPG, microstructural observation and chemical analysis of the couplers operated for the long time in the LPG stations and virgin 6/4 forged-brass corrosion-tested were conducted. Their microstructure was consisted of two phases that bright $\beta$ precipitates were irregularly dispersed in $\alpha$ matrix. The chemical compositions of oxide layer on the surface of the used coupler were composed of S, C, O, Al, Si, etc. as well as Cu and Zn. In environmental corrosion tests of both $10\%$ HCl and Mattsson solutions, no apparent deviations in mechanical impact strength of forged-brass was observed. While, in U-bend stress corrosion cracking specimen, some microcracks were observed.

• Journal of the Korean Society for Nondestructive Testing
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• v.35 no.3
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• pp.179-184
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• 2015

In this study, the flap fatigue test of a 48 m long wind turbine blade was performed for 1 million cycles to evaluate the characteristics of acoustic emission signals generated from fatigue damage of the wind blades. As the number of hits and total energy continued to increase during the first 0.6 million cycles, blade damage was constant. The rise-time result showed that the major aspects of damage were initiation and propagation of matrix cracks. In addition, the signal analysis of each channel showed that the most seriously damaged sections were the joint between the skin and spar, 20 m from the connection, and the spot of actual damage was observable by visual inspection. It turned out that the event source location was related to the change in each channel's total energy. It is expected that these findings will be useful for the optimal design of wind turbine blades.

• Journal of the Computational Structural Engineering Institute of Korea
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• v.24 no.5
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• pp.577-588
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• 2011

This paper provides a novel extended Moving Least Squares(MLS) difference method for the potential problem with weak and strong discontinuities. The conventional MLS difference method is enhanced with jump functions such as step function, wedge function and scissors function to model discontinuities in the solution and the derivative fields. When discretizing the governing equations, additional unknowns are not yielded because the jump functions are decided from the known interface condition. The Poisson type PDE's are discretized by the difference equations constructed on nodes. The system of equations built up by assembling the difference equations are directly solved, which is very efficient. Numerical examples show the excellence of the proposed numerical method. The method is expected to be applied to various discontinuity related problems such as crack problem, moving boundary problem and interaction problems.

• Journal of the Korean Society for Nondestructive Testing
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• v.21 no.3
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• pp.251-260
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• 2001

Damage Profess of CFRP laminates under monotonic tensile test was characterized by the correlation between Acoustic Emission(AE) and Ultrasonic Test(UT). The amplitude distribution of AE signal from a specimens is an aid to the determination of the extent of the different fracture mechanism such as matrix crack, debonding, fiber pullout and fiber fracture as load is increased. In addtion, the characteristics of ultrasonic amplitude attenuation are useful lot analysis of the different type of fracture mechanism. Different orientation of carbon fiber reinforced plastic specimens were used to investigate the AE amplitude range and ultrasonic amplitude attenuation. Finally, loading-unloading tests were carried out to check Felicity effect. During the tests, ultrasonic amplitude attenuation was investigated at the same time and compared with AE parameters. The result showed that two parameters of both AE and UT could be effectively used for analysis of fracture mechanism in CFRP laminates.